# Electronic Supplementary Material (ESI) for Dalton Transactions.
# This journal is © The Royal Society of Chemistry 2018

####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_EuL-Monoclinic
_database_code_depnum_ccdc_archive 'CCDC 1589835'
_audit_update_record             
;
2017-12-07 deposited with the CCDC.
2018-02-05 downloaded from the CCDC.
;
#==============================================================================
_audit_creation_date             2017-11-27
_audit_creation_method           CRYSTALS_ver_14.61_build_6156

_oxford_structure_analysis_title 6769a
_chemical_name_systematic        .
_chemical_melting_point          'not measured'

_refine_special_details          
; 
This was the first attempt to collect data on this 
material, using a laboratory instrument.  The data were 
exceptionally weak and there were additional, even weaker 
reflections that could not be indexed.  The structure 
solved without these, but with two molecules in the 
asymmetric unit, there was a suspicion that the 
additional reflections might be indicative of a phase
transition.  Subsequent attempts led to the 
identification of additional solvates/polymorphs (vide
infra) and, given how difficult the material was to 
work and how little crystalline sample was available,
these data are included for comparison.

The difference map indicated the presence of diffuse electron
density believed to be disordered solvent.  SQUEEZE was used 
leaving a void 
from which the electron density was removed.
;

loop_
_platon_squeeze_void_nr
_platon_squeeze_void_average_x
_platon_squeeze_void_average_y
_platon_squeeze_void_average_z
_platon_squeeze_void_volume
_platon_squeeze_void_count_electrons
_platon_squeeze_void_content
1 0.121 0.662 -0.073 10523 4672 ' '
_platon_squeeze_void_probe_radius 1.20
_platon_squeeze_details          
; 
The discrete Fourier transform of the void region were treated as 
contributions to the A and B parts of the calculated structure factors.
;



_cell_length_a                   52.668(3)
_cell_length_b                   18.1007(6)
_cell_length_c                   32.7146(17)
_cell_angle_alpha                90
_cell_angle_beta                 106.632(6)
_cell_angle_gamma                90
_cell_volume                     29883(3)

_symmetry_cell_setting           monoclinic
_symmetry_space_group_name_H-M   'P 1 2/c 1 '
_symmetry_space_group_name_Hall  '-P 2yc'
loop_
_symmetry_equiv_pos_as_xyz
x,y,z
-x,-y,-z
-x,y,-z+1/2
x,-y,z+1/2

loop_
_atom_type_symbol
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_Cromer_Mann_a1
_atom_type_scat_Cromer_Mann_b1
_atom_type_scat_Cromer_Mann_a2
_atom_type_scat_Cromer_Mann_b2
_atom_type_scat_Cromer_Mann_a3
_atom_type_scat_Cromer_Mann_b3
_atom_type_scat_Cromer_Mann_a4
_atom_type_scat_Cromer_Mann_b4
_atom_type_scat_Cromer_Mann_c
_atom_type_scat_source
C 0.0181 0.0091 2.3100 20.8439 1.0200 10.2075 1.5886 0.5687 0.8650 51.6512
0.2156 'International Tables Vol C 4.2.6.8 and 6.1.1.4'
H 0.0000 0.0000 0.4930 10.5109 0.3229 26.1257 0.1402 3.1424 0.0408 57.7998
0.0030 'International Tables Vol C 4.2.6.8 and 6.1.1.4'
Eu -8.9294 11.1857 24.6274 2.3879 19.0886 0.1942 13.7603 13.7546 2.9227
123.1740 2.5745 'International Tables Vol C 4.2.6.8 and 6.1.1.4'
N 0.0311 0.0180 12.2126 0.0057 3.1322 9.8933 2.0125 28.9975 1.1663 0.5826
-11.5290 'International Tables Vol C 4.2.6.8 and 6.1.1.4'
O 0.0492 0.0322 3.0485 13.2771 2.2868 5.7011 1.5463 0.3239 0.8670 32.9089
0.2508 'International Tables Vol C 4.2.6.8 and 6.1.1.4'
Cl 0.3639 0.7018 11.4604 0.0104 7.1964 1.1662 6.2556 18.5194 1.6455 47.7784
-9.5574 'International Tables Vol C 4.2.6.8 and 6.1.1.4'


_cell_formula_units_Z            8

# Given Formula = C262.50 H325.50 Cl10.50 Eu10.50 N42 O94.50 
# Dc =      3.36 Fooo =  30324.00 Mu =    342.76 M =   7549.03
# Found Formula = C100 H131.99 Eu4 N16 O40 
# Dc =      1.25 FOOO =  11328.00 Mu =    124.22 M =   2806.06

_chemical_formula_sum            'C100 H132 Eu4 N16 O40'
_chemical_formula_moiety         'C100 H132 Eu4 N16 O40'
_chemical_compound_source        .
_chemical_formula_weight         2806.06


_cell_measurement_reflns_used    10323
_cell_measurement_theta_min      3
_cell_measurement_theta_max      72
_cell_measurement_temperature    150

_exptl_crystal_description       plate
_exptl_crystal_colour            clear_pale_colourless
_exptl_crystal_size_min          0.10
_exptl_crystal_size_mid          0.22
_exptl_crystal_size_max          0.40

_exptl_crystal_density_diffrn    1.247
_exptl_crystal_density_meas      'not measured'
_exptl_crystal_density_method    'not measured'
# Non-dispersive F(000): 
_exptl_crystal_F_000             11328
_exptl_absorpt_coefficient_mu    12.422

# Sheldrick geometric approximatio 0.07 0.29 
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   'CrysAlisPro, (Agilent, 2011)'
_exptl_absorpt_correction_T_min  0.02
_exptl_absorpt_correction_T_max  0.29
_diffrn_measurement_device_type  'Oxford Diffraction SuperNova'
_diffrn_measurement_device       Area
_diffrn_radiation_monochromator  graphite
_diffrn_radiation_type           'Cu K\a'
_diffrn_radiation_wavelength     1.54184
_diffrn_measurement_method       ω

# If a reference occurs more than once, delete the author 
# and date from subsequent references. 
_computing_data_collection       'SuperNova, (Oxford Diffraction, 2010)'
_computing_cell_refinement       'CrysAlisPro, (Agilent, 2011)'
_computing_data_reduction        'CrysAlisPro, (Agilent, 2011)'
_computing_structure_solution    'Superflip (Palatinus & Chapuis, 2007)'
_computing_structure_refinement  'CRYSTALS (Betteridge et al., 2003)'
_computing_publication_material  'CRYSTALS (Betteridge et al., 2003)'
_computing_molecular_graphics    'CAMERON (Watkin et al., 1996)'

_diffrn_standards_interval_time  .
_diffrn_standards_interval_count .
_diffrn_standards_number         0
_diffrn_standards_decay_%        .

_diffrn_ambient_temperature      150
_diffrn_reflns_number            176702
_reflns_number_total             61303
_diffrn_reflns_av_R_equivalents  0.128
_diffrn_reflns_av_sigmaI/netI    0.1643
# Number of reflections without Friedels Law is 81281 
# Number of reflections with Friedels Law is 61303 
# Theoretical number of reflections is about 41132 


_diffrn_reflns_theta_min         2.441
_diffrn_reflns_theta_max         77.123
_diffrn_measured_fraction_theta_max 0.968

_diffrn_reflns_theta_full        69.411
_diffrn_measured_fraction_theta_full 0.995


_diffrn_reflns_limit_h_min       -63
_diffrn_reflns_limit_h_max       66
_diffrn_reflns_limit_k_min       -10
_diffrn_reflns_limit_k_max       22
_diffrn_reflns_limit_l_min       -41
_diffrn_reflns_limit_l_max       40
_reflns_limit_h_min              0
_reflns_limit_h_max              66
_reflns_limit_k_min              -22
_reflns_limit_k_max              0
_reflns_limit_l_min              -41
_reflns_limit_l_max              39

_oxford_diffrn_Wilson_B_factor   5.73
_oxford_diffrn_Wilson_scale      48.73

_atom_sites_solution_primary     Other #heavy,direct,difmap,geom,iterative
# _atom_sites_solution_secondary  difmap
_atom_sites_solution_hydrogens   difmap

_refine_diff_density_min         -1.14
_refine_diff_density_max         2.75


# The current dictionary definitions do not cover the 
# situation where the reflections used for refinement were 
# selected by a user-defined sigma threshold 


# The values actually used during refinement 
_oxford_reflns_threshold_expression_ref I>3.0\s(I)
_refine_ls_number_reflns         15564
_refine_ls_number_restraints     8786
_refine_ls_number_parameters     2881
_oxford_refine_ls_R_factor_ref   0.1540
_refine_ls_wR_factor_ref         0.1812
_refine_ls_goodness_of_fit_ref   1.1332
_refine_ls_shift/su_max          0.0030034
_refine_ls_shift/su_mean         0.0002220


# The values computed with all filters except I/sigma 
_oxford_reflns_number_all        41071
_refine_ls_R_factor_all          0.2314
_refine_ls_wR_factor_all         0.2790

# The values computed with a 2 sigma cutoff - a la SHELX 
_reflns_threshold_expression     I>2.0σ(I)
_reflns_number_gt                23126
_refine_ls_R_factor_gt           0.1773
_refine_ls_wR_factor_gt          0.2135

# choose from: rm (reference molecule of known chirality), 
# ad (anomolous dispersion - Flack), rmad (rm and ad), 
# syn (from synthesis), unk (unknown) or . (not applicable). 
_chemical_absolute_configuration .


_refine_ls_structure_factor_coef F
_refine_ls_matrix_type           full
_refine_ls_hydrogen_treatment    constr #undef, noref, refall,
# refxyz, refU, constr or mixed
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
;
 Method, part 1, Chebychev polynomial, (Watkin, 1994, Prince, 1982) 
 [weight] = 1.0/[A₀*T₀(x)+A₁*T₁(x) ... +Aₙ₋₁]*Tₙ₋₁(x)] 
 where Ai are the Chebychev coefficients listed below and x= Fcalc/Fmax 
 Method = Robust Weighting (Prince, 1982) 
 W = [weight] * [1-(deltaF/6*sigmaF)²]² 
 Ai are: 
 14.6 10.0 9.86 
;

# Uequiv = arithmetic mean of Ui i.e. Ueqiv = (U1+U2+U3)/3

# Replace last . with number of unfound hydrogen atoms attached to an atom.

# ..._refinement_flags_... 
# . no refinement constraints           S special position constraint on site
# G rigid group refinement of site      R riding atom
# D distance or angle restraint on site T thermal displacement constraints
# U Uiso or Uij restraint (rigid bond)  P partial occupancy constraint


loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_occupancy
_atom_site_adp_type
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
_atom_site_attached_hydrogens
Eu1 Eu 0.35706(5) 0.89781(10) 0.60480(5) 0.0936 1.0000 Uani D U . . . .
N101 N 0.40560(14) 0.9516(5) 0.6461(3) 0.1056 1.0000 Uani D U . . . .
N102 N 0.35591(19) 1.0423(4) 0.6269(3) 0.1076 1.0000 Uani D U . . . .
N103 N 0.3405(2) 0.9884(5) 0.5364(2) 0.1232 1.0000 Uani D U . . . .
N104 N 0.39052(18) 0.8984(5) 0.5552(3) 0.1144 1.0000 Uani D U . . . .
O101 O 0.3891(2) 0.8059(6) 0.6358(3) 0.1016 1.0000 Uani D U . . . .
O102 O 0.35800(16) 0.9201(6) 0.6767(2) 0.0968 1.0000 Uani D U . . . .
O103 O 0.31263(15) 0.9390(5) 0.5920(4) 0.1190 1.0000 Uani D U . . . .
O109 O 0.3321(4) 0.8053(9) 0.6306(6) 0.1158 1.0000 Uani D U . . . .
C101 C 0.4025(2) 1.0206(7) 0.6708(4) 0.1093 1.0000 Uani D U . . . .
C102 C 0.3837(2) 1.0742(6) 0.6440(5) 0.1156 1.0000 Uani D U . . . .
C103 C 0.3405(3) 1.0882(6) 0.5887(3) 0.1229 1.0000 Uani D U . . . .
C104 C 0.3476(3) 1.0679(6) 0.5494(3) 0.1292 1.0000 Uani D U . . . .
C105 C 0.3537(3) 0.9644(9) 0.5032(3) 0.1336 1.0000 Uani D U . . . .
C106 C 0.3830(3) 0.9592(8) 0.5216(5) 0.1265 1.0000 Uani D U . . . .
C107 C 0.4189(2) 0.9111(8) 0.5827(4) 0.1234 1.0000 Uani D U . . . .
C108 C 0.4202(3) 0.9721(7) 0.6136(3) 0.1198 1.0000 Uani D U . . . .
C111 C 0.4200(3) 0.8924(5) 0.6751(3) 0.1104 1.0000 Uani D U . . . .
C112 C 0.4138(2) 0.8142(5) 0.6599(3) 0.1148 1.0000 Uani D U . . . .
O113 O 0.4301(2) 0.7658(6) 0.6693(3) 0.1484 1.0000 Uani D U . . . .
C114 C 0.34196(16) 1.0415(6) 0.6605(3) 0.1105 1.0000 Uani D U . . . .
C115 C 0.34686(16) 0.9769(5) 0.6907(2) 0.0969 1.0000 Uani D U . . . .
O116 O 0.34121(16) 0.9787(6) 0.7236(3) 0.0844 1.0000 Uani D U . . . .
C117 C 0.3114(3) 0.9767(6) 0.5224(4) 0.1403 1.0000 Uani D U . . . .
C118 C 0.29814(17) 0.9737(5) 0.5575(4) 0.1425 1.0000 Uani D U . . . .
O119 O 0.27666(19) 1.0006(5) 0.5535(5) 0.1943 1.0000 Uani D U . . . .
O120 O 0.4160(3) 0.8306(6) 0.4022(4) 0.1274 1.0000 Uani D U . . . .
C121 C 0.3893(3) 0.8241(6) 0.5326(6) 0.1212 1.0000 Uani D U . . . .
C122 C 0.4078(3) 0.8060(6) 0.5046(5) 0.1226 1.0000 Uani D U . . . .
C123 C 0.4011(3) 0.8314(6) 0.4630(5) 0.1221 1.0000 Uani D U . . . .
C124 C 0.4202(3) 0.8100(6) 0.4401(4) 0.1250 1.0000 Uani D U . . . .
O125 O 0.4420(3) 0.7701(6) 0.4566(4) 0.1266 1.0000 Uani D U . . . .
C126 C 0.4463(3) 0.7475(6) 0.4977(4) 0.1237 1.0000 Uani D U . . . .
C127 C 0.4309(3) 0.7625(6) 0.5242(4) 0.1214 1.0000 Uani D U . . . .
C128 C 0.4382(3) 0.7355(6) 0.5652(4) 0.1231 1.0000 Uani D U . . . .
C129 C 0.4608(3) 0.6942(6) 0.5796(4) 0.1279 1.0000 Uani D U . . . .
C130 C 0.4763(3) 0.6795(6) 0.5532(4) 0.1324 1.0000 Uani D U . . . .
C131 C 0.4690(3) 0.7064(6) 0.5122(4) 0.1258 1.0000 Uani D U . . . .
O132 O 0.4996(3) 0.6369(6) 0.5679(5) 0.1423 1.0000 Uani D U . . . .
C133 C 0.5091(4) 0.6064(7) 0.6094(6) 0.1591 1.0000 Uani D U . . . .
Eu2 Eu 0.34625(4) 0.90694(9) 0.78966(5) 0.0753 1.0000 Uani D U . . . .
N201 N 0.31675(17) 0.8475(5) 0.8371(3) 0.0960 1.0000 Uani D U . . . .
N202 N 0.29612(13) 0.9566(5) 0.7662(3) 0.1006 1.0000 Uani D U . . . .
N203 N 0.34378(19) 1.0531(3) 0.8028(3) 0.1010 1.0000 Uani D U . . . .
N204 N 0.36439(18) 0.9422(5) 0.8734(2) 0.1034 1.0000 Uani D U . . . .
O201 O 0.3559(2) 0.7852(4) 0.8160(2) 0.0844 1.0000 Uani D U . . . .
O202 O 0.31486(17) 0.8401(6) 0.7359(3) 0.0864 1.0000 Uani D U . . . .
O203 O 0.38690(19) 0.9729(6) 0.8045(2) 0.0938 1.0000 Uani D U . . . .
O209 O 0.3706(3) 0.8419(7) 0.7485(4) 0.0776 1.0000 Uani D U . . . .
C201 C 0.2911(3) 0.8903(8) 0.8301(4) 0.1125 1.0000 Uani D U . . . .
C202 C 0.2789(2) 0.9072(8) 0.7842(4) 0.1138 1.0000 Uani D U . . . .
C203 C 0.2949(2) 1.0357(6) 0.7803(5) 0.1162 1.0000 Uani D U . . . .
C204 C 0.3174(2) 1.0803(6) 0.7743(5) 0.1121 1.0000 Uani D U . . . .
C205 C 0.3451(3) 1.0644(7) 0.8493(3) 0.1137 1.0000 Uani D U . . . .
C206 C 0.3687(3) 1.0250(5) 0.8776(4) 0.1143 1.0000 Uani D U . . . .
C207 C 0.3457(3) 0.9185(8) 0.8985(4) 0.1215 1.0000 Uani D U . . . .
C208 C 0.3323(3) 0.8479(7) 0.8839(3) 0.1107 1.0000 Uani D U . . . .
C211 C 0.3122(2) 0.7712(6) 0.8201(2) 0.0981 1.0000 Uani D U . . . .
C212 C 0.3367(2) 0.7367(4) 0.8133(2) 0.0953 1.0000 Uani D U . . . .
O213 O 0.3378(3) 0.6719(4) 0.8060(2) 0.1064 1.0000 Uani D U . . . .
C214 C 0.2900(2) 0.9500(6) 0.7191(3) 0.1101 1.0000 Uani D U . . . .
C215 C 0.29948(18) 0.8794(6) 0.7042(2) 0.1039 1.0000 Uani D U . . . .
O216 O 0.29329(19) 0.8621(7) 0.6671(3) 0.1344 1.0000 Uani D U . . . .
C217 C 0.3664(2) 1.0898(7) 0.7923(3) 0.1088 1.0000 Uani D U . . . .
C218 C 0.38983(17) 1.0418(6) 0.7930(2) 0.1090 1.0000 Uani D U . . . .
O219 O 0.4087(2) 1.0651(7) 0.7836(3) 0.1323 1.0000 Uani D U . . . .
O220 O 0.4199(3) 0.8853(7) 1.0405(4) 0.1593 1.0000 Uani D U . . . .
C221 C 0.3904(3) 0.9009(8) 0.8882(5) 0.1215 1.0000 Uani D U . . . .
C222 C 0.4101(3) 0.9202(6) 0.9318(5) 0.1195 1.0000 Uani D U . . . .
C223 C 0.4038(3) 0.8891(7) 0.9660(4) 0.1182 1.0000 Uani D U . . . .
C224 C 0.4230(3) 0.9096(7) 1.0063(4) 0.1285 1.0000 Uani D U . . . .
O225 O 0.4440(3) 0.9526(7) 1.0099(4) 0.1438 1.0000 Uani D U . . . .
C226 C 0.4477(3) 0.9792(6) 0.9734(5) 0.1376 1.0000 Uani D U . . . .
C227 C 0.4322(3) 0.9669(6) 0.9327(5) 0.1311 1.0000 Uani D U . . . .
C228 C 0.4387(3) 0.9981(6) 0.8987(5) 0.1293 1.0000 Uani D U . . . .
C229 C 0.4608(3) 1.0418(6) 0.9057(5) 0.1414 1.0000 Uani D U . . . .
C230 C 0.4764(2) 1.0541(6) 0.9466(5) 0.1485 1.0000 Uani D U . . . .
C231 C 0.4699(3) 1.0228(7) 0.9804(4) 0.1457 1.0000 Uani D U . . . .
O232 O 0.4993(2) 1.0992(6) 0.9539(6) 0.1702 1.0000 Uani D U . . . .
C233 C 0.5076(4) 1.1337(7) 0.9209(9) 0.1802 1.0000 Uani D U . . . .
Eu3 Eu 0.35766(5) 0.60109(9) 0.76737(6) 0.1006 1.0000 Uani D U . . . .
N301 N 0.40691(15) 0.5533(6) 0.7707(3) 0.1247 1.0000 Uani D U . . . .
N302 N 0.3586(2) 0.4566(4) 0.7456(3) 0.1327 1.0000 Uani D U . . . .
N303 N 0.3427(2) 0.5097(5) 0.8217(3) 0.1349 1.0000 Uani D U . . . .
N304 N 0.39162(18) 0.6052(5) 0.8476(2) 0.1198 1.0000 Uani D U . . . .
O301 O 0.3886(2) 0.6967(6) 0.7678(3) 0.1046 1.0000 Uani D U . . . .
O302 O 0.36095(17) 0.5767(6) 0.6980(2) 0.1149 1.0000 Uani D U . . . .
O303 O 0.31359(18) 0.5547(5) 0.7433(4) 0.1218 1.0000 Uani D U . . . .
O309 O 0.3356(4) 0.6973(8) 0.7184(5) 0.1100 1.0000 Uani D U . . . .
C301 C 0.4049(3) 0.4822(7) 0.7450(5) 0.1433 1.0000 Uani D U . . . .
C302 C 0.3870(2) 0.4281(6) 0.7568(5) 0.1511 1.0000 Uani D U . . . .
C303 C 0.3430(4) 0.4105(6) 0.7691(4) 0.1451 1.0000 Uani D U . . . .
C304 C 0.3499(4) 0.4300(6) 0.8149(4) 0.1482 1.0000 Uani D U . . . .
C305 C 0.3571(3) 0.5321(9) 0.8673(3) 0.1417 1.0000 Uani D U . . . .
C306 C 0.3861(3) 0.5388(7) 0.8729(4) 0.1365 1.0000 Uani D U . . . .
C307 C 0.4202(2) 0.5991(9) 0.8454(4) 0.1361 1.0000 Uani D U . . . .
C308 C 0.4232(3) 0.5388(8) 0.8166(3) 0.1371 1.0000 Uani D U . . . .
C311 C 0.4187(3) 0.6139(6) 0.7514(3) 0.1242 1.0000 Uani D U . . . .
C312 C 0.4133(2) 0.6892(5) 0.7663(3) 0.1154 1.0000 Uani D U . . . .
O313 O 0.4300(2) 0.7362(7) 0.7754(3) 0.1404 1.0000 Uani D U . . . .
C314 C 0.34586(17) 0.4544(7) 0.6989(3) 0.1333 1.0000 Uani D U . . . .
C315 C 0.35112(16) 0.5189(6) 0.6737(2) 0.1245 1.0000 Uani D U . . . .
O316 O 0.34657(16) 0.5165(7) 0.6357(3) 0.1295 1.0000 Uani D U . . . .
C317 C 0.3135(3) 0.5190(5) 0.8126(4) 0.1470 1.0000 Uani D U . . . .
C318 C 0.29846(17) 0.5474(5) 0.7692(4) 0.1414 1.0000 Uani D U . . . .
O319 O 0.2752(2) 0.5614(5) 0.7600(5) 0.1736 1.0000 Uani D U . . . .
O320 O 0.4247(4) 0.6916(8) 1.0235(5) 0.1793 1.0000 Uani D U . . . .
C321 C 0.3902(3) 0.6749(7) 0.8742(6) 0.1350 1.0000 Uani D U . . . .
C322 C 0.4130(3) 0.7070(7) 0.9115(6) 0.1507 1.0000 Uani D U . . . .
C323 C 0.4080(3) 0.6843(7) 0.9491(5) 0.1545 1.0000 Uani D U . . . .
C324 C 0.4276(3) 0.7096(7) 0.9882(5) 0.1713 1.0000 Uani D U . . . .
O325 O 0.4487(3) 0.7515(7) 0.9895(5) 0.1750 1.0000 Uani D U . . . .
C326 C 0.4517(4) 0.7711(7) 0.9510(5) 0.1658 1.0000 Uani D U . . . .
C327 C 0.4355(3) 0.7526(7) 0.9113(6) 0.1551 1.0000 Uani D U . . . .
C328 C 0.4415(3) 0.7775(7) 0.8755(5) 0.1561 1.0000 Uani D U . . . .
C329 C 0.4635(3) 0.8206(7) 0.8794(5) 0.1586 1.0000 Uani D U . . . .
C330 C 0.4796(3) 0.8389(7) 0.9191(5) 0.1688 1.0000 Uani D U . . . .
C331 C 0.4737(3) 0.8140(7) 0.9549(5) 0.1661 1.0000 Uani D U . . . .
O332 O 0.5023(3) 0.8834(7) 0.9232(7) 0.1788 1.0000 Uani D U . . . .
C333 C 0.5102(4) 0.9114(8) 0.8881(10) 0.2043 1.0000 Uani D U . . . .
Eu4 Eu 0.34984(5) 0.58685(11) 0.57561(6) 0.1083 1.0000 Uani D U . . . .
N401 N 0.31957(18) 0.6535(5) 0.5032(3) 0.1321 1.0000 Uani D U . . . .
N402 N 0.29928(14) 0.5386(5) 0.5525(4) 0.1394 1.0000 Uani D U . . . .
N403 N 0.3464(2) 0.4427(3) 0.5546(4) 0.1383 1.0000 Uani D U . . . .
N404 N 0.3669(2) 0.5594(5) 0.5069(3) 0.1351 1.0000 Uani D U . . . .
O401 O 0.3554(3) 0.7099(4) 0.5547(3) 0.1171 1.0000 Uani D U . . . .
O402 O 0.31552(17) 0.6522(6) 0.5943(3) 0.1264 1.0000 Uani D U . . . .
O403 O 0.39095(19) 0.5243(6) 0.6029(3) 0.1284 1.0000 Uani D U . . . .
O409 O 0.3752(4) 0.6502(11) 0.6395(4) 0.1250 1.0000 Uani D U . . . .
C401 C 0.2947(3) 0.6067(8) 0.4850(4) 0.1463 1.0000 Uani D U . . . .
C402 C 0.2817(2) 0.5898(8) 0.5188(4) 0.1516 1.0000 Uani D U . . . .
C403 C 0.2974(2) 0.4611(7) 0.5345(5) 0.1582 1.0000 Uani D U . . . .
C404 C 0.3199(2) 0.4137(6) 0.5569(6) 0.1505 1.0000 Uani D U . . . .
C405 C 0.3495(3) 0.4330(7) 0.5105(4) 0.1492 1.0000 Uani D U . . . .
C406 C 0.3719(3) 0.4775(5) 0.5042(5) 0.1506 1.0000 Uani D U . . . .
C407 C 0.3483(3) 0.5872(9) 0.4659(3) 0.1467 1.0000 Uani D U . . . .
C408 C 0.3350(3) 0.6569(7) 0.4702(4) 0.1453 1.0000 Uani D U . . . .
C411 C 0.3116(3) 0.7301(6) 0.5122(3) 0.1394 1.0000 Uani D U . . . .
C412 C 0.3370(3) 0.7612(4) 0.5405(3) 0.1249 1.0000 Uani D U . . . .
O413 O 0.3397(3) 0.8258(5) 0.5486(3) 0.1161 1.0000 Uani D U . . . .
C414 C 0.2915(2) 0.5417(6) 0.5926(3) 0.1480 1.0000 Uani D U . . . .
C415 C 0.29940(18) 0.6167(6) 0.6121(2) 0.1430 1.0000 Uani D U . . . .
O416 O 0.2916(2) 0.6400(8) 0.6408(3) 0.1727 1.0000 Uani D U . . . .
C417 C 0.3687(2) 0.4100(8) 0.5881(3) 0.1402 1.0000 Uani D U . . . .
C418 C 0.39242(18) 0.4532(6) 0.6132(3) 0.1352 1.0000 Uani D U . . . .
O419 O 0.4105(2) 0.4245(7) 0.6395(3) 0.1563 1.0000 Uani D U . . . .
O420 O 0.4163(3) 0.6269(7) 0.3846(4) 0.1399 1.0000 Uani D U . . . .
C421 C 0.3927(3) 0.6022(9) 0.5187(6) 0.1433 1.0000 Uani D U . . . .
C422 C 0.4088(3) 0.5885(7) 0.4867(5) 0.1443 1.0000 Uani D U . . . .
C423 C 0.4027(3) 0.6202(7) 0.4466(5) 0.1435 1.0000 Uani D U . . . .
C424 C 0.4204(3) 0.6003(7) 0.4210(4) 0.1359 1.0000 Uani D U . . . .
O425 O 0.4408(3) 0.5551(7) 0.4350(4) 0.1426 1.0000 Uani D U . . . .
C426 C 0.4457(3) 0.5255(7) 0.4747(4) 0.1442 1.0000 Uani D U . . . .
C427 C 0.4309(3) 0.5395(7) 0.5022(5) 0.1450 1.0000 Uani D U . . . .
C428 C 0.4375(3) 0.5073(7) 0.5418(4) 0.1466 1.0000 Uani D U . . . .
C429 C 0.4590(3) 0.4612(7) 0.5540(4) 0.1537 1.0000 Uani D U . . . .
C430 C 0.4739(3) 0.4471(7) 0.5266(5) 0.1570 1.0000 Uani D U . . . .
C431 C 0.4672(3) 0.4792(7) 0.4870(4) 0.1522 1.0000 Uani D U . . . .
O432 O 0.4961(3) 0.3995(7) 0.5392(6) 0.1694 1.0000 Uani D U . . . .
C433 C 0.5046(4) 0.3633(7) 0.5793(7) 0.1888 1.0000 Uani D U . . . .
Eu5 Eu 0.13964(6) 0.89683(16) 0.23184(10) 0.1490 1.0000 Uani D U . . . .
N501 N 0.09159(16) 0.9515(8) 0.2304(4) 0.1646 1.0000 Uani D U . . . .
N502 N 0.1420(3) 1.0403(5) 0.2558(5) 0.1720 1.0000 Uani D U . . . .
N503 N 0.1559(3) 0.9853(6) 0.1781(3) 0.1688 1.0000 Uani D U . . . .
N504 N 0.1052(2) 0.8980(7) 0.1523(3) 0.1560 1.0000 Uani D U . . . .
O501 O 0.1077(3) 0.8046(8) 0.2326(3) 0.1539 1.0000 Uani D U . . . .
O502 O 0.14665(16) 0.9125(10) 0.3064(3) 0.1596 1.0000 Uani D U . . . .
O503 O 0.18492(16) 0.9300(5) 0.2593(6) 0.1670 1.0000 Uani D U . . . .
O509 O 0.1703(4) 0.8090(11) 0.2755(7) 0.1518 1.0000 Uani D U . . . .
C501 C 0.0958(3) 1.0202(10) 0.2581(6) 0.1787 1.0000 Uani D U . . . .
C502 C 0.1143(3) 1.0727(7) 0.2462(6) 0.1841 1.0000 Uani D U . . . .
C503 C 0.1583(4) 1.0831(8) 0.2325(6) 0.1794 1.0000 Uani D U . . . .
C504 C 0.1513(4) 1.0655(7) 0.1865(5) 0.1795 1.0000 Uani D U . . . .
C505 C 0.1415(4) 0.9642(12) 0.1327(4) 0.1722 1.0000 Uani D U . . . .
C506 C 0.1126(3) 0.9570(10) 0.1249(5) 0.1708 1.0000 Uani D U . . . .
C507 C 0.0771(2) 0.9113(10) 0.1545(5) 0.1655 1.0000 Uani D U . . . .
C508 C 0.0762(3) 0.9716(8) 0.1849(4) 0.1697 1.0000 Uani D U . . . .
C511 C 0.0782(4) 0.8917(8) 0.2474(3) 0.1679 1.0000 Uani D U . . . .
C512 C 0.0842(3) 0.8126(7) 0.2393(3) 0.1601 1.0000 Uani D U . . . .
O513 O 0.0689(3) 0.7632(9) 0.2391(3) 0.1588 1.0000 Uani D U . . . .
C514 C 0.15521(17) 1.0398(10) 0.3028(5) 0.1753 1.0000 Uani D U . . . .
C515 C 0.15284(17) 0.9736(9) 0.3293(3) 0.1765 1.0000 Uani D U . . . .
O516 O 0.15622(16) 0.9779(10) 0.3672(3) 0.1920 1.0000 Uani D U . . . .
C517 C 0.1844(4) 0.9662(7) 0.1899(6) 0.1756 1.0000 Uani D U . . . .
C518 C 0.1996(2) 0.9577(5) 0.2362(6) 0.1798 1.0000 Uani D U . . . .
O519 O 0.2225(2) 0.9746(5) 0.2496(7) 0.2187 1.0000 Uani D U . . . .
O520 O 0.0778(4) 0.8328(7) -0.0239(5) 0.1541 1.0000 Uani D U . . . .
C521 C 0.1066(4) 0.8221(8) 0.1327(6) 0.1459 1.0000 Uani D U . . . .
C522 C 0.0883(3) 0.8050(7) 0.0873(6) 0.1347 1.0000 Uani D U . . . .
C523 C 0.0935(3) 0.8318(7) 0.0508(5) 0.1378 1.0000 Uani D U . . . .
C524 C 0.0744(3) 0.8109(6) 0.0102(5) 0.1350 1.0000 Uani D U . . . .
O525 O 0.0533(3) 0.7689(6) 0.0077(5) 0.1327 1.0000 Uani D U . . . .
C526 C 0.0494(3) 0.7439(6) 0.0447(5) 0.1273 1.0000 Uani D U . . . .
C527 C 0.0656(3) 0.7591(6) 0.0848(6) 0.1306 1.0000 Uani D U . . . .
C528 C 0.0598(3) 0.7312(7) 0.1200(5) 0.1356 1.0000 Uani D U . . . .
C529 C 0.0377(3) 0.6878(6) 0.1152(5) 0.1408 1.0000 Uani D U . . . .
C530 C 0.0216(3) 0.6723(6) 0.0751(5) 0.1407 1.0000 Uani D U . . . .
C531 C 0.0274(3) 0.7003(7) 0.0398(5) 0.1348 1.0000 Uani D U . . . .
O532 O -0.0012(3) 0.6275(6) 0.0701(7) 0.1580 1.0000 Uani D U . . . .
C533 C -0.0089(4) 0.5961(7) 0.1044(9) 0.1787 1.0000 Uani D U . . . .
Eu6 Eu 0.15542(8) 0.9133(2) 0.42800(10) 0.1884 1.0000 Uani D U . . . .
N601 N 0.1858(2) 0.8625(8) 0.5038(3) 0.2000 1.0000 Uani D U . . . .
N602 N 0.20381(18) 0.9757(7) 0.4512(4) 0.2085 1.0000 Uani D U . . . .
N603 N 0.1531(3) 1.0612(4) 0.4379(5) 0.2051 1.0000 Uani D U . . . .
N604 N 0.1356(2) 0.9496(7) 0.4929(3) 0.2042 1.0000 Uani D U . . . .
O601 O 0.1493(4) 0.7849(5) 0.4362(5) 0.1843 1.0000 Uani D U . . . .
O602 O 0.1784(3) 0.8588(9) 0.3830(3) 0.1923 1.0000 Uani D U . . . .
O603 O 0.1134(2) 0.9720(9) 0.4056(3) 0.1888 1.0000 Uani D U . . . .
O609 O 0.1265(6) 0.8419(15) 0.3704(7) 0.1788 1.0000 Uani D U . . . .
C601 C 0.2111(3) 0.9058(11) 0.5195(4) 0.2103 1.0000 Uani D U . . . .
C602 C 0.2223(2) 0.9315(12) 0.4857(5) 0.2127 1.0000 Uani D U . . . .
C603 C 0.2026(3) 1.0555(9) 0.4620(6) 0.2149 1.0000 Uani D U . . . .
C604 C 0.1791(3) 1.0944(7) 0.4351(8) 0.2138 1.0000 Uani D U . . . .
C605 C 0.1494(4) 1.0773(7) 0.4815(4) 0.2105 1.0000 Uani D U . . . .
C606 C 0.1279(4) 1.0307(8) 0.4892(6) 0.2105 1.0000 Uani D U . . . .
C607 C 0.1563(3) 0.9362(9) 0.5354(4) 0.2107 1.0000 Uani D U . . . .
C608 C 0.1702(4) 0.8648(9) 0.5362(4) 0.2018 1.0000 Uani D U . . . .
C611 C 0.1899(4) 0.7864(11) 0.4907(6) 0.1981 1.0000 Uani D U . . . .
C612 C 0.1664(3) 0.7433(6) 0.4645(5) 0.1887 1.0000 Uani D U . . . .
O613 O 0.1641(4) 0.6781(7) 0.4696(5) 0.1854 1.0000 Uani D U . . . .
C614 C 0.2062(4) 0.9614(8) 0.4081(4) 0.2040 1.0000 Uani D U . . . .
C615 C 0.2001(3) 0.8932(8) 0.3806(3) 0.2001 1.0000 Uani D U . . . .
O616 O 0.2140(3) 0.8738(10) 0.3591(4) 0.2015 1.0000 Uani D U . . . .
C617 C 0.1303(3) 1.0921(11) 0.4034(3) 0.2104 1.0000 Uani D U . . . .
C618 C 0.1067(2) 1.0421(8) 0.3970(3) 0.2065 1.0000 Uani D U . . . .
O619 O 0.0844(3) 1.0653(9) 0.3856(3) 0.2447 1.0000 Uani D U . . . .
O620 O 0.0698(5) 0.8803(11) 0.6016(7) 0.2175 1.0000 Uani D U . . . .
C621 C 0.1112(3) 0.9025(10) 0.4907(8) 0.2041 1.0000 Uani D U . . . .
C622 C 0.0879(3) 0.9266(11) 0.5082(8) 0.2085 1.0000 Uani D U . . . .
C623 C 0.0900(4) 0.8916(11) 0.5466(8) 0.2067 1.0000 Uani D U . . . .
C624 C 0.0694(4) 0.9097(10) 0.5669(7) 0.2110 1.0000 Uani D U . . . .
O625 O 0.0498(4) 0.9567(10) 0.5502(7) 0.2243 1.0000 Uani D U . . . .
C626 C 0.0488(5) 0.9896(10) 0.5124(6) 0.2262 1.0000 Uani D U . . . .
C627 C 0.0667(4) 0.9777(10) 0.4897(7) 0.2246 1.0000 Uani D U . . . .
C628 C 0.0638(4) 1.0138(10) 0.4518(7) 0.2325 1.0000 Uani D U . . . .
C629 C 0.0430(4) 1.0616(10) 0.4365(6) 0.2419 1.0000 Uani D U . . . .
C630 C 0.0251(4) 1.0734(10) 0.4592(7) 0.2404 1.0000 Uani D U . . . .
C631 C 0.0280(4) 1.0374(11) 0.4971(7) 0.2371 1.0000 Uani D U . . . .
O632 O 0.0037(4) 1.1228(10) 0.4432(8) 0.2521 1.0000 Uani D U . . . .
C633 C -0.0006(5) 1.1623(10) 0.4042(9) 0.2448 1.0000 Uani D U . . . .
Eu7 Eu 0.13889(7) 0.60700(19) 0.39676(10) 0.1601 1.0000 Uani D U . . . .
N701 N 0.09032(16) 0.5595(8) 0.3515(4) 0.1632 1.0000 Uani D U . . . .
N702 N 0.1395(3) 0.4658(5) 0.3694(4) 0.1701 1.0000 Uani D U . . . .
N703 N 0.1543(3) 0.5096(6) 0.4622(3) 0.1880 1.0000 Uani D U . . . .
N704 N 0.1046(2) 0.6011(7) 0.4444(3) 0.1687 1.0000 Uani D U . . . .
O701 O 0.1068(3) 0.7013(8) 0.3710(4) 0.1589 1.0000 Uani D U . . . .
O702 O 0.14412(17) 0.5919(10) 0.3274(3) 0.1562 1.0000 Uani D U . . . .
O703 O 0.18366(18) 0.5658(6) 0.4179(6) 0.1802 1.0000 Uani D U . . . .
O709 O 0.1640(6) 0.7015(13) 0.3726(9) 0.1661 1.0000 Uani D U . . . .
C701 C 0.0937(3) 0.4936(10) 0.3246(5) 0.1698 1.0000 Uani D U . . . .
C702 C 0.1114(3) 0.4370(7) 0.3505(6) 0.1735 1.0000 Uani D U . . . .
C703 C 0.1537(4) 0.4157(8) 0.4066(4) 0.1835 1.0000 Uani D U . . . .
C704 C 0.1454(4) 0.4321(8) 0.4453(5) 0.1863 1.0000 Uani D U . . . .
C705 C 0.1401(4) 0.5295(12) 0.4954(4) 0.1885 1.0000 Uani D U . . . .
C706 C 0.1112(3) 0.5377(10) 0.4761(6) 0.1825 1.0000 Uani D U . . . .
C707 C 0.0764(2) 0.5917(11) 0.4157(5) 0.1712 1.0000 Uani D U . . . .
C708 C 0.0749(3) 0.5355(8) 0.3821(4) 0.1733 1.0000 Uani D U . . . .
C711 C 0.0768(4) 0.6217(8) 0.3240(5) 0.1671 1.0000 Uani D U . . . .
C712 C 0.0832(3) 0.6977(7) 0.3424(4) 0.1586 1.0000 Uani D U . . . .
O713 O 0.0682(3) 0.7486(9) 0.3315(4) 0.1693 1.0000 Uani D U . . . .
C714 C 0.15409(17) 0.4648(10) 0.3362(5) 0.1677 1.0000 Uani D U . . . .
C715 C 0.15024(17) 0.5325(9) 0.3085(3) 0.1585 1.0000 Uani D U . . . .
O716 O 0.15246(16) 0.5309(10) 0.2729(3) 0.1459 1.0000 Uani D U . . . .
C717 C 0.1837(3) 0.5100(7) 0.4829(6) 0.1981 1.0000 Uani D U . . . .
C718 C 0.19850(19) 0.5297(6) 0.4514(5) 0.1938 1.0000 Uani D U . . . .
O719 O 0.2214(2) 0.5133(6) 0.4571(6) 0.2038 1.0000 Uani D U . . . .
O720 O 0.0672(4) 0.6826(9) 0.5838(6) 0.1892 1.0000 Uani D U . . . .
C721 C 0.1066(3) 0.6739(8) 0.4686(8) 0.1655 1.0000 Uani D U . . . .
C722 C 0.0839(3) 0.7024(8) 0.4862(7) 0.1639 1.0000 Uani D U . . . .
C723 C 0.0864(4) 0.6782(8) 0.5273(7) 0.1662 1.0000 Uani D U . . . .
C724 C 0.0661(3) 0.7021(8) 0.5469(6) 0.1740 1.0000 Uani D U . . . .
O725 O 0.0460(4) 0.7446(8) 0.5262(6) 0.1784 1.0000 Uani D U . . . .
C726 C 0.0440(4) 0.7677(8) 0.4859(5) 0.1784 1.0000 Uani D U . . . .
C727 C 0.0619(4) 0.7489(7) 0.4643(6) 0.1735 1.0000 Uani D U . . . .
C728 C 0.0586(4) 0.7746(8) 0.4237(6) 0.1822 1.0000 Uani D U . . . .
C729 C 0.0373(4) 0.8187(8) 0.4046(5) 0.1950 1.0000 Uani D U . . . .
C730 C 0.0194(3) 0.8375(7) 0.4261(6) 0.1996 1.0000 Uani D U . . . .
C731 C 0.0228(4) 0.8120(8) 0.4668(6) 0.1897 1.0000 Uani D U . . . .
O732 O -0.0025(4) 0.8832(7) 0.4062(8) 0.2157 1.0000 Uani D U . . . .
C733 C -0.0076(5) 0.9118(8) 0.3642(8) 0.2163 1.0000 Uani D U . . . .
Eu8 Eu 0.15637(5) 0.58752(16) 0.21553(8) 0.1318 1.0000 Uani D U . . . .
N801 N 0.18667(19) 0.6527(7) 0.1713(3) 0.1486 1.0000 Uani D U . . . .
N802 N 0.20713(15) 0.5387(6) 0.2394(4) 0.1611 1.0000 Uani D U . . . .
N803 N 0.1604(3) 0.4447(4) 0.1953(4) 0.1556 1.0000 Uani D U . . . .
N804 N 0.1379(2) 0.5638(5) 0.1307(2) 0.1435 1.0000 Uani D U . . . .
O801 O 0.1495(3) 0.7146(4) 0.1978(2) 0.1381 1.0000 Uani D U . . . .
O802 O 0.1849(2) 0.6450(8) 0.2768(2) 0.1467 1.0000 Uani D U . . . .
O803 O 0.1155(2) 0.5270(9) 0.2108(2) 0.1440 1.0000 Uani D U . . . .
O809 O 0.1243(4) 0.6566(14) 0.2405(8) 0.1433 1.0000 Uani D U . . . .
C801 C 0.2117(3) 0.6074(10) 0.1763(4) 0.1644 1.0000 Uani D U . . . .
C802 C 0.2247(2) 0.5908(10) 0.2223(5) 0.1680 1.0000 Uani D U . . . .
C803 C 0.2096(3) 0.4618(8) 0.2232(7) 0.1737 1.0000 Uani D U . . . .
C804 C 0.1868(3) 0.4137(7) 0.2195(6) 0.1694 1.0000 Uani D U . . . .
C805 C 0.1550(3) 0.4362(7) 0.1477(4) 0.1594 1.0000 Uani D U . . . .
C806 C 0.1322(3) 0.4821(6) 0.1235(4) 0.1493 1.0000 Uani D U . . . .
C807 C 0.1576(3) 0.5886(9) 0.1076(4) 0.1494 1.0000 Uani D U . . . .
C808 C 0.1712(3) 0.6583(8) 0.1248(3) 0.1519 1.0000 Uani D U . . . .
C811 C 0.1929(3) 0.7259(10) 0.1921(3) 0.1531 1.0000 Uani D U . . . .
C812 C 0.1668(3) 0.7616(5) 0.1900(3) 0.1513 1.0000 Uani D U . . . .
O813 O 0.1627(4) 0.8259(6) 0.1816(3) 0.1594 1.0000 Uani D U . . . .
C814 C 0.2140(3) 0.5431(8) 0.2865(5) 0.1661 1.0000 Uani D U . . . .
C815 C 0.2074(2) 0.6176(8) 0.3015(3) 0.1646 1.0000 Uani D U . . . .
O816 O 0.2216(3) 0.6474(10) 0.3326(3) 0.1957 1.0000 Uani D U . . . .
C817 C 0.1385(3) 0.4153(12) 0.2109(2) 0.1613 1.0000 Uani D U . . . .
C818 C 0.1131(2) 0.4542(9) 0.2096(3) 0.1589 1.0000 Uani D U . . . .
O819 O 0.0929(3) 0.4209(9) 0.2074(3) 0.1825 1.0000 Uani D U . . . .
O820 O 0.0805(3) 0.6299(8) -0.0398(5) 0.1434 1.0000 Uani D U . . . .
C821 C 0.1126(3) 0.6086(9) 0.1157(6) 0.1390 1.0000 Uani D U . . . .
C822 C 0.0938(3) 0.5914(7) 0.0706(5) 0.1261 1.0000 Uani D U . . . .
C823 C 0.0976(3) 0.6242(7) 0.0347(5) 0.1334 1.0000 Uani D U . . . .
C824 C 0.0786(3) 0.6028(7) -0.0058(5) 0.1361 1.0000 Uani D U . . . .
O825 O 0.0589(3) 0.5555(7) -0.0085(5) 0.1433 1.0000 Uani D U . . . .
C826 C 0.0564(3) 0.5251(7) 0.0281(5) 0.1392 1.0000 Uani D U . . . .
C827 C 0.0726(3) 0.5399(6) 0.0683(6) 0.1342 1.0000 Uani D U . . . .
C828 C 0.0680(3) 0.5062(7) 0.1031(5) 0.1383 1.0000 Uani D U . . . .
C829 C 0.0473(3) 0.4576(7) 0.0977(5) 0.1465 1.0000 Uani D U . . . .
C830 C 0.0311(2) 0.4429(6) 0.0575(5) 0.1521 1.0000 Uani D U . . . .
C831 C 0.0356(3) 0.4768(7) 0.0227(5) 0.1493 1.0000 Uani D U . . . .
O832 O 0.0097(2) 0.3926(6) 0.0518(7) 0.1650 1.0000 Uani D U . . . .
C833 C 0.0033(4) 0.3551(7) 0.0857(9) 0.1752 1.0000 Uani D U . . . .
H1011 H 0.4193 1.0429 0.6828 0.1338 1.0000 Uiso R . . . . .
H1012 H 0.3950 1.0074 0.6930 0.1338 1.0000 Uiso R . . . . .
H1021 H 0.3833 1.1192 0.6587 0.1403 1.0000 Uiso R . . . . .
H1022 H 0.3902 1.0833 0.6202 0.1403 1.0000 Uiso R . . . . .
H1031 H 0.3439 1.1392 0.5949 0.1491 1.0000 Uiso R . . . . .
H1032 H 0.3221 1.0791 0.5823 0.1491 1.0000 Uiso R . . . . .
H1041 H 0.3664 1.0703 0.5572 0.1557 1.0000 Uiso R . . . . .
H1042 H 0.3404 1.1009 0.5264 0.1557 1.0000 Uiso R . . . . .
H1051 H 0.3480 0.9161 0.4935 0.1618 1.0000 Uiso R . . . . .
H1052 H 0.3495 0.9977 0.4798 0.1618 1.0000 Uiso R . . . . .
H1061 H 0.3884 1.0048 0.5358 0.1522 1.0000 Uiso R . . . . .
H1062 H 0.3919 0.9522 0.5003 0.1522 1.0000 Uiso R . . . . .
H1071 H 0.4253 0.8682 0.5992 0.1476 1.0000 Uiso R . . . . .
H1072 H 0.4300 0.9221 0.5651 0.1476 1.0000 Uiso R . . . . .
H1081 H 0.4379 0.9864 0.6278 0.1447 1.0000 Uiso R . . . . .
H1082 H 0.4111 1.0126 0.5975 0.1447 1.0000 Uiso R . . . . .
H1111 H 0.4384 0.9005 0.6800 0.1296 1.0000 Uiso R . . . . .
H1112 H 0.4157 0.8959 0.7014 0.1296 1.0000 Uiso R . . . . .
H1141 H 0.3464 1.0855 0.6769 0.1329 1.0000 Uiso R . . . . .
H1142 H 0.3235 1.0412 0.6464 0.1329 1.0000 Uiso R . . . . .
H1171 H 0.3074 0.9325 0.5061 0.1700 1.0000 Uiso R . . . . .
H1172 H 0.3040 1.0177 0.5049 0.1700 1.0000 Uiso R . . . . .
H1211 H 0.3925 0.7870 0.5541 0.1448 1.0000 Uiso R . . . . .
H1212 H 0.3716 0.8198 0.5148 0.1448 1.0000 Uiso R . . . . .
H1231 H 0.3858 0.8600 0.4504 0.1438 1.0000 Uiso R . . . . .
H1281 H 0.4274 0.7450 0.5835 0.1444 1.0000 Uiso R . . . . .
H1291 H 0.4658 0.6753 0.6079 0.1498 1.0000 Uiso R . . . . .
H1311 H 0.4797 0.6969 0.4939 0.1458 1.0000 Uiso R . . . . .
H1331 H 0.5251 0.5801 0.6121 0.1804 1.0000 Uiso R . . . . .
H1332 H 0.5122 0.6450 0.6299 0.1804 1.0000 Uiso R . . . . .
H1333 H 0.4961 0.5737 0.6139 0.1804 1.0000 Uiso R . . . . .
H2011 H 0.2957 0.9367 0.8437 0.1370 1.0000 Uiso R . . . . .
H2012 H 0.2793 0.8650 0.8423 0.1370 1.0000 Uiso R . . . . .
H2021 H 0.2766 0.8609 0.7700 0.1375 1.0000 Uiso R . . . . .
H2022 H 0.2620 0.9298 0.7802 0.1375 1.0000 Uiso R . . . . .
H2031 H 0.2976 1.0341 0.8102 0.1409 1.0000 Uiso R . . . . .
H2032 H 0.2782 1.0574 0.7669 0.1409 1.0000 Uiso R . . . . .
H2041 H 0.3151 1.1310 0.7801 0.1357 1.0000 Uiso R . . . . .
H2042 H 0.3166 1.0746 0.7452 0.1357 1.0000 Uiso R . . . . .
H2051 H 0.3450 1.1155 0.8560 0.1374 1.0000 Uiso R . . . . .
H2052 H 0.3299 1.0412 0.8539 0.1374 1.0000 Uiso R . . . . .
H2061 H 0.3718 1.0398 0.9065 0.1395 1.0000 Uiso R . . . . .
H2062 H 0.3835 1.0388 0.8680 0.1395 1.0000 Uiso R . . . . .
H2071 H 0.3546 0.9176 0.9281 0.1479 1.0000 Uiso R . . . . .
H2072 H 0.3319 0.9544 0.8930 0.1479 1.0000 Uiso R . . . . .
H2081 H 0.3461 0.8123 0.8885 0.1360 1.0000 Uiso R . . . . .
H2082 H 0.3208 0.8354 0.9005 0.1360 1.0000 Uiso R . . . . .
H2111 H 0.3057 0.7410 0.8387 0.1191 1.0000 Uiso R . . . . .
H2112 H 0.2992 0.7743 0.7932 0.1191 1.0000 Uiso R . . . . .
H2141 H 0.2988 0.9899 0.7101 0.1317 1.0000 Uiso R . . . . .
H2142 H 0.2715 0.9545 0.7065 0.1317 1.0000 Uiso R . . . . .
H2171 H 0.3726 1.1273 0.8132 0.1325 1.0000 Uiso R . . . . .
H2172 H 0.3603 1.1118 0.7649 0.1325 1.0000 Uiso R . . . . .
H2211 H 0.3858 0.8503 0.8897 0.1469 1.0000 Uiso R . . . . .
H2212 H 0.3993 0.9069 0.8671 0.1469 1.0000 Uiso R . . . . .
H2231 H 0.3889 0.8581 0.9639 0.1392 1.0000 Uiso R . . . . .
H2281 H 0.4281 0.9886 0.8704 0.1549 1.0000 Uiso R . . . . .
H2291 H 0.4655 1.0631 0.8824 0.1721 1.0000 Uiso R . . . . .
H2311 H 0.4805 1.0321 1.0088 0.1744 1.0000 Uiso R . . . . .
H2331 H 0.5232 1.1617 0.9329 0.2304 1.0000 Uiso R . . . . .
H2332 H 0.5111 1.0965 0.9028 0.2304 1.0000 Uiso R . . . . .
H2333 H 0.4940 1.1654 0.9049 0.2304 1.0000 Uiso R . . . . .
H3011 H 0.4220 0.4615 0.7490 0.1694 1.0000 Uiso R . . . . .
H3012 H 0.3970 0.4921 0.7156 0.1694 1.0000 Uiso R . . . . .
H3021 H 0.3930 0.4248 0.7870 0.1796 1.0000 Uiso R . . . . .
H3022 H 0.3877 0.3806 0.7448 0.1796 1.0000 Uiso R . . . . .
H3031 H 0.3461 0.3594 0.7658 0.1703 1.0000 Uiso R . . . . .
H3032 H 0.3246 0.4206 0.7580 0.1703 1.0000 Uiso R . . . . .
H3041 H 0.3686 0.4264 0.8250 0.1734 1.0000 Uiso R . . . . .
H3042 H 0.3421 0.3972 0.8305 0.1734 1.0000 Uiso R . . . . .
H3051 H 0.3539 0.4969 0.8868 0.1663 1.0000 Uiso R . . . . .
H3052 H 0.3513 0.5794 0.8735 0.1663 1.0000 Uiso R . . . . .
H3061 H 0.3961 0.5420 0.9020 0.1606 1.0000 Uiso R . . . . .
H3062 H 0.3911 0.4955 0.8606 0.1606 1.0000 Uiso R . . . . .
H3071 H 0.4318 0.5910 0.8732 0.1601 1.0000 Uiso R . . . . .
H3072 H 0.4252 0.6433 0.8340 0.1601 1.0000 Uiso R . . . . .
H3081 H 0.4412 0.5302 0.8179 0.1604 1.0000 Uiso R . . . . .
H3082 H 0.4160 0.4959 0.8258 0.1604 1.0000 Uiso R . . . . .
H3111 H 0.4374 0.6067 0.7585 0.1473 1.0000 Uiso R . . . . .
H3112 H 0.4115 0.6127 0.7213 0.1473 1.0000 Uiso R . . . . .
H3141 H 0.3520 0.4111 0.6884 0.1571 1.0000 Uiso R . . . . .
H3142 H 0.3272 0.4516 0.6937 0.1571 1.0000 Uiso R . . . . .
H3171 H 0.3102 0.5525 0.8328 0.1719 1.0000 Uiso R . . . . .
H3172 H 0.3064 0.4720 0.8160 0.1719 1.0000 Uiso R . . . . .
H3211 H 0.3763 0.6652 0.8864 0.1550 1.0000 Uiso R . . . . .
H3212 H 0.3852 0.7137 0.8539 0.1550 1.0000 Uiso R . . . . .
H3231 H 0.3931 0.6551 0.9494 0.1736 1.0000 Uiso R . . . . .
H3281 H 0.4303 0.7654 0.8480 0.1749 1.0000 Uiso R . . . . .
H3291 H 0.4675 0.8378 0.8545 0.1824 1.0000 Uiso R . . . . .
H3311 H 0.4849 0.8261 0.9823 0.1912 1.0000 Uiso R . . . . .
H3331 H 0.5260 0.9393 0.8981 0.2510 1.0000 Uiso R . . . . .
H3332 H 0.5131 0.8713 0.8713 0.2510 1.0000 Uiso R . . . . .
H3333 H 0.4965 0.9421 0.8713 0.2510 1.0000 Uiso R . . . . .
H4011 H 0.3005 0.5605 0.4773 0.1760 1.0000 Uiso R . . . . .
H4012 H 0.2832 0.6295 0.4605 0.1760 1.0000 Uiso R . . . . .
H4021 H 0.2791 0.6360 0.5309 0.1821 1.0000 Uiso R . . . . .
H4022 H 0.2650 0.5672 0.5063 0.1821 1.0000 Uiso R . . . . .
H4031 H 0.2808 0.4396 0.5336 0.1903 1.0000 Uiso R . . . . .
H4032 H 0.2989 0.4651 0.5063 0.1903 1.0000 Uiso R . . . . .
H4041 H 0.3196 0.4144 0.5858 0.1813 1.0000 Uiso R . . . . .
H4042 H 0.3173 0.3646 0.5463 0.1813 1.0000 Uiso R . . . . .
H4051 H 0.3505 0.3822 0.5039 0.1816 1.0000 Uiso R . . . . .
H4052 H 0.3340 0.4539 0.4915 0.1816 1.0000 Uiso R . . . . .
H4061 H 0.3870 0.4625 0.5263 0.1859 1.0000 Uiso R . . . . .
H4062 H 0.3744 0.4662 0.4773 0.1859 1.0000 Uiso R . . . . .
H4071 H 0.3571 0.5901 0.4443 0.1768 1.0000 Uiso R . . . . .
H4072 H 0.3342 0.5526 0.4576 0.1768 1.0000 Uiso R . . . . .
H4081 H 0.3491 0.6911 0.4799 0.1776 1.0000 Uiso R . . . . .
H4082 H 0.3237 0.6727 0.4435 0.1776 1.0000 Uiso R . . . . .
H4111 H 0.2988 0.7271 0.5275 0.1674 1.0000 Uiso R . . . . .
H4112 H 0.3047 0.7585 0.4870 0.1674 1.0000 Uiso R . . . . .
H4141 H 0.3008 0.5055 0.6122 0.1819 1.0000 Uiso R . . . . .
H4142 H 0.2729 0.5337 0.5868 0.1819 1.0000 Uiso R . . . . .
H4171 H 0.3616 0.3875 0.6086 0.1711 1.0000 Uiso R . . . . .
H4172 H 0.3756 0.3729 0.5737 0.1711 1.0000 Uiso R . . . . .
H4211 H 0.4033 0.5861 0.5459 0.1669 1.0000 Uiso R . . . . .
H4212 H 0.3888 0.6533 0.5199 0.1669 1.0000 Uiso R . . . . .
H4231 H 0.3881 0.6528 0.4362 0.1563 1.0000 Uiso R . . . . .
H4281 H 0.4273 0.5169 0.5609 0.1639 1.0000 Uiso R . . . . .
H4291 H 0.4638 0.4391 0.5815 0.1732 1.0000 Uiso R . . . . .
H4311 H 0.4774 0.4693 0.4678 0.1651 1.0000 Uiso R . . . . .
H4331 H 0.5198 0.3341 0.5807 0.2203 1.0000 Uiso R . . . . .
H4333 H 0.5089 0.3994 0.6013 0.2203 1.0000 Uiso R . . . . .
H4334 H 0.4908 0.3326 0.5828 0.2203 1.0000 Uiso R . . . . .
H5011 H 0.1039 1.0078 0.2871 0.2089 1.0000 Uiso R . . . . .
H5012 H 0.0792 1.0436 0.2556 0.2089 1.0000 Uiso R . . . . .
H5021 H 0.1146 1.1199 0.2590 0.2153 1.0000 Uiso R . . . . .
H5022 H 0.1079 1.0775 0.2160 0.2153 1.0000 Uiso R . . . . .
H5031 H 0.1764 1.0698 0.2436 0.2127 1.0000 Uiso R . . . . .
H5032 H 0.1563 1.1346 0.2364 0.2127 1.0000 Uiso R . . . . .
H5041 H 0.1601 1.0966 0.1716 0.2134 1.0000 Uiso R . . . . .
H5043 H 0.1327 1.0735 0.1760 0.2134 1.0000 Uiso R . . . . .
H5051 H 0.1473 0.9169 0.1266 0.2069 1.0000 Uiso R . . . . .
H5052 H 0.1453 0.9997 0.1138 0.2069 1.0000 Uiso R . . . . .
H5061 H 0.1071 1.0029 0.1336 0.2041 1.0000 Uiso R . . . . .
H5062 H 0.1037 0.9489 0.0956 0.2041 1.0000 Uiso R . . . . .
H5071 H 0.0707 0.8683 0.1650 0.1970 1.0000 Uiso R . . . . .
H5072 H 0.0660 0.9226 0.1269 0.1970 1.0000 Uiso R . . . . .
H5081 H 0.0850 1.0125 0.1768 0.2010 1.0000 Uiso R . . . . .
H5082 H 0.0586 0.9852 0.1834 0.2010 1.0000 Uiso R . . . . .
H5112 H 0.0827 0.8972 0.2775 0.1966 1.0000 Uiso R . . . . .
H5113 H 0.0596 0.8986 0.2355 0.1966 1.0000 Uiso R . . . . .
H5141 H 0.1735 1.0503 0.3074 0.2079 1.0000 Uiso R . . . . .
H5142 H 0.1472 1.0789 0.3140 0.2079 1.0000 Uiso R . . . . .
H5171 H 0.1930 1.0044 0.1789 0.2101 1.0000 Uiso R . . . . .
H5172 H 0.1861 0.9208 0.1762 0.2101 1.0000 Uiso R . . . . .
H5211 H 0.1244 0.8167 0.1320 0.1749 1.0000 Uiso R . . . . .
H5212 H 0.1028 0.7861 0.1512 0.1749 1.0000 Uiso R . . . . .
H5231 H 0.1085 0.8616 0.0518 0.1658 1.0000 Uiso R . . . . .
H5282 H 0.0711 0.7414 0.1478 0.1648 1.0000 Uiso R . . . . .
H5291 H 0.0337 0.6683 0.1395 0.1686 1.0000 Uiso R . . . . .
H5311 H 0.0161 0.6901 0.0121 0.1583 1.0000 Uiso R . . . . .
H5332 H -0.0247 0.5685 0.0941 0.2049 1.0000 Uiso R . . . . .
H5333 H 0.0049 0.5645 0.1201 0.2049 1.0000 Uiso R . . . . .
H5334 H -0.0116 0.6346 0.1225 0.2049 1.0000 Uiso R . . . . .
H6011 H 0.2237 0.8789 0.5409 0.2356 1.0000 Uiso R . . . . .
H6012 H 0.2066 0.9499 0.5315 0.2356 1.0000 Uiso R . . . . .
H6021 H 0.2381 0.9589 0.4975 0.2408 1.0000 Uiso R . . . . .
H6023 H 0.2264 0.8873 0.4732 0.2408 1.0000 Uiso R . . . . .
H6031 H 0.2005 1.0556 0.4898 0.2429 1.0000 Uiso R . . . . .
H6032 H 0.2187 1.0800 0.4624 0.2429 1.0000 Uiso R . . . . .
H6041 H 0.1797 1.1449 0.4431 0.2424 1.0000 Uiso R . . . . .
H6042 H 0.1803 1.0905 0.4067 0.2424 1.0000 Uiso R . . . . .
H6051 H 0.1652 1.0617 0.5021 0.2351 1.0000 Uiso R . . . . .
H6052 H 0.1467 1.1284 0.4851 0.2351 1.0000 Uiso R . . . . .
H6061 H 0.1238 1.0459 0.5144 0.2356 1.0000 Uiso R . . . . .
H6062 H 0.1130 1.0385 0.4652 0.2356 1.0000 Uiso R . . . . .
H6072 H 0.1487 0.9402 0.5583 0.2327 1.0000 Uiso R . . . . .
H6073 H 0.1695 0.9734 0.5382 0.2327 1.0000 Uiso R . . . . .
H6081 H 0.1818 0.8555 0.5639 0.2249 1.0000 Uiso R . . . . .
H6083 H 0.1567 0.8281 0.5293 0.2249 1.0000 Uiso R . . . . .
H6111 H 0.1981 0.7580 0.5154 0.2282 1.0000 Uiso R . . . . .
H6112 H 0.2016 0.7911 0.4736 0.2282 1.0000 Uiso R . . . . .
H6141 H 0.2235 0.9760 0.4084 0.2317 1.0000 Uiso R . . . . .
H6142 H 0.1937 0.9956 0.3917 0.2317 1.0000 Uiso R . . . . .
H6171 H 0.1260 1.1390 0.4125 0.2391 1.0000 Uiso R . . . . .
H6173 H 0.1348 1.0974 0.3774 0.2391 1.0000 Uiso R . . . . .
H6211 H 0.1178 0.8601 0.5075 0.2212 1.0000 Uiso R . . . . .
H6212 H 0.1042 0.8884 0.4617 0.2212 1.0000 Uiso R . . . . .
H6231 H 0.1039 0.8577 0.5588 0.2176 1.0000 Uiso R . . . . .
H6281 H 0.0760 1.0056 0.4359 0.2525 1.0000 Uiso R . . . . .
H6291 H 0.0410 1.0868 0.4103 0.2663 1.0000 Uiso R . . . . .
H6311 H 0.0158 1.0457 0.5130 0.2574 1.0000 Uiso R . . . . .
H6331 H -0.0160 1.1924 0.3997 0.2838 1.0000 Uiso R . . . . .
H6332 H 0.0143 1.1926 0.4057 0.2838 1.0000 Uiso R . . . . .
H6334 H -0.0030 1.1284 0.3813 0.2838 1.0000 Uiso R . . . . .
H7011 H 0.0769 0.4725 0.3105 0.2062 1.0000 Uiso R . . . . .
H7012 H 0.1019 0.5102 0.3040 0.2062 1.0000 Uiso R . . . . .
H7022 H 0.1045 0.4261 0.3737 0.2113 1.0000 Uiso R . . . . .
H7023 H 0.1116 0.3932 0.3346 0.2113 1.0000 Uiso R . . . . .
H7031 H 0.1500 0.3654 0.3990 0.2209 1.0000 Uiso R . . . . .
H7032 H 0.1723 0.4239 0.4135 0.2209 1.0000 Uiso R . . . . .
H7041 H 0.1520 0.3967 0.4671 0.2247 1.0000 Uiso R . . . . .
H7042 H 0.1266 0.4316 0.4371 0.2247 1.0000 Uiso R . . . . .
H7052 H 0.1441 0.4932 0.5174 0.2261 1.0000 Uiso R . . . . .
H7053 H 0.1461 0.5764 0.5073 0.2261 1.0000 Uiso R . . . . .
H7061 H 0.1024 0.5435 0.4975 0.2182 1.0000 Uiso R . . . . .
H7062 H 0.1056 0.4929 0.4611 0.2182 1.0000 Uiso R . . . . .
H7071 H 0.0654 0.5781 0.4330 0.2066 1.0000 Uiso R . . . . .
H7072 H 0.0697 0.6354 0.4004 0.2066 1.0000 Uiso R . . . . .
H7081 H 0.0849 0.4952 0.3971 0.2118 1.0000 Uiso R . . . . .
H7082 H 0.0574 0.5194 0.3681 0.2118 1.0000 Uiso R . . . . .
H7111 H 0.0588 0.6150 0.3234 0.2051 1.0000 Uiso R . . . . .
H7113 H 0.0783 0.6179 0.2959 0.2051 1.0000 Uiso R . . . . .
H7141 H 0.1725 0.4605 0.3501 0.2014 1.0000 Uiso R . . . . .
H7142 H 0.1483 0.4232 0.3183 0.2014 1.0000 Uiso R . . . . .
H7172 H 0.1895 0.4630 0.4951 0.2345 1.0000 Uiso R . . . . .
H7173 H 0.1881 0.5467 0.5045 0.2345 1.0000 Uiso R . . . . .
H7211 H 0.1218 0.6704 0.4926 0.1955 1.0000 Uiso R . . . . .
H7212 H 0.1094 0.7106 0.4497 0.1955 1.0000 Uiso R . . . . .
H7231 H 0.1007 0.6477 0.5425 0.1903 1.0000 Uiso R . . . . .
H7281 H 0.0711 0.7619 0.4090 0.2189 1.0000 Uiso R . . . . .
H7292 H 0.0351 0.8363 0.3764 0.2377 1.0000 Uiso R . . . . .
H7311 H 0.0103 0.8249 0.4816 0.2305 1.0000 Uiso R . . . . .
H7331 H -0.0233 0.9407 0.3569 0.2903 1.0000 Uiso R . . . . .
H7332 H 0.0070 0.9416 0.3629 0.2903 1.0000 Uiso R . . . . .
H7333 H -0.0095 0.8718 0.3448 0.2903 1.0000 Uiso R . . . . .
H8011 H 0.2064 0.5612 0.1628 0.1973 1.0000 Uiso R . . . . .
H8012 H 0.2233 0.6314 0.1631 0.1973 1.0000 Uiso R . . . . .
H8021 H 0.2416 0.5689 0.2257 0.2035 1.0000 Uiso R . . . . .
H8022 H 0.2268 0.6367 0.2370 0.2035 1.0000 Uiso R . . . . .
H8032 H 0.2256 0.4396 0.2394 0.2096 1.0000 Uiso R . . . . .
H8033 H 0.2098 0.4670 0.1944 0.2096 1.0000 Uiso R . . . . .
H8041 H 0.1893 0.3671 0.2077 0.2046 1.0000 Uiso R . . . . .
H8043 H 0.1869 0.4073 0.2484 0.2046 1.0000 Uiso R . . . . .
H8051 H 0.1531 0.3855 0.1398 0.1901 1.0000 Uiso R . . . . .
H8052 H 0.1702 0.4557 0.1413 0.1901 1.0000 Uiso R . . . . .
H8061 H 0.1283 0.4712 0.0940 0.1773 1.0000 Uiso R . . . . .
H8062 H 0.1176 0.4684 0.1335 0.1773 1.0000 Uiso R . . . . .
H8071 H 0.1712 0.5525 0.1129 0.1770 1.0000 Uiso R . . . . .
H8073 H 0.1492 0.5916 0.0777 0.1770 1.0000 Uiso R . . . . .
H8081 H 0.1827 0.6733 0.1086 0.1808 1.0000 Uiso R . . . . .
H8082 H 0.1574 0.6936 0.1216 0.1808 1.0000 Uiso R . . . . .
H8111 H 0.2030 0.7191 0.2210 0.1833 1.0000 Uiso R . . . . .
H8112 H 0.2027 0.7554 0.1779 0.1833 1.0000 Uiso R . . . . .
H8141 H 0.2323 0.5327 0.2990 0.2008 1.0000 Uiso R . . . . .
H8142 H 0.2036 0.5072 0.2956 0.2008 1.0000 Uiso R . . . . .
H8171 H 0.1459 0.4013 0.2398 0.1926 1.0000 Uiso R . . . . .
H8172 H 0.1328 0.3724 0.1940 0.1926 1.0000 Uiso R . . . . .
H8212 H 0.1027 0.6008 0.1354 0.1667 1.0000 Uiso R . . . . .
H8213 H 0.1177 0.6590 0.1164 0.1667 1.0000 Uiso R . . . . .
H8231 H 0.1115 0.6582 0.0358 0.1615 1.0000 Uiso R . . . . .
H8282 H 0.0792 0.5163 0.1309 0.1675 1.0000 Uiso R . . . . .
H8291 H 0.0441 0.4340 0.1217 0.1766 1.0000 Uiso R . . . . .
H8311 H 0.0244 0.4670 -0.0052 0.1788 1.0000 Uiso R . . . . .
H8331 H -0.0117 0.3244 0.0745 0.2220 1.0000 Uiso R . . . . .
H8332 H 0.0180 0.3257 0.1006 0.2220 1.0000 Uiso R . . . . .
H8333 H -0.0005 0.3903 0.1046 0.2220 1.0000 Uiso R . . . . .
H1091 H 0.3193 0.8248 0.6430 0.1405 1.0000 Uiso R . . . . .
H1092 H 0.3270 0.7577 0.6189 0.1405 1.0000 Uiso R . . . . .
H2091 H 0.3663 0.8699 0.7225 0.0940 1.0000 Uiso R . . . . .
H2092 H 0.3864 0.8136 0.7560 0.0940 1.0000 Uiso R . . . . .
H3091 H 0.3291 0.7440 0.7242 0.1310 1.0000 Uiso R . . . . .
H3092 H 0.3219 0.6820 0.6940 0.1310 1.0000 Uiso R . . . . .
H4091 H 0.3902 0.6820 0.6472 0.1530 1.0000 Uiso R . . . . .
H4092 H 0.3701 0.6232 0.6614 0.1530 1.0000 Uiso R . . . . .
H5091 H 0.1830 0.8283 0.3000 0.1813 1.0000 Uiso R . . . . .
H5092 H 0.1748 0.7581 0.2757 0.1813 1.0000 Uiso R . . . . .
H6091 H 0.1224 0.8339 0.3405 0.2104 1.0000 Uiso R . . . . .
H6092 H 0.1197 0.7933 0.3702 0.2104 1.0000 Uiso R . . . . .
H7091 H 0.1685 0.7523 0.3764 0.1953 1.0000 Uiso R . . . . .
H7092 H 0.1785 0.6877 0.3624 0.1953 1.0000 Uiso R . . . . .
H8091 H 0.1187 0.7068 0.2374 0.1726 1.0000 Uiso R . . . . .
H8092 H 0.1207 0.6656 0.2669 0.1726 1.0000 Uiso R . . . . .

_refine_ls_extinction_method     None
_oxford_refine_ls_scale          0.4042(8)
loop_
_geom_bond_atom_site_label_1
_geom_bond_site_symmetry_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_2
_geom_bond_distance
_geom_bond_publ_flag
Eu1 . N101 . 2.708(7) yes
Eu1 . N102 . 2.720(6) yes
Eu1 . N103 . 2.710(7) yes
Eu1 . N104 . 2.715(6) yes
Eu1 . O101 . 2.379(7) yes
Eu1 . O102 . 2.374(7) yes
Eu1 . O103 . 2.376(7) yes
Eu1 . O109 . 2.424(7) yes
Eu1 . O413 . 2.225(11) yes
N101 . C101 . 1.522(7) yes
N101 . C108 . 1.526(7) yes
N101 . C111 . 1.488(7) yes
N102 . C102 . 1.524(7) yes
N102 . C103 . 1.526(7) yes
N102 . C114 . 1.487(7) yes
N103 . C104 . 1.518(7) yes
N103 . C105 . 1.513(7) yes
N103 . C117 . 1.482(7) yes
N104 . C106 . 1.525(7) yes
N104 . C107 . 1.527(7) yes
N104 . C121 . 1.528(7) yes
O101 . C112 . 1.325(6) yes
O102 . C115 . 1.328(5) yes
O103 . C118 . 1.326(6) yes
O109 . H1091 . 0.950 no
O109 . H1092 . 0.950 no
C101 . C102 . 1.481(7) yes
C101 . H1011 . 0.950 no
C101 . H1012 . 0.950 no
C102 . H1021 . 0.950 no
C102 . H1022 . 0.950 no
C103 . C104 . 1.483(7) yes
C103 . H1031 . 0.950 no
C103 . H1032 . 0.950 no
C104 . H1041 . 0.950 no
C104 . H1042 . 0.950 no
C105 . C106 . 1.490(7) yes
C105 . H1051 . 0.950 no
C105 . H1052 . 0.950 no
C106 . H1061 . 0.950 no
C106 . H1062 . 0.950 no
C107 . C108 . 1.486(7) yes
C107 . H1071 . 0.950 no
C107 . H1072 . 0.950 no
C108 . H1081 . 0.950 no
C108 . H1082 . 0.950 no
C111 . C112 . 1.505(6) yes
C111 . H1111 . 0.950 no
C111 . H1112 . 0.950 no
C112 . O113 . 1.203(6) yes
C114 . C115 . 1.504(5) yes
C114 . H1141 . 0.950 no
C114 . H1142 . 0.950 no
C115 . O116 . 1.199(5) yes
O116 . Eu2 . 2.469(9) yes
C117 . C118 . 1.507(6) yes
C117 . H1171 . 0.950 no
C117 . H1172 . 0.950 no
C118 . O119 . 1.205(6) yes
O120 . C124 . 1.251(7) yes
C121 . C122 . 1.551(8) yes
C121 . H1211 . 0.950 no
C121 . H1212 . 0.950 no
C122 . C123 . 1.382(8) yes
C122 . C127 . 1.439(8) yes
C123 . C124 . 1.469(7) yes
C123 . H1231 . 0.950 no
C124 . O125 . 1.331(7) yes
O125 . C126 . 1.361(7) yes
C126 . C127 . 1.373(7) yes
C126 . C131 . 1.369(6) yes
C127 . C128 . 1.375(7) yes
C128 . C129 . 1.372(6) yes
C128 . H1281 . 0.950 no
C129 . C130 . 1.371(6) yes
C129 . H1291 . 0.950 no
C130 . C131 . 1.375(6) yes
C130 . O132 . 1.416(5) yes
C131 . H1311 . 0.950 no
O132 . C133 . 1.416(6) yes
C133 . H1331 . 0.950 no
C133 . H1332 . 0.950 no
C133 . H1333 . 0.950 no
Eu2 . N201 . 2.713(6) yes
Eu2 . N202 . 2.685(7) yes
Eu2 . N203 . 2.689(6) yes
Eu2 . N204 . 2.706(6) yes
Eu2 . O201 . 2.368(7) yes
Eu2 . O202 . 2.372(7) yes
Eu2 . O203 . 2.377(7) yes
Eu2 . O209 . 2.415(7) yes
N201 . C201 . 1.515(7) yes
N201 . C208 . 1.515(7) yes
N201 . C211 . 1.481(7) yes
N202 . C202 . 1.510(7) yes
N202 . C203 . 1.511(7) yes
N202 . C214 . 1.485(7) yes
N203 . C204 . 1.518(7) yes
N203 . C205 . 1.519(7) yes
N203 . C217 . 1.487(7) yes
N204 . C206 . 1.518(7) yes
N204 . C207 . 1.515(7) yes
N204 . C221 . 1.511(7) yes
O201 . C212 . 1.326(5) yes
O202 . C215 . 1.326(5) yes
O203 . C218 . 1.323(5) yes
O209 . H2091 . 0.958 no
O209 . H2092 . 0.950 no
C201 . C202 . 1.487(7) yes
C201 . H2011 . 0.950 no
C201 . H2012 . 0.950 no
C202 . H2021 . 0.950 no
C202 . H2022 . 0.950 no
C203 . C204 . 1.488(7) yes
C203 . H2031 . 0.950 no
C203 . H2032 . 0.950 no
C204 . H2041 . 0.950 no
C204 . H2042 . 0.950 no
C205 . C206 . 1.502(7) yes
C205 . H2051 . 0.950 no
C205 . H2052 . 0.950 no
C206 . H2061 . 0.950 no
C206 . H2062 . 0.950 no
C207 . C208 . 1.471(7) yes
C207 . H2071 . 0.950 no
C207 . H2072 . 0.950 no
C208 . H2081 . 0.950 no
C208 . H2082 . 0.950 no
C211 . C212 . 1.505(6) yes
C211 . H2111 . 0.950 no
C211 . H2112 . 0.950 no
C212 . O213 . 1.202(5) yes
O213 . Eu3 . 2.255(10) yes
C214 . C215 . 1.503(6) yes
C214 . H2141 . 0.950 no
C214 . H2142 . 0.950 no
C215 . O216 . 1.204(5) yes
C217 . C218 . 1.505(6) yes
C217 . H2171 . 0.950 no
C217 . H2172 . 0.950 no
C218 . O219 . 1.199(6) yes
O220 . C224 . 1.256(7) yes
C221 . C222 . 1.544(8) yes
C221 . H2211 . 0.950 no
C221 . H2212 . 0.950 no
C222 . C223 . 1.376(8) yes
C222 . C227 . 1.433(8) yes
C223 . C224 . 1.463(8) yes
C223 . H2231 . 0.950 no
C224 . O225 . 1.328(8) yes
O225 . C226 . 1.352(7) yes
C226 . C227 . 1.367(7) yes
C226 . C231 . 1.373(6) yes
C227 . C228 . 1.375(7) yes
C228 . C229 . 1.373(7) yes
C228 . H2281 . 0.950 no
C229 . C230 . 1.373(6) yes
C229 . H2291 . 0.950 no
C230 . C231 . 1.371(6) yes
C230 . O232 . 1.418(5) yes
C231 . H2311 . 0.950 no
O232 . C233 . 1.419(6) yes
C233 . H2331 . 0.950 no
C233 . H2332 . 0.950 no
C233 . H2333 . 0.950 no
Eu3 . N301 . 2.707(7) yes
Eu3 . N302 . 2.714(7) yes
Eu3 . N303 . 2.707(6) yes
Eu3 . N304 . 2.722(7) yes
Eu3 . O301 . 2.373(7) yes
Eu3 . O302 . 2.367(7) yes
Eu3 . O303 . 2.380(7) yes
Eu3 . O309 . 2.427(7) yes
N301 . C301 . 1.523(7) yes
N301 . C308 . 1.523(7) yes
N301 . C311 . 1.487(7) yes
N302 . C302 . 1.524(7) yes
N302 . C303 . 1.525(7) yes
N302 . C314 . 1.483(7) yes
N303 . C304 . 1.523(7) yes
N303 . C305 . 1.523(7) yes
N303 . C317 . 1.488(7) yes
N304 . C306 . 1.533(7) yes
N304 . C307 . 1.533(7) yes
N304 . C321 . 1.545(7) yes
O301 . C312 . 1.324(6) yes
O302 . C315 . 1.326(5) yes
O303 . C318 . 1.326(6) yes
O309 . H3091 . 0.950 no
O309 . H3092 . 0.950 no
C301 . C302 . 1.485(7) yes
C301 . H3011 . 0.950 no
C301 . H3012 . 0.950 no
C302 . H3021 . 0.950 no
C302 . H3022 . 0.950 no
C303 . C304 . 1.479(7) yes
C303 . H3031 . 0.950 no
C303 . H3032 . 0.950 no
C304 . H3041 . 0.950 no
C304 . H3042 . 0.950 no
C305 . C306 . 1.490(7) yes
C305 . H3051 . 0.950 no
C305 . H3052 . 0.950 no
C306 . H3061 . 0.950 no
C306 . H3062 . 0.950 no
C307 . C308 . 1.481(7) yes
C307 . H3071 . 0.950 no
C307 . H3072 . 0.950 no
C308 . H3081 . 0.950 no
C308 . H3082 . 0.950 no
C311 . C312 . 1.502(6) yes
C311 . H3111 . 0.950 no
C311 . H3112 . 0.950 no
C312 . O313 . 1.200(6) yes
C314 . C315 . 1.499(6) yes
C314 . H3141 . 0.950 no
C314 . H3142 . 0.950 no
C315 . O316 . 1.200(5) yes
O316 . Eu4 . 2.388(11) yes
C317 . C318 . 1.506(6) yes
C317 . H3171 . 0.950 no
C317 . H3172 . 0.950 no
C318 . O319 . 1.204(6) yes
O320 . C324 . 1.251(7) yes
C321 . C322 . 1.558(8) yes
C321 . H3211 . 0.950 no
C321 . H3212 . 0.950 no
C322 . C323 . 1.389(8) yes
C322 . C327 . 1.447(8) yes
C323 . C324 . 1.471(8) yes
C323 . H3231 . 0.950 no
C324 . O325 . 1.337(8) yes
O325 . C326 . 1.360(8) yes
C326 . C327 . 1.375(7) yes
C326 . C331 . 1.369(6) yes
C327 . C328 . 1.374(7) yes
C328 . C329 . 1.372(7) yes
C328 . H3281 . 0.950 no
C329 . C330 . 1.372(6) yes
C329 . H3291 . 0.950 no
C330 . C331 . 1.372(6) yes
C330 . O332 . 1.416(5) yes
C331 . H3311 . 0.950 no
O332 . C333 . 1.419(6) yes
C333 . H3331 . 0.950 no
C333 . H3332 . 0.950 no
C333 . H3333 . 0.950 no
Eu4 . N401 . 2.730(7) yes
Eu4 . N402 . 2.697(7) yes
Eu4 . N403 . 2.692(7) yes
Eu4 . N404 . 2.697(6) yes
Eu4 . O401 . 2.372(7) yes
Eu4 . O402 . 2.382(7) yes
Eu4 . O403 . 2.379(7) yes
Eu4 . O409 . 2.423(7) yes
N401 . C401 . 1.532(7) yes
N401 . C408 . 1.526(7) yes
N401 . C411 . 1.502(7) yes
N402 . C402 . 1.532(7) yes
N402 . C403 . 1.515(7) yes
N402 . C414 . 1.486(7) yes
N403 . C404 . 1.511(7) yes
N403 . C405 . 1.510(7) yes
N403 . C417 . 1.483(7) yes
N404 . C406 . 1.512(7) yes
N404 . C407 . 1.505(7) yes
N404 . C421 . 1.511(7) yes
O401 . C412 . 1.325(6) yes
O402 . C415 . 1.325(5) yes
O403 . C418 . 1.328(6) yes
O409 . H4091 . 0.950 no
O409 . H4092 . 0.965 no
C401 . C402 . 1.487(7) yes
C401 . H4011 . 0.950 no
C401 . H4012 . 0.950 no
C402 . H4021 . 0.950 no
C402 . H4022 . 0.950 no
C403 . C404 . 1.474(7) yes
C403 . H4031 . 0.950 no
C403 . H4032 . 0.950 no
C404 . H4041 . 0.950 no
C404 . H4042 . 0.950 no
C405 . C406 . 1.490(7) yes
C405 . H4051 . 0.950 no
C405 . H4052 . 0.950 no
C406 . H4061 . 0.950 no
C406 . H4062 . 0.950 no
C407 . C408 . 1.468(7) yes
C407 . H4071 . 0.950 no
C407 . H4072 . 0.950 no
C408 . H4081 . 0.950 no
C408 . H4082 . 0.950 no
C411 . C412 . 1.501(6) yes
C411 . H4111 . 0.950 no
C411 . H4112 . 0.950 no
C412 . O413 . 1.200(5) yes
C414 . C415 . 1.506(6) yes
C414 . H4141 . 0.950 no
C414 . H4142 . 0.950 no
C415 . O416 . 1.205(6) yes
C417 . C418 . 1.502(6) yes
C417 . H4171 . 0.950 no
C417 . H4172 . 0.950 no
C418 . O419 . 1.203(6) yes
O420 . C424 . 1.246(7) yes
C421 . C422 . 1.547(8) yes
C421 . H4211 . 0.950 no
C421 . H4212 . 0.950 no
C422 . C423 . 1.382(8) yes
C422 . C427 . 1.436(8) yes
C423 . C424 . 1.463(8) yes
C423 . H4231 . 0.950 no
C424 . O425 . 1.324(7) yes
O425 . C426 . 1.360(7) yes
C426 . C427 . 1.372(7) yes
C426 . C431 . 1.373(6) yes
C427 . C428 . 1.373(7) yes
C428 . C429 . 1.371(7) yes
C428 . H4281 . 0.950 no
C429 . C430 . 1.372(6) yes
C429 . H4291 . 0.950 no
C430 . C431 . 1.373(6) yes
C430 . O432 . 1.417(5) yes
C431 . H4311 . 0.950 no
O432 . C433 . 1.417(6) yes
C433 . H4331 . 0.950 no
C433 . H4333 . 0.950 no
C433 . H4334 . 0.950 no
Eu5 . N501 . 2.704(7) yes
Eu5 . N502 . 2.704(7) yes
Eu5 . N503 . 2.694(7) yes
Eu5 . N504 . 2.712(7) yes
Eu5 . O501 . 2.375(8) yes
Eu5 . O502 . 2.376(8) yes
Eu5 . O503 . 2.373(8) yes
Eu5 . O509 . 2.420(8) yes
Eu5 . O813 . 2.639(15) yes
N501 . C501 . 1.519(7) yes
N501 . C508 . 1.520(7) yes
N501 . C511 . 1.486(7) yes
N502 . C502 . 1.520(7) yes
N502 . C503 . 1.514(7) yes
N502 . C514 . 1.497(7) yes
N503 . C504 . 1.510(7) yes
N503 . C505 . 1.509(7) yes
N503 . C517 . 1.481(7) yes
N504 . C506 . 1.516(7) yes
N504 . C507 . 1.521(7) yes
N504 . C521 . 1.528(7) yes
O501 . C512 . 1.324(6) yes
O502 . C515 . 1.325(6) yes
O503 . C518 . 1.325(6) yes
O509 . H5091 . 0.950 no
O509 . H5092 . 0.950 no
C501 . C502 . 1.492(7) yes
C501 . H5011 . 0.950 no
C501 . H5012 . 0.950 no
C502 . H5021 . 0.950 no
C502 . H5022 . 0.950 no
C503 . C504 . 1.479(7) yes
C503 . H5031 . 0.950 no
C503 . H5032 . 0.950 no
C504 . H5041 . 0.950 no
C504 . H5043 . 0.950 no
C505 . C506 . 1.475(7) yes
C505 . H5051 . 0.950 no
C505 . H5052 . 0.950 no
C506 . H5061 . 0.950 no
C506 . H5062 . 0.950 no
C507 . C508 . 1.486(7) yes
C507 . H5071 . 0.950 no
C507 . H5072 . 0.950 no
C508 . H5081 . 0.950 no
C508 . H5082 . 0.950 no
C511 . C512 . 1.507(6) yes
C511 . H5112 . 0.950 no
C511 . H5113 . 0.950 no
C512 . O513 . 1.204(6) yes
C514 . C515 . 1.503(6) yes
C514 . H5141 . 0.950 no
C514 . H5142 . 0.950 no
C515 . O516 . 1.203(6) yes
O516 . Eu6 . 2.319(16) yes
C517 . C518 . 1.505(6) yes
C517 . H5171 . 0.950 no
C517 . H5172 . 0.950 no
C518 . O519 . 1.203(6) yes
O520 . C524 . 1.244(7) yes
C521 . C522 . 1.552(8) yes
C521 . H5211 . 0.950 no
C521 . H5212 . 0.950 no
C522 . C523 . 1.384(8) yes
C522 . C527 . 1.440(8) yes
C523 . C524 . 1.467(8) yes
C523 . H5231 . 0.950 no
C524 . O525 . 1.331(8) yes
O525 . C526 . 1.361(7) yes
C526 . C527 . 1.373(7) yes
C526 . C531 . 1.372(6) yes
C527 . C528 . 1.371(7) yes
C528 . C529 . 1.372(7) yes
C528 . H5282 . 0.950 no
C529 . C530 . 1.373(6) yes
C529 . H5291 . 0.950 no
C530 . C531 . 1.371(6) yes
C530 . O532 . 1.418(5) yes
C531 . H5311 . 0.950 no
O532 . C533 . 1.417(6) yes
C533 . H5332 . 0.950 no
C533 . H5333 . 0.950 no
C533 . H5334 . 0.950 no
Eu6 . N601 . 2.698(7) yes
Eu6 . N602 . 2.691(7) yes
Eu6 . N603 . 2.703(7) yes
Eu6 . N604 . 2.699(7) yes
Eu6 . O601 . 2.373(8) yes
Eu6 . O602 . 2.372(8) yes
Eu6 . O603 . 2.373(8) yes
Eu6 . O609 . 2.429(8) yes
N601 . C601 . 1.506(7) yes
N601 . C608 . 1.515(7) yes
N601 . C611 . 1.478(7) yes
N602 . C602 . 1.494(7) yes
N602 . C603 . 1.493(7) yes
N602 . C614 . 1.472(7) yes
N603 . C604 . 1.518(7) yes
N603 . C605 . 1.522(7) yes
N603 . C617 . 1.501(7) yes
N604 . C606 . 1.520(7) yes
N604 . C607 . 1.520(7) yes
N604 . C621 . 1.529(7) yes
O601 . C612 . 1.325(6) yes
O602 . C615 . 1.327(6) yes
O603 . C618 . 1.324(6) yes
O609 . H6091 . 0.950 no
O609 . H6092 . 0.950 no
C601 . C602 . 1.470(7) yes
C601 . H6011 . 0.950 no
C601 . H6012 . 0.950 no
C602 . H6021 . 0.950 no
C602 . H6023 . 0.950 no
C603 . C604 . 1.478(7) yes
C603 . H6031 . 0.950 no
C603 . H6032 . 0.950 no
C604 . H6041 . 0.950 no
C604 . H6042 . 0.950 no
C605 . C606 . 1.490(7) yes
C605 . H6051 . 0.950 no
C605 . H6052 . 0.950 no
C606 . H6061 . 0.950 no
C606 . H6062 . 0.950 no
C607 . C608 . 1.483(7) yes
C607 . H6072 . 0.950 no
C607 . H6073 . 0.950 no
C608 . H6081 . 0.950 no
C608 . H6083 . 0.950 no
C611 . C612 . 1.505(6) yes
C611 . H6111 . 0.950 no
C611 . H6112 . 0.950 no
C612 . O613 . 1.202(6) yes
O613 . Eu7 . 2.698(18) yes
C614 . C615 . 1.507(6) yes
C614 . H6141 . 0.950 no
C614 . H6142 . 0.950 no
C615 . O616 . 1.203(6) yes
C617 . C618 . 1.504(6) yes
C617 . H6171 . 0.950 no
C617 . H6173 . 0.950 no
C618 . O619 . 1.205(6) yes
O620 . C624 . 1.248(7) yes
C621 . C622 . 1.557(8) yes
C621 . H6211 . 0.950 no
C621 . H6212 . 0.950 no
C622 . C623 . 1.383(8) yes
C622 . C627 . 1.442(8) yes
C623 . C624 . 1.463(8) yes
C623 . H6231 . 0.950 no
C624 . O625 . 1.330(8) yes
O625 . C626 . 1.359(8) yes
C626 . C627 . 1.373(7) yes
C626 . C631 . 1.374(6) yes
C627 . C628 . 1.372(7) yes
C628 . C629 . 1.371(7) yes
C628 . H6281 . 0.950 no
C629 . C630 . 1.373(6) yes
C629 . H6291 . 0.950 no
C630 . C631 . 1.369(6) yes
C630 . O632 . 1.419(5) yes
C631 . H6311 . 0.950 no
O632 . C633 . 1.421(6) yes
C633 . H6331 . 0.950 no
C633 . H6332 . 0.950 no
C633 . H6334 . 0.950 no
Eu7 . N701 . 2.703(7) yes
Eu7 . N702 . 2.710(7) yes
Eu7 . N703 . 2.712(7) yes
Eu7 . N704 . 2.703(7) yes
Eu7 . O701 . 2.379(8) yes
Eu7 . O702 . 2.378(8) yes
Eu7 . O703 . 2.379(8) yes
Eu7 . O709 . 2.428(8) yes
N701 . C701 . 1.523(7) yes
N701 . C708 . 1.521(7) yes
N701 . C711 . 1.489(7) yes
N702 . C702 . 1.525(7) yes
N702 . C703 . 1.530(7) yes
N702 . C714 . 1.500(7) yes
N703 . C704 . 1.531(7) yes
N703 . C705 . 1.528(7) yes
N703 . C717 . 1.503(7) yes
N704 . C706 . 1.521(7) yes
N704 . C707 . 1.523(7) yes
N704 . C721 . 1.527(7) yes
O701 . C712 . 1.325(6) yes
O702 . C715 . 1.326(6) yes
O703 . C718 . 1.323(6) yes
O709 . H7091 . 0.950 no
O709 . H7092 . 0.950 no
C701 . C702 . 1.479(7) yes
C701 . H7011 . 0.950 no
C701 . H7012 . 0.950 no
C702 . H7022 . 0.950 no
C702 . H7023 . 0.950 no
C703 . C704 . 1.481(7) yes
C703 . H7031 . 0.950 no
C703 . H7032 . 0.950 no
C704 . H7041 . 0.950 no
C704 . H7042 . 0.950 no
C705 . C706 . 1.478(7) yes
C705 . H7052 . 0.950 no
C705 . H7053 . 0.950 no
C706 . H7061 . 0.950 no
C706 . H7062 . 0.950 no
C707 . C708 . 1.484(7) yes
C707 . H7071 . 0.950 no
C707 . H7072 . 0.950 no
C708 . H7081 . 0.950 no
C708 . H7082 . 0.950 no
C711 . C712 . 1.502(6) yes
C711 . H7111 . 0.950 no
C711 . H7113 . 0.950 no
C712 . O713 . 1.200(6) yes
C714 . C715 . 1.503(6) yes
C714 . H7141 . 0.950 no
C714 . H7142 . 0.950 no
C715 . O716 . 1.203(6) yes
O716 . Eu8 . 2.199(14) yes
C717 . C718 . 1.501(6) yes
C717 . H7172 . 0.950 no
C717 . H7173 . 0.950 no
C718 . O719 . 1.204(6) yes
O720 . C724 . 1.245(7) yes
C721 . C722 . 1.555(8) yes
C721 . H7211 . 0.950 no
C721 . H7212 . 0.950 no
C722 . C723 . 1.386(8) yes
C722 . C727 . 1.443(8) yes
C723 . C724 . 1.463(8) yes
C723 . H7231 . 0.950 no
C724 . O725 . 1.325(8) yes
O725 . C726 . 1.359(8) yes
C726 . C727 . 1.373(7) yes
C726 . C731 . 1.372(6) yes
C727 . C728 . 1.372(7) yes
C728 . C729 . 1.372(7) yes
C728 . H7281 . 0.950 no
C729 . C730 . 1.373(6) yes
C729 . H7292 . 0.950 no
C730 . C731 . 1.371(6) yes
C730 . O732 . 1.418(5) yes
C731 . H7311 . 0.950 no
O732 . C733 . 1.420(6) yes
C733 . H7331 . 0.950 no
C733 . H7332 . 0.950 no
C733 . H7333 . 0.950 no
Eu8 . N801 . 2.711(7) yes
Eu8 . N802 . 2.710(7) yes
Eu8 . N803 . 2.692(7) yes
Eu8 . N804 . 2.698(7) yes
Eu8 . O801 . 2.374(8) yes
Eu8 . O802 . 2.375(7) yes
Eu8 . O803 . 2.380(8) yes
Eu8 . O809 . 2.425(8) yes
N801 . C801 . 1.522(7) yes
N801 . C808 . 1.510(7) yes
N801 . C811 . 1.483(7) yes
N802 . C802 . 1.535(7) yes
N802 . C803 . 1.508(7) yes
N802 . C814 . 1.482(7) yes
N803 . C804 . 1.500(7) yes
N803 . C805 . 1.508(7) yes
N803 . C817 . 1.486(7) yes
N804 . C806 . 1.514(7) yes
N804 . C807 . 1.516(7) yes
N804 . C821 . 1.518(7) yes
O801 . C812 . 1.325(6) yes
O802 . C815 . 1.324(6) yes
O803 . C818 . 1.324(6) yes
O809 . H8091 . 0.950 no
O809 . H8092 . 0.950 no
C801 . C802 . 1.492(7) yes
C801 . H8011 . 0.950 no
C801 . H8012 . 0.950 no
C802 . H8021 . 0.950 no
C802 . H8022 . 0.950 no
C803 . C804 . 1.457(7) yes
C803 . H8032 . 0.950 no
C803 . H8033 . 0.950 no
C804 . H8041 . 0.950 no
C804 . H8043 . 0.950 no
C805 . C806 . 1.490(7) yes
C805 . H8051 . 0.950 no
C805 . H8052 . 0.950 no
C806 . H8061 . 0.950 no
C806 . H8062 . 0.950 no
C807 . C808 . 1.480(7) yes
C807 . H8071 . 0.950 no
C807 . H8073 . 0.950 no
C808 . H8081 . 0.950 no
C808 . H8082 . 0.950 no
C811 . C812 . 1.502(6) yes
C811 . H8111 . 0.950 no
C811 . H8112 . 0.950 no
C812 . O813 . 1.201(6) yes
C814 . C815 . 1.509(6) yes
C814 . H8141 . 0.950 no
C814 . H8142 . 0.950 no
C815 . O816 . 1.203(6) yes
C817 . C818 . 1.503(6) yes
C817 . H8171 . 0.950 no
C817 . H8172 . 0.950 no
C818 . O819 . 1.203(6) yes
O820 . C824 . 1.247(7) yes
C821 . C822 . 1.555(8) yes
C821 . H8212 . 0.950 no
C821 . H8213 . 0.950 no
C822 . C823 . 1.383(8) yes
C822 . C827 . 1.439(8) yes
C823 . C824 . 1.466(8) yes
C823 . H8231 . 0.950 no
C824 . O825 . 1.329(8) yes
O825 . C826 . 1.358(8) yes
C826 . C827 . 1.373(7) yes
C826 . C831 . 1.372(6) yes
C827 . C828 . 1.372(7) yes
C828 . C829 . 1.374(7) yes
C828 . H8282 . 0.950 no
C829 . C830 . 1.372(6) yes
C829 . H8291 . 0.950 no
C830 . C831 . 1.373(6) yes
C830 . O832 . 1.418(5) yes
C831 . H8311 . 0.950 no
O832 . C833 . 1.419(6) yes
C833 . H8331 . 0.950 no
C833 . H8332 . 0.950 no
C833 . H8333 . 0.950 no
loop_
_geom_angle_atom_site_label_1
_geom_angle_site_symmetry_1
_geom_angle_atom_site_label_2
_geom_angle_site_symmetry_2
_geom_angle_atom_site_label_3
_geom_angle_site_symmetry_3
_geom_angle
_geom_angle_publ_flag
N101 . Eu1 . N102 . 67.1(2) yes
N101 . Eu1 . N103 . 103.3(3) yes
N102 . Eu1 . N103 . 67.1(2) yes
N101 . Eu1 . N104 . 67.3(2) yes
N102 . Eu1 . N104 . 102.9(2) yes
N103 . Eu1 . N104 . 67.4(2) yes
N101 . Eu1 . O101 . 65.6(4) yes
N102 . Eu1 . O101 . 128.8(4) yes
N103 . Eu1 . O101 . 142.9(3) yes
N104 . Eu1 . O101 . 75.9(3) yes
N101 . Eu1 . O102 . 72.3(3) yes
N102 . Eu1 . O102 . 64.4(3) yes
N103 . Eu1 . O102 . 128.8(3) yes
N104 . Eu1 . O102 . 139.3(3) yes
O101 . Eu1 . O102 . 83.4(3) yes
N101 . Eu1 . O103 . 135.8(3) yes
N102 . Eu1 . O103 . 69.5(3) yes
N103 . Eu1 . O103 . 66.2(4) yes
N104 . Eu1 . O103 . 131.9(4) yes
O101 . Eu1 . O103 . 146.7(4) yes
N101 . Eu1 . O109 . 127.1(6) yes
N102 . Eu1 . O109 . 121.1(5) yes
N103 . Eu1 . O109 . 128.8(6) yes
N104 . Eu1 . O109 . 136.0(5) yes
O101 . Eu1 . O109 . 75.9(6) yes
N101 . Eu1 . O413 . 136.7(4) yes
N102 . Eu1 . O413 . 138.4(4) yes
N103 . Eu1 . O413 . 73.3(3) yes
N104 . Eu1 . O413 . 72.0(3) yes
O101 . Eu1 . O413 . 90.9(5) yes
O102 . Eu1 . O103 . 82.0(4) yes
O102 . Eu1 . O109 . 68.4(5) yes
O103 . Eu1 . O109 . 71.0(7) yes
O102 . Eu1 . O413 . 143.7(3) yes
O103 . Eu1 . O413 . 83.6(4) yes
O109 . Eu1 . O413 . 75.4(5) yes
Eu1 . N101 . C101 . 109.3(5) yes
Eu1 . N101 . C108 . 109.5(5) yes
C101 . N101 . C108 . 108.9(6) yes
Eu1 . N101 . C111 . 107.2(8) yes
C101 . N101 . C111 . 111.3(5) yes
C108 . N101 . C111 . 110.7(6) yes
Eu1 . N102 . C102 . 111.6(4) yes
Eu1 . N102 . C103 . 110.6(4) yes
C102 . N102 . C103 . 108.8(6) yes
Eu1 . N102 . C114 . 103.9(7) yes
C102 . N102 . C114 . 111.1(6) yes
C103 . N102 . C114 . 110.7(5) yes
Eu1 . N103 . C104 . 110.3(5) yes
Eu1 . N103 . C105 . 108.2(5) yes
C104 . N103 . C105 . 110.2(6) yes
Eu1 . N103 . C117 . 103.3(8) yes
C104 . N103 . C117 . 111.9(6) yes
C105 . N103 . C117 . 112.7(6) yes
Eu1 . N104 . C106 . 110.9(5) yes
Eu1 . N104 . C107 . 110.1(4) yes
C106 . N104 . C107 . 108.9(6) yes
Eu1 . N104 . C121 . 109.9(7) yes
C106 . N104 . C121 . 108.6(6) yes
C107 . N104 . C121 . 108.4(6) yes
Eu1 . O101 . C112 . 129.1(6) yes
Eu1 . O102 . C115 . 125.9(5) yes
Eu1 . O103 . C118 . 126.6(6) yes
Eu1 . O109 . H1091 . 114.5 no
Eu1 . O109 . H1092 . 127.2 no
H1091 . O109 . H1092 . 110.8 no
N101 . C101 . C102 . 112.1(6) yes
N101 . C101 . H1011 . 109.7 no
C102 . C101 . H1011 . 110.5 no
N101 . C101 . H1012 . 109.4 no
C102 . C101 . H1012 . 105.4 no
H1011 . C101 . H1012 . 109.5 no
N102 . C102 . C101 . 112.2(6) yes
N102 . C102 . H1021 . 110.3 no
C101 . C102 . H1021 . 111.7 no
N102 . C102 . H1022 . 107.5 no
C101 . C102 . H1022 . 105.4 no
H1021 . C102 . H1022 . 109.5 no
N102 . C103 . C104 . 111.7(7) yes
N102 . C103 . H1031 . 109.3 no
C104 . C103 . H1031 . 110.3 no
N102 . C103 . H1032 . 110.9 no
C104 . C103 . H1032 . 105.0 no
H1031 . C103 . H1032 . 109.5 no
N103 . C104 . C103 . 112.0(6) yes
N103 . C104 . H1041 . 105.8 no
C103 . C104 . H1041 . 104.8 no
N103 . C104 . H1042 . 111.3 no
C103 . C104 . H1042 . 113.0 no
H1041 . C104 . H1042 . 109.5 no
N103 . C105 . C106 . 111.5(7) yes
N103 . C105 . H1051 . 109.5 no
C106 . C105 . H1051 . 105.8 no
N103 . C105 . H1052 . 110.3 no
C106 . C105 . H1052 . 110.2 no
H1051 . C105 . H1052 . 109.5 no
N104 . C106 . C105 . 111.2(7) yes
N104 . C106 . H1061 . 107.2 no
C105 . C106 . H1061 . 105.7 no
N104 . C106 . H1062 . 110.7 no
C105 . C106 . H1062 . 112.4 no
H1061 . C106 . H1062 . 109.5 no
N104 . C107 . C108 . 111.1(7) yes
N104 . C107 . H1071 . 109.9 no
C108 . C107 . H1071 . 106.3 no
N104 . C107 . H1072 . 110.2 no
C108 . C107 . H1072 . 109.9 no
H1071 . C107 . H1072 . 109.5 no
N101 . C108 . C107 . 111.0(6) yes
N101 . C108 . H1081 . 110.3 no
C107 . C108 . H1081 . 112.5 no
N101 . C108 . H1082 . 107.2 no
C107 . C108 . H1082 . 106.1 no
H1081 . C108 . H1082 . 109.5 no
N101 . C111 . C112 . 116.3(7) yes
N101 . C111 . H1111 . 107.8 no
C112 . C111 . H1111 . 108.2 no
N101 . C111 . H1112 . 108.8 no
C112 . C111 . H1112 . 106.1 no
H1111 . C111 . H1112 . 109.5 no
C111 . C112 . O101 . 112.76(7) yes
C111 . C112 . O113 . 121.99(7) yes
O101 . C112 . O113 . 125.25(7) yes
N102 . C114 . C115 . 117.6(7) yes
N102 . C114 . H1141 . 108.3 no
C115 . C114 . H1141 . 108.3 no
N102 . C114 . H1142 . 107.1 no
C115 . C114 . H1142 . 105.9 no
H1141 . C114 . H1142 . 109.5 no
C114 . C115 . O102 . 112.77(7) yes
C114 . C115 . O116 . 121.98(7) yes
O102 . C115 . O116 . 125.26(7) yes
C115 . O116 . Eu2 . 141.4(4) yes
N103 . C117 . C118 . 115.6(8) yes
N103 . C117 . H1171 . 109.6 no
C118 . C117 . H1171 . 108.7 no
N103 . C117 . H1172 . 106.5 no
C118 . C117 . H1172 . 106.8 no
H1171 . C117 . H1172 . 109.5 no
C117 . C118 . O103 . 112.76(7) yes
C117 . C118 . O119 . 121.99(7) yes
O103 . C118 . O119 . 125.25(7) yes
N104 . C121 . C122 . 121.7(8) yes
N104 . C121 . H1211 . 107.0 no
C122 . C121 . H1211 . 106.1 no
N104 . C121 . H1212 . 105.4 no
C122 . C121 . H1212 . 106.8 no
H1211 . C121 . H1212 . 109.5 no
C121 . C122 . C123 . 119.1(13) yes
C121 . C122 . C127 . 116.5(14) yes
C123 . C122 . C127 . 124.4(13) yes
C122 . C123 . C124 . 113.4(12) yes
C122 . C123 . H1231 . 123.6 no
C124 . C123 . H1231 . 123.0 no
C123 . C124 . O120 . 118.4(8) yes
C123 . C124 . O125 . 124.8(11) yes
O120 . C124 . O125 . 116.8(8) yes
C124 . O125 . C126 . 116.5(13) yes
O125 . C126 . C127 . 127.0(12) yes
O125 . C126 . C131 . 112.9(12) yes
C127 . C126 . C131 . 120.2(6) yes
C122 . C127 . C126 . 113.9(11) yes
C122 . C127 . C128 . 126.4(11) yes
C126 . C127 . C128 . 119.8(6) yes
C127 . C128 . C129 . 120.0(6) yes
C127 . C128 . H1281 . 120.1 no
C129 . C128 . H1281 . 119.9 no
C128 . C129 . C130 . 120.2(6) yes
C128 . C129 . H1291 . 120.0 no
C130 . C129 . H1291 . 119.8 no
C129 . C130 . C131 . 119.8(5) yes
C129 . C130 . O132 . 120.4(6) yes
C131 . C130 . O132 . 119.9(6) yes
C130 . C131 . C126 . 120.1(6) yes
C130 . C131 . H1311 . 120.1 no
C126 . C131 . H1311 . 119.8 no
C130 . O132 . C133 . 124.9(8) yes
O132 . C133 . H1331 . 110.3 no
O132 . C133 . H1332 . 109.5 no
H1331 . C133 . H1332 . 109.5 no
O132 . C133 . H1333 . 108.6 no
H1331 . C133 . H1333 . 109.5 no
H1332 . C133 . H1333 . 109.5 no
O116 . Eu2 . N201 . 140.7(3) yes
O116 . Eu2 . N202 . 73.9(3) yes
N201 . Eu2 . N202 . 67.6(2) yes
O116 . Eu2 . N203 . 67.9(3) yes
N201 . Eu2 . N203 . 103.7(3) yes
N202 . Eu2 . N203 . 68.2(2) yes
O116 . Eu2 . N204 . 132.9(3) yes
N201 . Eu2 . N204 . 67.0(2) yes
N202 . Eu2 . N204 . 104.1(3) yes
N203 . Eu2 . N204 . 68.05(19) yes
O116 . Eu2 . O201 . 140.0(3) yes
N201 . Eu2 . O201 . 61.4(4) yes
N202 . Eu2 . O201 . 120.5(3) yes
N203 . Eu2 . O201 . 150.8(3) yes
N204 . Eu2 . O201 . 82.8(3) yes
O116 . Eu2 . O202 . 75.0(3) yes
N201 . Eu2 . O202 . 80.2(3) yes
N202 . Eu2 . O202 . 62.5(4) yes
N203 . Eu2 . O202 . 124.4(3) yes
N204 . Eu2 . O202 . 147.1(3) yes
O116 . Eu2 . O203 . 77.2(3) yes
N201 . Eu2 . O203 . 135.5(3) yes
N202 . Eu2 . O203 . 130.1(4) yes
N203 . Eu2 . O203 . 63.6(4) yes
N204 . Eu2 . O203 . 68.8(3) yes
O116 . Eu2 . O209 . 73.1(4) yes
N201 . Eu2 . O209 . 127.4(4) yes
N202 . Eu2 . O209 . 129.7(5) yes
N203 . Eu2 . O209 . 128.7(4) yes
N204 . Eu2 . O209 . 126.1(4) yes
O201 . Eu2 . O202 . 80.0(4) yes
O201 . Eu2 . O203 . 107.8(4) yes
O202 . Eu2 . O203 . 143.4(3) yes
O201 . Eu2 . O209 . 69.9(4) yes
O202 . Eu2 . O209 . 72.9(5) yes
O203 . Eu2 . O209 . 76.6(5) yes
Eu2 . N201 . C201 . 109.9(5) yes
Eu2 . N201 . C208 . 110.1(4) yes
C201 . N201 . C208 . 110.5(6) yes
Eu2 . N201 . C211 . 102.3(6) yes
C201 . N201 . C211 . 112.2(6) yes
C208 . N201 . C211 . 111.5(5) yes
Eu2 . N202 . C202 . 110.1(4) yes
Eu2 . N202 . C203 . 110.6(5) yes
C202 . N202 . C203 . 111.1(6) yes
Eu2 . N202 . C214 . 99.9(6) yes
C202 . N202 . C214 . 112.5(5) yes
C203 . N202 . C214 . 112.1(6) yes
Eu2 . N203 . C204 . 107.4(5) yes
Eu2 . N203 . C205 . 107.6(5) yes
C204 . N203 . C205 . 109.9(6) yes
Eu2 . N203 . C217 . 109.0(7) yes
C204 . N203 . C217 . 111.6(5) yes
C205 . N203 . C217 . 111.1(6) yes
Eu2 . N204 . C206 . 109.0(4) yes
Eu2 . N204 . C207 . 112.7(4) yes
C206 . N204 . C207 . 109.5(6) yes
Eu2 . N204 . C221 . 103.5(7) yes
C206 . N204 . C221 . 111.1(6) yes
C207 . N204 . C221 . 110.9(6) yes
Eu2 . O201 . C212 . 120.8(5) yes
Eu2 . O202 . C215 . 116.5(5) yes
Eu2 . O203 . C218 . 126.0(5) yes
Eu2 . O209 . H2091 . 102.1 no
Eu2 . O209 . H2092 . 133.3 no
H2091 . O209 . H2092 . 118.7 no
N201 . C201 . C202 . 111.7(6) yes
N201 . C201 . H2011 . 106.8 no
C202 . C201 . H2011 . 105.7 no
N201 . C201 . H2012 . 110.8 no
C202 . C201 . H2012 . 112.1 no
H2011 . C201 . H2012 . 109.5 no
N202 . C202 . C201 . 112.3(7) yes
N202 . C202 . H2021 . 109.5 no
C201 . C202 . H2021 . 105.6 no
N202 . C202 . H2022 . 109.5 no
C201 . C202 . H2022 . 110.3 no
H2021 . C202 . H2022 . 109.5 no
N202 . C203 . C204 . 111.8(6) yes
N202 . C203 . H2031 . 106.2 no
C204 . C203 . H2031 . 105.2 no
N202 . C203 . H2032 . 111.3 no
C204 . C203 . H2032 . 112.5 no
H2031 . C203 . H2032 . 109.5 no
N203 . C204 . C203 . 111.5(6) yes
N203 . C204 . H2041 . 109.6 no
C203 . C204 . H2041 . 110.4 no
N203 . C204 . H2042 . 110.3 no
C203 . C204 . H2042 . 105.4 no
H2041 . C204 . H2042 . 109.5 no
N203 . C205 . C206 . 110.2(6) yes
N203 . C205 . H2051 . 111.1 no
C206 . C205 . H2051 . 112.3 no
N203 . C205 . H2052 . 107.3 no
C206 . C205 . H2052 . 106.2 no
H2051 . C205 . H2052 . 109.5 no
N204 . C206 . C205 . 109.6(6) yes
N204 . C206 . H2061 . 110.3 no
C205 . C206 . H2061 . 110.7 no
N204 . C206 . H2062 . 110.2 no
C205 . C206 . H2062 . 106.5 no
H2061 . C206 . H2062 . 109.5 no
N204 . C207 . C208 . 113.2(7) yes
N204 . C207 . H2071 . 110.4 no
C208 . C207 . H2071 . 111.6 no
N204 . C207 . H2072 . 106.4 no
C208 . C207 . H2072 . 105.4 no
H2071 . C207 . H2072 . 109.5 no
N201 . C208 . C207 . 113.7(7) yes
N201 . C208 . H2081 . 108.9 no
C207 . C208 . H2081 . 105.3 no
N201 . C208 . H2082 . 109.2 no
C207 . C208 . H2082 . 110.1 no
H2081 . C208 . H2082 . 109.5 no
N201 . C211 . C212 . 112.8(7) yes
N201 . C211 . H2111 . 110.3 no
C212 . C211 . H2111 . 109.4 no
N201 . C211 . H2112 . 106.9 no
C212 . C211 . H2112 . 107.9 no
H2111 . C211 . H2112 . 109.5 no
C211 . C212 . O201 . 112.77(7) yes
C211 . C212 . O213 . 121.98(7) yes
O201 . C212 . O213 . 125.25(7) yes
C212 . O213 . Eu3 . 136.5(5) yes
N202 . C214 . C215 . 114.4(7) yes
N202 . C214 . H2141 . 106.4 no
C215 . C214 . H2141 . 107.9 no
N202 . C214 . H2142 . 109.6 no
C215 . C214 . H2142 . 109.0 no
H2141 . C214 . H2142 . 109.5 no
C214 . C215 . O202 . 112.76(7) yes
C214 . C215 . O216 . 121.99(7) yes
O202 . C215 . O216 . 125.25(7) yes
N203 . C217 . C218 . 116.5(7) yes
N203 . C217 . H2171 . 106.7 no
C218 . C217 . H2171 . 106.9 no
N203 . C217 . H2172 . 109.1 no
C218 . C217 . H2172 . 108.1 no
H2171 . C217 . H2172 . 109.5 no
C217 . C218 . O203 . 112.76(7) yes
C217 . C218 . O219 . 121.99(7) yes
O203 . C218 . O219 . 125.25(7) yes
N204 . C221 . C222 . 119.5(8) yes
N204 . C221 . H2211 . 106.0 no
C222 . C221 . H2211 . 106.4 no
N204 . C221 . H2212 . 107.6 no
C222 . C221 . H2212 . 107.6 no
H2211 . C221 . H2212 . 109.5 no
C221 . C222 . C223 . 113.8(13) yes
C221 . C222 . C227 . 118.8(15) yes
C223 . C222 . C227 . 127.4(14) yes
C222 . C223 . C224 . 111.3(12) yes
C222 . C223 . H2231 . 124.5 no
C224 . C223 . H2231 . 124.2 no
C223 . C224 . O220 . 118.6(8) yes
C223 . C224 . O225 . 124.9(11) yes
O220 . C224 . O225 . 116.5(8) yes
C224 . O225 . C226 . 117.3(13) yes
O225 . C226 . C227 . 127.1(12) yes
O225 . C226 . C231 . 112.8(13) yes
C227 . C226 . C231 . 120.0(6) yes
C222 . C227 . C226 . 111.9(12) yes
C222 . C227 . C228 . 127.9(12) yes
C226 . C227 . C228 . 120.2(6) yes
C227 . C228 . C229 . 119.8(6) yes
C227 . C228 . H2281 . 120.3 no
C229 . C228 . H2281 . 119.9 no
C228 . C229 . C230 . 119.9(6) yes
C228 . C229 . H2291 . 120.2 no
C230 . C229 . H2291 . 119.9 no
C229 . C230 . C231 . 120.1(5) yes
C229 . C230 . O232 . 120.0(6) yes
C231 . C230 . O232 . 119.9(6) yes
C226 . C231 . C230 . 120.0(6) yes
C226 . C231 . H2311 . 119.9 no
C230 . C231 . H2311 . 120.2 no
C230 . O232 . C233 . 123.8(8) yes
O232 . C233 . H2331 . 109.9 no
O232 . C233 . H2332 . 108.7 no
H2331 . C233 . H2332 . 109.5 no
O232 . C233 . H2333 . 109.8 no
H2331 . C233 . H2333 . 109.5 no
H2332 . C233 . H2333 . 109.5 no
O213 . Eu3 . N301 . 138.7(4) yes
O213 . Eu3 . N302 . 137.8(3) yes
N301 . Eu3 . N302 . 67.3(2) yes
O213 . Eu3 . N303 . 73.2(3) yes
N301 . Eu3 . N303 . 103.6(3) yes
N302 . Eu3 . N303 . 67.3(2) yes
O213 . Eu3 . N304 . 74.1(3) yes
N301 . Eu3 . N304 . 67.2(2) yes
N302 . Eu3 . N304 . 102.9(3) yes
N303 . Eu3 . N304 . 67.5(2) yes
O213 . Eu3 . O301 . 90.5(4) yes
N301 . Eu3 . O301 . 65.5(4) yes
N302 . Eu3 . O301 . 129.9(4) yes
N303 . Eu3 . O301 . 140.4(3) yes
N304 . Eu3 . O301 . 73.4(3) yes
O213 . Eu3 . O302 . 144.7(3) yes
N301 . Eu3 . O302 . 69.3(3) yes
N302 . Eu3 . O302 . 63.7(4) yes
N303 . Eu3 . O302 . 129.1(3) yes
N304 . Eu3 . O302 . 136.2(3) yes
O213 . Eu3 . O303 . 79.8(4) yes
N301 . Eu3 . O303 . 137.1(3) yes
N302 . Eu3 . O303 . 70.3(3) yes
N303 . Eu3 . O303 . 64.0(4) yes
N304 . Eu3 . O303 . 129.7(4) yes
O213 . Eu3 . O309 . 75.6(5) yes
N301 . Eu3 . O309 . 121.9(5) yes
N302 . Eu3 . O309 . 124.0(5) yes
N303 . Eu3 . O309 . 134.3(5) yes
N304 . Eu3 . O309 . 132.5(5) yes
O301 . Eu3 . O302 . 84.5(4) yes
O301 . Eu3 . O303 . 149.4(4) yes
O302 . Eu3 . O303 . 87.1(4) yes
O301 . Eu3 . O309 . 71.3(6) yes
O302 . Eu3 . O309 . 69.7(5) yes
O303 . Eu3 . O309 . 78.3(6) yes
Eu3 . N301 . C301 . 109.4(5) yes
Eu3 . N301 . C308 . 110.9(5) yes
C301 . N301 . C308 . 109.2(6) yes
Eu3 . N301 . C311 . 105.1(8) yes
C301 . N301 . C311 . 111.2(5) yes
C308 . N301 . C311 . 111.0(6) yes
Eu3 . N302 . C302 . 110.7(5) yes
Eu3 . N302 . C303 . 110.1(4) yes
C302 . N302 . C303 . 109.0(6) yes
Eu3 . N302 . C314 . 105.0(7) yes
C302 . N302 . C314 . 111.1(6) yes
C303 . N302 . C314 . 110.8(5) yes
Eu3 . N303 . C304 . 110.5(5) yes
Eu3 . N303 . C305 . 108.9(5) yes
C304 . N303 . C305 . 108.7(6) yes
Eu3 . N303 . C317 . 106.1(7) yes
C304 . N303 . C317 . 111.3(6) yes
C305 . N303 . C317 . 111.4(6) yes
Eu3 . N304 . C306 . 109.0(5) yes
Eu3 . N304 . C307 . 109.7(5) yes
C306 . N304 . C307 . 107.9(6) yes
Eu3 . N304 . C321 . 116.2(8) yes
C306 . N304 . C321 . 106.9(6) yes
C307 . N304 . C321 . 106.9(6) yes
Eu3 . O301 . C312 . 127.2(6) yes
Eu3 . O302 . C315 . 126.7(5) yes
Eu3 . O303 . C318 . 122.1(5) yes
Eu3 . O309 . H3091 . 129.4 no
Eu3 . O309 . H3092 . 116.7 no
H3091 . O309 . H3092 . 101.6 no
N301 . C301 . C302 . 111.4(7) yes
N301 . C301 . H3011 . 110.1 no
C302 . C301 . H3011 . 110.5 no
N301 . C301 . H3012 . 110.0 no
C302 . C301 . H3012 . 105.3 no
H3011 . C301 . H3012 . 109.5 no
N302 . C302 . C301 . 111.5(7) yes
N302 . C302 . H3021 . 106.6 no
C301 . C302 . H3021 . 105.1 no
N302 . C302 . H3022 . 111.2 no
C301 . C302 . H3022 . 112.7 no
H3021 . C302 . H3022 . 109.5 no
N302 . C303 . C304 . 111.6(7) yes
N302 . C303 . H3031 . 109.9 no
C304 . C303 . H3031 . 110.4 no
N302 . C303 . H3032 . 109.7 no
C304 . C303 . H3032 . 105.6 no
H3031 . C303 . H3032 . 109.5 no
N303 . C304 . C303 . 112.1(7) yes
N303 . C304 . H3041 . 106.9 no
C303 . C304 . H3041 . 105.4 no
N303 . C304 . H3042 . 110.5 no
C303 . C304 . H3042 . 112.2 no
H3041 . C304 . H3042 . 109.5 no
N303 . C305 . C306 . 110.4(7) yes
N303 . C305 . H3051 . 110.1 no
C306 . C305 . H3051 . 110.3 no
N303 . C305 . H3052 . 110.2 no
C306 . C305 . H3052 . 106.3 no
H3051 . C305 . H3052 . 109.5 no
N304 . C306 . C305 . 110.1(7) yes
N304 . C306 . H3061 . 110.9 no
C305 . C306 . H3061 . 112.4 no
N304 . C306 . H3062 . 107.6 no
C305 . C306 . H3062 . 106.1 no
H3061 . C306 . H3062 . 109.5 no
N304 . C307 . C308 . 111.5(7) yes
N304 . C307 . H3071 . 109.7 no
C308 . C307 . H3071 . 109.9 no
N304 . C307 . H3072 . 109.9 no
C308 . C307 . H3072 . 106.2 no
H3071 . C307 . H3072 . 109.5 no
N301 . C308 . C307 . 111.7(7) yes
N301 . C308 . H3081 . 110.3 no
C307 . C308 . H3081 . 112.1 no
N301 . C308 . H3082 . 107.0 no
C307 . C308 . H3082 . 106.0 no
H3081 . C308 . H3082 . 109.5 no
N301 . C311 . C312 . 112.9(7) yes
N301 . C311 . H3111 . 108.9 no
C312 . C311 . H3111 . 109.0 no
N301 . C311 . H3112 . 109.3 no
C312 . C311 . H3112 . 107.3 no
H3111 . C311 . H3112 . 109.5 no
C311 . C312 . O301 . 112.76(7) yes
C311 . C312 . O313 . 121.99(7) yes
O301 . C312 . O313 . 125.25(7) yes
N302 . C314 . C315 . 116.5(7) yes
N302 . C314 . H3141 . 107.1 no
C315 . C314 . H3141 . 108.0 no
N302 . C314 . H3142 . 109.0 no
C315 . C314 . H3142 . 106.8 no
H3141 . C314 . H3142 . 109.5 no
C314 . C315 . O302 . 112.77(7) yes
C314 . C315 . O316 . 121.98(7) yes
O302 . C315 . O316 . 125.25(7) yes
C315 . O316 . Eu4 . 142.7(5) yes
N303 . C317 . C318 . 117.5(8) yes
N303 . C317 . H3171 . 108.4 no
C318 . C317 . H3171 . 106.6 no
N303 . C317 . H3172 . 107.2 no
C318 . C317 . H3172 . 107.4 no
H3171 . C317 . H3172 . 109.5 no
C317 . C318 . O303 . 112.76(7) yes
C317 . C318 . O319 . 121.99(7) yes
O303 . C318 . O319 . 125.25(7) yes
N304 . C321 . C322 . 126.6(8) yes
N304 . C321 . H3211 . 104.6 no
C322 . C321 . H3211 . 104.6 no
N304 . C321 . H3212 . 105.1 no
C322 . C321 . H3212 . 105.8 no
H3211 . C321 . H3212 . 109.5 no
C321 . C322 . C323 . 106.6(13) yes
C321 . C322 . C327 . 130.9(18) yes
C323 . C322 . C327 . 122.4(15) yes
C322 . C323 . C324 . 114.5(13) yes
C322 . C323 . H3231 . 122.8 no
C324 . C323 . H3231 . 122.7 no
C323 . C324 . O320 . 118.7(9) yes
C323 . C324 . O325 . 125.1(12) yes
O320 . C324 . O325 . 116.1(9) yes
C324 . O325 . C326 . 115.7(14) yes
O325 . C326 . C327 . 127.4(14) yes
O325 . C326 . C331 . 112.3(14) yes
C327 . C326 . C331 . 120.3(6) yes
C322 . C327 . C326 . 114.9(13) yes
C322 . C327 . C328 . 125.5(14) yes
C326 . C327 . C328 . 119.5(6) yes
C327 . C328 . C329 . 120.2(6) yes
C327 . C328 . H3281 . 119.8 no
C329 . C328 . H3281 . 120.0 no
C328 . C329 . C330 . 120.1(6) yes
C328 . C329 . H3291 . 119.8 no
C330 . C329 . H3291 . 120.1 no
C329 . C330 . C331 . 119.9(5) yes
C329 . C330 . O332 . 120.2(6) yes
C331 . C330 . O332 . 119.9(6) yes
C330 . C331 . C326 . 120.0(6) yes
C330 . C331 . H3311 . 119.9 no
C326 . C331 . H3311 . 120.1 no
C330 . O332 . C333 . 124.1(8) yes
O332 . C333 . H3331 . 110.1 no
O332 . C333 . H3332 . 109.2 no
H3331 . C333 . H3332 . 109.5 no
O332 . C333 . H3333 . 109.1 no
H3331 . C333 . H3333 . 109.5 no
H3332 . C333 . H3333 . 109.5 no
O316 . Eu4 . N401 . 142.0(3) yes
O316 . Eu4 . N402 . 76.1(3) yes
N401 . Eu4 . N402 . 67.4(2) yes
O316 . Eu4 . N403 . 71.2(3) yes
N401 . Eu4 . N403 . 103.1(3) yes
N402 . Eu4 . N403 . 68.0(2) yes
O316 . Eu4 . N404 . 135.1(3) yes
N401 . Eu4 . N404 . 67.0(2) yes
N402 . Eu4 . N404 . 104.2(3) yes
N403 . Eu4 . N404 . 67.9(2) yes
O316 . Eu4 . O401 . 141.4(4) yes
N401 . Eu4 . O401 . 54.9(4) yes
N402 . Eu4 . O401 . 114.6(4) yes
N403 . Eu4 . O401 . 147.4(3) yes
N404 . Eu4 . O401 . 80.5(3) yes
O316 . Eu4 . O402 . 79.3(3) yes
N401 . Eu4 . O402 . 72.9(3) yes
N402 . Eu4 . O402 . 58.1(4) yes
N403 . Eu4 . O402 . 123.1(4) yes
N404 . Eu4 . O402 . 139.9(3) yes
O316 . Eu4 . O403 . 73.2(3) yes
N401 . Eu4 . O403 . 141.1(3) yes
N402 . Eu4 . O403 . 132.1(4) yes
N403 . Eu4 . O403 . 67.8(4) yes
N404 . Eu4 . O403 . 74.9(3) yes
O316 . Eu4 . O409 . 72.2(6) yes
N401 . Eu4 . O409 . 125.5(6) yes
N402 . Eu4 . O409 . 130.6(6) yes
N403 . Eu4 . O409 . 131.3(6) yes
N404 . Eu4 . O409 . 125.0(5) yes
O401 . Eu4 . O402 . 76.9(4) yes
O401 . Eu4 . O403 . 112.4(4) yes
O402 . Eu4 . O403 . 144.7(3) yes
O401 . Eu4 . O409 . 73.8(6) yes
O402 . Eu4 . O409 . 79.3(6) yes
O403 . Eu4 . O409 . 71.6(7) yes
Eu4 . N401 . C401 . 108.4(5) yes
Eu4 . N401 . C408 . 109.5(5) yes
C401 . N401 . C408 . 108.5(6) yes
Eu4 . N401 . C411 . 111.4(7) yes
C401 . N401 . C411 . 109.3(6) yes
C408 . N401 . C411 . 109.7(5) yes
Eu4 . N402 . C402 . 110.6(4) yes
Eu4 . N402 . C403 . 110.9(5) yes
C402 . N402 . C403 . 108.8(6) yes
Eu4 . N402 . C414 . 104.0(7) yes
C402 . N402 . C414 . 110.5(5) yes
C403 . N402 . C414 . 112.0(6) yes
Eu4 . N403 . C404 . 108.7(5) yes
Eu4 . N403 . C405 . 109.8(5) yes
C404 . N403 . C405 . 111.2(6) yes
Eu4 . N403 . C417 . 102.5(8) yes
C404 . N403 . C417 . 112.0(6) yes
C405 . N403 . C417 . 112.3(6) yes
Eu4 . N404 . C406 . 109.4(5) yes
Eu4 . N404 . C407 . 113.1(5) yes
C406 . N404 . C407 . 110.9(6) yes
Eu4 . N404 . C421 . 100.4(7) yes
C406 . N404 . C421 . 111.1(6) yes
C407 . N404 . C421 . 111.5(6) yes
Eu4 . O401 . C412 . 128.5(6) yes
Eu4 . O402 . C415 . 120.0(5) yes
Eu4 . O403 . C418 . 122.5(6) yes
Eu4 . O409 . H4091 . 136.4 no
Eu4 . O409 . H4092 . 101.5 no
H4091 . O409 . H4092 . 119.8 no
N401 . C401 . C402 . 110.5(6) yes
N401 . C401 . H4011 . 106.5 no
C402 . C401 . H4011 . 105.5 no
N401 . C401 . H4012 . 110.8 no
C402 . C401 . H4012 . 113.7 no
H4011 . C401 . H4012 . 109.5 no
N402 . C402 . C401 . 110.3(7) yes
N402 . C402 . H4021 . 111.1 no
C401 . C402 . H4021 . 106.1 no
N402 . C402 . H4022 . 110.1 no
C401 . C402 . H4022 . 109.6 no
H4021 . C402 . H4022 . 109.5 no
N402 . C403 . C404 . 113.1(7) yes
N402 . C403 . H4031 . 110.3 no
C404 . C403 . H4031 . 112.2 no
N402 . C403 . H4032 . 107.0 no
C404 . C403 . H4032 . 104.3 no
H4031 . C403 . H4032 . 109.5 no
N403 . C404 . C403 . 113.2(7) yes
N403 . C404 . H4041 . 108.7 no
C403 . C404 . H4041 . 104.4 no
N403 . C404 . H4042 . 110.2 no
C403 . C404 . H4042 . 110.6 no
H4041 . C404 . H4042 . 109.5 no
N403 . C405 . C406 . 112.0(6) yes
N403 . C405 . H4051 . 110.9 no
C406 . C405 . H4051 . 113.2 no
N403 . C405 . H4052 . 105.8 no
C406 . C405 . H4052 . 105.1 no
H4051 . C405 . H4052 . 109.5 no
N404 . C406 . C405 . 111.5(7) yes
N404 . C406 . H4061 . 111.0 no
C405 . C406 . H4061 . 105.5 no
N404 . C406 . H4062 . 109.6 no
C405 . C406 . H4062 . 109.6 no
H4061 . C406 . H4062 . 109.5 no
N404 . C407 . C408 . 114.1(7) yes
N404 . C407 . H4071 . 110.2 no
C408 . C407 . H4071 . 111.8 no
N404 . C407 . H4072 . 107.0 no
C408 . C407 . H4072 . 103.9 no
H4071 . C407 . H4072 . 109.5 no
N401 . C408 . C407 . 113.5(7) yes
N401 . C408 . H4081 . 108.4 no
C407 . C408 . H4081 . 104.0 no
N401 . C408 . H4082 . 110.0 no
C407 . C408 . H4082 . 111.2 no
H4081 . C408 . H4082 . 109.5 no
N401 . C411 . C412 . 102.5(7) yes
N401 . C411 . H4111 . 109.3 no
C412 . C411 . H4111 . 109.9 no
N401 . C411 . H4112 . 112.8 no
C412 . C411 . H4112 . 112.6 no
H4111 . C411 . H4112 . 109.5 no
C411 . C412 . O401 . 112.76(7) yes
C411 . C412 . O413 . 121.98(7) yes
O401 . C412 . O413 . 125.25(7) yes
C412 . O413 . Eu1 . 138.5(6) yes
N402 . C414 . C415 . 107.1(7) yes
N402 . C414 . H4141 . 110.5 no
C415 . C414 . H4141 . 108.0 no
N402 . C414 . H4142 . 110.1 no
C415 . C414 . H4142 . 111.6 no
H4141 . C414 . H4142 . 109.5 no
C414 . C415 . O402 . 112.76(7) yes
C414 . C415 . O416 . 121.99(7) yes
O402 . C415 . O416 . 125.25(7) yes
N403 . C417 . C418 . 123.8(9) yes
N403 . C417 . H4171 . 107.6 no
C418 . C417 . H4171 . 105.7 no
N403 . C417 . H4172 . 104.6 no
C418 . C417 . H4172 . 105.3 no
H4171 . C417 . H4172 . 109.5 no
C417 . C418 . O403 . 112.76(7) yes
C417 . C418 . O419 . 121.98(7) yes
O403 . C418 . O419 . 125.25(7) yes
N404 . C421 . C422 . 111.8(8) yes
N404 . C421 . H4211 . 109.0 no
C422 . C421 . H4211 . 107.3 no
N404 . C421 . H4212 . 108.8 no
C422 . C421 . H4212 . 110.5 no
H4211 . C421 . H4212 . 109.5 no
C421 . C422 . C423 . 123.5(14) yes
C421 . C422 . C427 . 114.0(15) yes
C423 . C422 . C427 . 122.5(13) yes
C422 . C423 . C424 . 115.2(12) yes
C422 . C423 . H4231 . 123.0 no
C424 . C423 . H4231 . 121.8 no
C423 . C424 . O420 . 119.3(9) yes
C423 . C424 . O425 . 122.7(11) yes
O420 . C424 . O425 . 117.9(8) yes
C424 . O425 . C426 . 119.2(14) yes
O425 . C426 . C427 . 124.3(12) yes
O425 . C426 . C431 . 115.9(13) yes
C427 . C426 . C431 . 119.8(6) yes
C422 . C427 . C426 . 115.9(12) yes
C422 . C427 . C428 . 123.8(12) yes
C426 . C427 . C428 . 120.2(6) yes
C427 . C428 . C429 . 119.9(6) yes
C427 . C428 . H4281 . 120.3 no
C429 . C428 . H4281 . 119.8 no
C428 . C429 . C430 . 120.1(6) yes
C428 . C429 . H4291 . 120.2 no
C430 . C429 . H4291 . 119.7 no
C429 . C430 . C431 . 120.0(5) yes
C429 . C430 . O432 . 120.1(6) yes
C431 . C430 . O432 . 120.0(6) yes
C426 . C431 . C430 . 120.1(6) yes
C426 . C431 . H4311 . 119.7 no
C430 . C431 . H4311 . 120.2 no
C430 . O432 . C433 . 124.5(8) yes
O432 . C433 . H4331 . 110.0 no
O432 . C433 . H4333 . 109.1 no
H4331 . C433 . H4333 . 109.5 no
O432 . C433 . H4334 . 109.3 no
H4331 . C433 . H4334 . 109.5 no
H4333 . C433 . H4334 . 109.5 no
N501 . Eu5 . N502 . 67.6(2) yes
N501 . Eu5 . N503 . 104.0(4) yes
N502 . Eu5 . N503 . 67.8(2) yes
N501 . Eu5 . N504 . 67.4(2) yes
N502 . Eu5 . N504 . 103.5(4) yes
N503 . Eu5 . N504 . 67.6(2) yes
N501 . Eu5 . O501 . 66.1(6) yes
N502 . Eu5 . O501 . 130.2(5) yes
N503 . Eu5 . O501 . 141.6(3) yes
N504 . Eu5 . O501 . 74.6(4) yes
N501 . Eu5 . O502 . 81.1(3) yes
N502 . Eu5 . O502 . 66.9(6) yes
N503 . Eu5 . O502 . 127.9(5) yes
N504 . Eu5 . O502 . 148.1(3) yes
O501 . Eu5 . O502 . 88.6(5) yes
N501 . Eu5 . O503 . 138.4(3) yes
N502 . Eu5 . O503 . 71.9(3) yes
N503 . Eu5 . O503 . 67.9(6) yes
N504 . Eu5 . O503 . 133.2(6) yes
O501 . Eu5 . O503 . 144.3(5) yes
N501 . Eu5 . O509 . 135.5(7) yes
N502 . Eu5 . O509 . 119.5(7) yes
N503 . Eu5 . O509 . 119.5(7) yes
N504 . Eu5 . O509 . 136.2(7) yes
O501 . Eu5 . O509 . 83.5(7) yes
N501 . Eu5 . O813 . 139.6(4) yes
N502 . Eu5 . O813 . 131.0(4) yes
N503 . Eu5 . O813 . 66.0(4) yes
N504 . Eu5 . O813 . 73.0(4) yes
O501 . Eu5 . O813 . 96.8(5) yes
O502 . Eu5 . O503 . 74.7(5) yes
O502 . Eu5 . O509 . 65.8(7) yes
O503 . Eu5 . O509 . 60.9(7) yes
O502 . Eu5 . O813 . 137.1(4) yes
O503 . Eu5 . O813 . 76.5(5) yes
O509 . Eu5 . O813 . 72.5(7) yes
Eu5 . N501 . C501 . 108.3(5) yes
Eu5 . N501 . C508 . 109.7(6) yes
C501 . N501 . C508 . 109.5(6) yes
Eu5 . N501 . C511 . 105.7(11) yes
C501 . N501 . C511 . 112.0(6) yes
C508 . N501 . C511 . 111.4(6) yes
Eu5 . N502 . C502 . 110.4(5) yes
Eu5 . N502 . C503 . 109.4(5) yes
C502 . N502 . C503 . 110.3(6) yes
Eu5 . N502 . C514 . 105.2(10) yes
C502 . N502 . C514 . 110.5(6) yes
C503 . N502 . C514 . 110.9(6) yes
Eu5 . N503 . C504 . 110.7(5) yes
Eu5 . N503 . C505 . 109.1(5) yes
C504 . N503 . C505 . 111.1(7) yes
Eu5 . N503 . C517 . 100.3(11) yes
C504 . N503 . C517 . 112.5(7) yes
C505 . N503 . C517 . 112.5(6) yes
Eu5 . N504 . C506 . 111.1(5) yes
Eu5 . N504 . C507 . 110.4(5) yes
C506 . N504 . C507 . 109.6(6) yes
Eu5 . N504 . C521 . 107.3(8) yes
C506 . N504 . C521 . 109.5(6) yes
C507 . N504 . C521 . 109.0(6) yes
Eu5 . O501 . C512 . 128.6(8) yes
Eu5 . O502 . C515 . 128.4(8) yes
Eu5 . O503 . C518 . 124.4(8) yes
Eu5 . O509 . H5091 . 116.4 no
Eu5 . O509 . H5092 . 139.7 no
H5091 . O509 . H5092 . 103.8 no
N501 . C501 . C502 . 111.0(7) yes
N501 . C501 . H5011 . 110.4 no
C502 . C501 . H5011 . 105.8 no
N501 . C501 . H5012 . 109.9 no
C502 . C501 . H5012 . 110.2 no
H5011 . C501 . H5012 . 109.5 no
N502 . C502 . C501 . 111.2(7) yes
N502 . C502 . H5021 . 111.1 no
C501 . C502 . H5021 . 112.8 no
N502 . C502 . H5022 . 106.4 no
C501 . C502 . H5022 . 105.5 no
H5021 . C502 . H5022 . 109.5 no
N502 . C503 . C504 . 112.9(7) yes
N502 . C503 . H5031 . 109.2 no
C504 . C503 . H5031 . 105.4 no
N502 . C503 . H5032 . 109.6 no
C504 . C503 . H5032 . 110.1 no
H5031 . C503 . H5032 . 109.5 no
N503 . C504 . C503 . 112.7(7) yes
N503 . C504 . H5041 . 110.3 no
C503 . C504 . H5041 . 112.0 no
N503 . C504 . H5043 . 106.6 no
C503 . C504 . H5043 . 105.4 no
H5041 . C504 . H5043 . 109.5 no
N503 . C505 . C506 . 113.3(7) yes
N503 . C505 . H5051 . 109.6 no
C506 . C505 . H5051 . 105.0 no
N503 . C505 . H5052 . 109.2 no
C506 . C505 . H5052 . 110.2 no
H5051 . C505 . H5052 . 109.5 no
N504 . C506 . C505 . 112.7(7) yes
N504 . C506 . H5061 . 106.6 no
C505 . C506 . H5061 . 105.0 no
N504 . C506 . H5062 . 110.5 no
C505 . C506 . H5062 . 112.2 no
H5061 . C506 . H5062 . 109.5 no
N504 . C507 . C508 . 111.4(7) yes
N504 . C507 . H5071 . 109.8 no
C508 . C507 . H5071 . 106.1 no
N504 . C507 . H5072 . 109.6 no
C508 . C507 . H5072 . 110.4 no
H5071 . C507 . H5072 . 109.5 no
N501 . C508 . C507 . 111.6(7) yes
N501 . C508 . H5081 . 107.1 no
C507 . C508 . H5081 . 105.9 no
N501 . C508 . H5082 . 110.5 no
C507 . C508 . H5082 . 111.9 no
H5081 . C508 . H5082 . 109.5 no
N501 . C511 . C512 . 118.6(10) yes
N501 . C511 . H5112 . 108.0 no
C512 . C511 . H5112 . 106.3 no
N501 . C511 . H5113 . 107.1 no
C512 . C511 . H5113 . 107.3 no
H5112 . C511 . H5113 . 109.5 no
C511 . C512 . O501 . 112.76(7) yes
C511 . C512 . O513 . 121.99(7) yes
O501 . C512 . O513 . 125.25(7) yes
N502 . C514 . C515 . 120.4(10) yes
N502 . C514 . H5141 . 108.2 no
C515 . C514 . H5141 . 108.4 no
N502 . C514 . H5142 . 105.3 no
C515 . C514 . H5142 . 104.7 no
H5141 . C514 . H5142 . 109.5 no
C514 . C515 . O502 . 112.76(7) yes
C514 . C515 . O516 . 121.99(7) yes
O502 . C515 . O516 . 125.25(7) yes
C515 . O516 . Eu6 . 144.9(7) yes
N503 . C517 . C518 . 119.5(10) yes
N503 . C517 . H5171 . 106.7 no
C518 . C517 . H5171 . 106.3 no
N503 . C517 . H5172 . 107.7 no
C518 . C517 . H5172 . 106.9 no
H5171 . C517 . H5172 . 109.5 no
C517 . C518 . O503 . 112.76(7) yes
C517 . C518 . O519 . 121.99(7) yes
O503 . C518 . O519 . 125.25(7) yes
N504 . C521 . C522 . 119.4(9) yes
N504 . C521 . H5211 . 105.6 no
C522 . C521 . H5211 . 107.7 no
N504 . C521 . H5212 . 107.7 no
C522 . C521 . H5212 . 106.8 no
H5211 . C521 . H5212 . 109.5 no
C521 . C522 . C523 . 122.2(14) yes
C521 . C522 . C527 . 116.6(17) yes
C523 . C522 . C527 . 121.2(15) yes
C522 . C523 . C524 . 116.0(13) yes
C522 . C523 . H5231 . 122.4 no
C524 . C523 . H5231 . 121.6 no
C523 . C524 . O520 . 119.6(9) yes
C523 . C524 . O525 . 123.0(12) yes
O520 . C524 . O525 . 117.4(9) yes
C524 . O525 . C526 . 118.3(14) yes
O525 . C526 . C527 . 124.8(13) yes
O525 . C526 . C531 . 115.3(13) yes
C527 . C526 . C531 . 119.9(6) yes
C522 . C527 . C526 . 116.7(13) yes
C522 . C527 . C528 . 123.2(13) yes
C526 . C527 . C528 . 120.1(6) yes
C527 . C528 . C529 . 120.0(6) yes
C527 . C528 . H5282 . 120.1 no
C529 . C528 . H5282 . 119.9 no
C528 . C529 . C530 . 119.9(6) yes
C528 . C529 . H5291 . 120.2 no
C530 . C529 . H5291 . 119.9 no
C529 . C530 . C531 . 120.2(5) yes
C529 . C530 . O532 . 119.9(6) yes
C531 . C530 . O532 . 119.9(6) yes
C526 . C531 . C530 . 120.0(6) yes
C526 . C531 . H5311 . 119.9 no
C530 . C531 . H5311 . 120.1 no
C530 . O532 . C533 . 124.2(8) yes
O532 . C533 . H5332 . 110.5 no
O532 . C533 . H5333 . 108.9 no
H5332 . C533 . H5333 . 109.5 no
O532 . C533 . H5334 . 109.0 no
H5332 . C533 . H5334 . 109.5 no
H5333 . C533 . H5334 . 109.5 no
O516 . Eu6 . N601 . 144.0(3) yes
O516 . Eu6 . N602 . 77.4(4) yes
N601 . Eu6 . N602 . 67.7(2) yes
O516 . Eu6 . N603 . 67.4(5) yes
N601 . Eu6 . N603 . 105.2(4) yes
N602 . Eu6 . N603 . 67.8(2) yes
O516 . Eu6 . N604 . 131.1(4) yes
N601 . Eu6 . N604 . 67.7(2) yes
N602 . Eu6 . N604 . 102.9(4) yes
N603 . Eu6 . N604 . 68.0(2) yes
O516 . Eu6 . O601 . 128.9(5) yes
N601 . Eu6 . O601 . 68.0(7) yes
N602 . Eu6 . O601 . 121.9(6) yes
N603 . Eu6 . O601 . 160.8(3) yes
N604 . Eu6 . O601 . 93.1(3) yes
O516 . Eu6 . O602 . 62.6(4) yes
N601 . Eu6 . O602 . 99.0(4) yes
N602 . Eu6 . O602 . 74.9(6) yes
N603 . Eu6 . O602 . 122.3(5) yes
N604 . Eu6 . O602 . 165.8(4) yes
O516 . Eu6 . O603 . 75.7(4) yes
N601 . Eu6 . O603 . 133.7(3) yes
N602 . Eu6 . O603 . 128.5(6) yes
N603 . Eu6 . O603 . 61.6(6) yes
N604 . Eu6 . O603 . 66.4(3) yes
O516 . Eu6 . O609 . 76.3(8) yes
N601 . Eu6 . O609 . 127.4(8) yes
N602 . Eu6 . O609 . 140.8(8) yes
N603 . Eu6 . O609 . 125.4(9) yes
N604 . Eu6 . O609 . 116.2(8) yes
O601 . Eu6 . O602 . 76.9(5) yes
O601 . Eu6 . O603 . 109.2(6) yes
O602 . Eu6 . O603 . 126.1(3) yes
O601 . Eu6 . O609 . 59.4(9) yes
O602 . Eu6 . O609 . 67.3(9) yes
O603 . Eu6 . O609 . 71.1(9) yes
Eu6 . N601 . C601 . 111.7(5) yes
Eu6 . N601 . C608 . 109.7(5) yes
C601 . N601 . C608 . 110.6(6) yes
Eu6 . N601 . C611 . 98.5(12) yes
C601 . N601 . C611 . 113.3(7) yes
C608 . N601 . C611 . 112.4(6) yes
Eu6 . N602 . C602 . 110.4(5) yes
Eu6 . N602 . C603 . 111.9(5) yes
C602 . N602 . C603 . 113.7(6) yes
Eu6 . N602 . C614 . 89.3(12) yes
C602 . N602 . C614 . 114.4(6) yes
C603 . N602 . C614 . 114.7(7) yes
Eu6 . N603 . C604 . 108.2(5) yes
Eu6 . N603 . C605 . 108.9(6) yes
C604 . N603 . C605 . 109.9(6) yes
Eu6 . N603 . C617 . 109.4(11) yes
C604 . N603 . C617 . 110.3(6) yes
C605 . N603 . C617 . 110.1(6) yes
Eu6 . N604 . C606 . 109.1(5) yes
Eu6 . N604 . C607 . 110.1(6) yes
C606 . N604 . C607 . 109.4(6) yes
Eu6 . N604 . C621 . 109.8(10) yes
C606 . N604 . C621 . 109.4(6) yes
C607 . N604 . C621 . 109.1(6) yes
Eu6 . O601 . C612 . 123.3(9) yes
Eu6 . O602 . C615 . 116.3(9) yes
Eu6 . O603 . C618 . 131.5(8) yes
Eu6 . O609 . H6091 . 141.8 no
Eu6 . O609 . H6092 . 130.4 no
H6091 . O609 . H6092 . 83.1 no
N601 . C601 . C602 . 114.5(7) yes
N601 . C601 . H6011 . 110.4 no
C602 . C601 . H6011 . 111.7 no
N601 . C601 . H6012 . 106.0 no
C602 . C601 . H6012 . 104.4 no
H6011 . C601 . H6012 . 109.5 no
N602 . C602 . C601 . 115.0(7) yes
N602 . C602 . H6021 . 109.5 no
C601 . C602 . H6021 . 110.4 no
N602 . C602 . H6023 . 107.9 no
C601 . C602 . H6023 . 104.3 no
H6021 . C602 . H6023 . 109.5 no
N602 . C603 . C604 . 113.8(7) yes
N602 . C603 . H6031 . 104.6 no
C604 . C603 . H6031 . 105.1 no
N602 . C603 . H6032 . 111.0 no
C604 . C603 . H6032 . 112.2 no
H6031 . C603 . H6032 . 109.5 no
N603 . C604 . C603 . 113.1(7) yes
N603 . C604 . H6041 . 109.0 no
C603 . C604 . H6041 . 109.7 no
N603 . C604 . H6042 . 110.0 no
C603 . C604 . H6042 . 105.5 no
H6041 . C604 . H6042 . 109.5 no
N603 . C605 . C606 . 111.0(7) yes
N603 . C605 . H6051 . 106.7 no
C606 . C605 . H6051 . 105.4 no
N603 . C605 . H6052 . 111.7 no
C606 . C605 . H6052 . 112.3 no
H6051 . C605 . H6052 . 109.5 no
N604 . C606 . C605 . 111.1(7) yes
N604 . C606 . H6061 . 109.4 no
C605 . C606 . H6061 . 110.9 no
N604 . C606 . H6062 . 110.4 no
C605 . C606 . H6062 . 105.5 no
H6061 . C606 . H6062 . 109.5 no
N604 . C607 . C608 . 112.0(7) yes
N604 . C607 . H6072 . 110.8 no
C608 . C607 . H6072 . 111.7 no
N604 . C607 . H6073 . 106.7 no
C608 . C607 . H6073 . 105.9 no
H6072 . C607 . H6073 . 109.5 no
N601 . C608 . C607 . 111.9(7) yes
N601 . C608 . H6081 . 109.5 no
C607 . C608 . H6081 . 110.5 no
N601 . C608 . H6083 . 109.5 no
C607 . C608 . H6083 . 106.0 no
H6081 . C608 . H6083 . 109.5 no
N601 . C611 . C612 . 119.0(11) yes
N601 . C611 . H6111 . 109.1 no
C612 . C611 . H6111 . 107.7 no
N601 . C611 . H6112 . 105.1 no
C612 . C611 . H6112 . 106.2 no
H6111 . C611 . H6112 . 109.5 no
C611 . C612 . O601 . 112.76(7) yes
C611 . C612 . O613 . 121.99(7) yes
O601 . C612 . O613 . 125.25(7) yes
C612 . O613 . Eu7 . 112.9(5) yes
N602 . C614 . C615 . 130.9(11) yes
N602 . C614 . H6141 . 106.6 no
C615 . C614 . H6141 . 105.7 no
N602 . C614 . H6142 . 101.2 no
C615 . C614 . H6142 . 101.7 no
H6141 . C614 . H6142 . 109.5 no
C614 . C615 . O602 . 112.76(7) yes
C614 . C615 . O616 . 121.99(7) yes
O602 . C615 . O616 . 125.25(7) yes
N603 . C617 . C618 . 109.4(9) yes
N603 . C617 . H6171 . 108.1 no
C618 . C617 . H6171 . 108.5 no
N603 . C617 . H6173 . 111.2 no
C618 . C617 . H6173 . 110.1 no
H6171 . C617 . H6173 . 109.5 no
C617 . C618 . O603 . 112.76(7) yes
C617 . C618 . O619 . 121.99(7) yes
O603 . C618 . O619 . 125.25(7) yes
N604 . C621 . C622 . 124.7(9) yes
N604 . C621 . H6211 . 105.0 no
C622 . C621 . H6211 . 102.1 no
N604 . C621 . H6212 . 106.1 no
C622 . C621 . H6212 . 108.7 no
H6211 . C621 . H6212 . 109.5 no
C621 . C622 . C623 . 109.7(17) yes
C621 . C622 . C627 . 128(2) yes
C623 . C622 . C627 . 121.8(18) yes
C622 . C623 . C624 . 115.6(16) yes
C622 . C623 . H6231 . 122.2 no
C624 . C623 . H6231 . 122.2 no
C623 . C624 . O620 . 119.8(10) yes
C623 . C624 . O625 . 123.1(14) yes
O620 . C624 . O625 . 117.1(9) yes
C624 . O625 . C626 . 118.6(17) yes
O625 . C626 . C627 . 124.7(17) yes
O625 . C626 . C631 . 115.3(17) yes
C627 . C626 . C631 . 120.0(6) yes
C622 . C627 . C626 . 116.2(16) yes
C622 . C627 . C628 . 123.9(16) yes
C626 . C627 . C628 . 119.9(6) yes
C627 . C628 . C629 . 120.2(6) yes
C627 . C628 . H6281 . 120.2 no
C629 . C628 . H6281 . 119.6 no
C628 . C629 . C630 . 119.9(6) yes
C628 . C629 . H6291 . 120.3 no
C630 . C629 . H6291 . 119.7 no
C629 . C630 . C631 . 120.0(5) yes
C629 . C630 . O632 . 119.7(6) yes
C631 . C630 . O632 . 120.3(6) yes
C626 . C631 . C630 . 120.1(6) yes
C626 . C631 . H6311 . 119.7 no
C630 . C631 . H6311 . 120.3 no
C630 . O632 . C633 . 123.7(9) yes
O632 . C633 . H6331 . 109.8 no
O632 . C633 . H6332 . 109.1 no
H6331 . C633 . H6332 . 109.5 no
O632 . C633 . H6334 . 109.5 no
H6331 . C633 . H6334 . 109.5 no
H6332 . C633 . H6334 . 109.5 no
O613 . Eu7 . N701 . 141.6(4) yes
O613 . Eu7 . N702 . 133.8(4) yes
N701 . Eu7 . N702 . 67.6(2) yes
O613 . Eu7 . N703 . 69.7(4) yes
N701 . Eu7 . N703 . 104.3(4) yes
N702 . Eu7 . N703 . 67.6(2) yes
O613 . Eu7 . N704 . 75.6(3) yes
N701 . Eu7 . N704 . 67.7(2) yes
N702 . Eu7 . N704 . 103.1(4) yes
N703 . Eu7 . N704 . 67.5(2) yes
O613 . Eu7 . O701 . 95.2(6) yes
N701 . Eu7 . O701 . 64.5(6) yes
N702 . Eu7 . O701 . 129.3(5) yes
N703 . Eu7 . O701 . 140.1(4) yes
N704 . Eu7 . O701 . 73.1(4) yes
O613 . Eu7 . O702 . 137.3(4) yes
N701 . Eu7 . O702 . 77.9(3) yes
N702 . Eu7 . O702 . 63.9(6) yes
N703 . Eu7 . O702 . 126.0(5) yes
N704 . Eu7 . O702 . 145.5(3) yes
O613 . Eu7 . O703 . 72.4(4) yes
N701 . Eu7 . O703 . 139.8(3) yes
N702 . Eu7 . O703 . 72.3(3) yes
N703 . Eu7 . O703 . 61.3(6) yes
N704 . Eu7 . O703 . 126.1(6) yes
O613 . Eu7 . O709 . 77.0(7) yes
N701 . Eu7 . O709 . 124.3(8) yes
N702 . Eu7 . O709 . 119.8(8) yes
N703 . Eu7 . O709 . 130.4(8) yes
N704 . Eu7 . O709 . 137.0(8) yes
O701 . Eu7 . O702 . 90.5(5) yes
O701 . Eu7 . O703 . 150.6(5) yes
O702 . Eu7 . O703 . 82.3(5) yes
O701 . Eu7 . O709 . 77.1(8) yes
O702 . Eu7 . O709 . 63.1(8) yes
O703 . Eu7 . O709 . 74.3(9) yes
Eu7 . N701 . C701 . 108.6(5) yes
Eu7 . N701 . C708 . 109.3(6) yes
C701 . N701 . C708 . 109.2(6) yes
Eu7 . N701 . C711 . 107.8(11) yes
C701 . N701 . C711 . 110.9(6) yes
C708 . N701 . C711 . 111.0(7) yes
Eu7 . N702 . C702 . 110.8(5) yes
Eu7 . N702 . C703 . 110.2(5) yes
C702 . N702 . C703 . 108.4(6) yes
Eu7 . N702 . C714 . 107.9(11) yes
C702 . N702 . C714 . 110.0(6) yes
C703 . N702 . C714 . 109.5(6) yes
Eu7 . N703 . C704 . 108.6(6) yes
Eu7 . N703 . C705 . 108.2(5) yes
C704 . N703 . C705 . 108.3(7) yes
Eu7 . N703 . C717 . 112.9(11) yes
C704 . N703 . C717 . 109.6(6) yes
C705 . N703 . C717 . 109.2(6) yes
Eu7 . N704 . C706 . 111.3(5) yes
Eu7 . N704 . C707 . 110.2(5) yes
C706 . N704 . C707 . 109.2(6) yes
Eu7 . N704 . C721 . 107.9(9) yes
C706 . N704 . C721 . 109.2(6) yes
C707 . N704 . C721 . 109.1(6) yes
Eu7 . O701 . C712 . 129.9(8) yes
Eu7 . O702 . C715 . 130.5(8) yes
Eu7 . O703 . C718 . 134.2(8) yes
Eu7 . O709 . H7091 . 141.3 no
Eu7 . O709 . H7092 . 119.8 no
H7091 . O709 . H7092 . 95.8 no
N701 . C701 . C702 . 111.6(7) yes
N701 . C701 . H7011 . 110.6 no
C702 . C701 . H7011 . 110.2 no
N701 . C701 . H7012 . 108.3 no
C702 . C701 . H7012 . 106.5 no
H7011 . C701 . H7012 . 109.5 no
N702 . C702 . C701 . 112.0(7) yes
N702 . C702 . H7022 . 107.2 no
C701 . C702 . H7022 . 106.4 no
N702 . C702 . H7023 . 110.1 no
C701 . C702 . H7023 . 111.6 no
H7022 . C702 . H7023 . 109.5 no
N702 . C703 . C704 . 111.4(7) yes
N702 . C703 . H7031 . 110.0 no
C704 . C703 . H7031 . 109.1 no
N702 . C703 . H7032 . 109.4 no
C704 . C703 . H7032 . 107.4 no
H7031 . C703 . H7032 . 109.5 no
N703 . C704 . C703 . 111.1(7) yes
N703 . C704 . H7041 . 109.7 no
C703 . C704 . H7041 . 112.0 no
N703 . C704 . H7042 . 107.3 no
C703 . C704 . H7042 . 107.2 no
H7041 . C704 . H7042 . 109.5 no
N703 . C705 . C706 . 111.9(7) yes
N703 . C705 . H7052 . 109.1 no
C706 . C705 . H7052 . 111.6 no
N703 . C705 . H7053 . 109.3 no
C706 . C705 . H7053 . 105.3 no
H7052 . C705 . H7053 . 109.5 no
N704 . C706 . C705 . 112.0(7) yes
N704 . C706 . H7061 . 110.7 no
C705 . C706 . H7061 . 111.0 no
N704 . C706 . H7062 . 108.2 no
C705 . C706 . H7062 . 105.3 no
H7061 . C706 . H7062 . 109.5 no
N704 . C707 . C708 . 111.6(7) yes
N704 . C707 . H7071 . 108.5 no
C708 . C707 . H7071 . 110.6 no
N704 . C707 . H7072 . 112.4 no
C708 . C707 . H7072 . 104.2 no
H7071 . C707 . H7072 . 109.5 no
N701 . C708 . C707 . 111.6(7) yes
N701 . C708 . H7081 . 103.6 no
C707 . C708 . H7081 . 103.9 no
N701 . C708 . H7082 . 113.3 no
C707 . C708 . H7082 . 113.9 no
H7081 . C708 . H7082 . 109.5 no
N701 . C711 . C712 . 115.9(10) yes
N701 . C711 . H7111 . 102.7 no
C712 . C711 . H7111 . 103.6 no
N701 . C711 . H7113 . 111.7 no
C712 . C711 . H7113 . 112.5 no
H7111 . C711 . H7113 . 109.5 no
C711 . C712 . O701 . 112.76(7) yes
C711 . C712 . O713 . 121.98(7) yes
O701 . C712 . O713 . 125.25(7) yes
N702 . C714 . C715 . 114.7(10) yes
N702 . C714 . H7141 . 108.6 no
C715 . C714 . H7141 . 107.4 no
N702 . C714 . H7142 . 108.4 no
C715 . C714 . H7142 . 108.1 no
H7141 . C714 . H7142 . 109.5 no
C714 . C715 . O702 . 112.76(7) yes
C714 . C715 . O716 . 121.99(7) yes
O702 . C715 . O716 . 125.25(7) yes
C715 . O716 . Eu8 . 150.8(7) yes
N703 . C717 . C718 . 111.2(10) yes
N703 . C717 . H7172 . 110.4 no
C718 . C717 . H7172 . 109.6 no
N703 . C717 . H7173 . 109.8 no
C718 . C717 . H7173 . 106.2 no
H7172 . C717 . H7173 . 109.5 no
C717 . C718 . O703 . 112.75(7) yes
C717 . C718 . O719 . 121.99(7) yes
O703 . C718 . O719 . 125.25(7) yes
N704 . C721 . C722 . 122.2(8) yes
N704 . C721 . H7211 . 106.8 no
C722 . C721 . H7211 . 105.9 no
N704 . C721 . H7212 . 105.4 no
C722 . C721 . H7212 . 106.8 no
H7211 . C721 . H7212 . 109.5 no
C721 . C722 . C723 . 112.5(16) yes
C721 . C722 . C727 . 127.1(20) yes
C723 . C722 . C727 . 120.4(16) yes
C722 . C723 . C724 . 116.9(14) yes
C722 . C723 . H7231 . 122.2 no
C724 . C723 . H7231 . 120.9 no
C723 . C724 . O720 . 120.3(9) yes
C723 . C724 . O725 . 121.7(14) yes
O720 . C724 . O725 . 118.0(9) yes
C724 . O725 . C726 . 120.2(17) yes
O725 . C726 . C727 . 123.3(15) yes
O725 . C726 . C731 . 116.6(16) yes
C727 . C726 . C731 . 120.1(6) yes
C722 . C727 . C726 . 117.6(14) yes
C722 . C727 . C728 . 122.7(15) yes
C726 . C727 . C728 . 119.8(6) yes
C727 . C728 . C729 . 120.1(6) yes
C727 . C728 . H7281 . 119.6 no
C729 . C728 . H7281 . 120.3 no
C728 . C729 . C730 . 120.1(6) yes
C728 . C729 . H7292 . 119.7 no
C730 . C729 . H7292 . 120.3 no
C729 . C730 . C731 . 119.9(5) yes
C729 . C730 . O732 . 119.9(6) yes
C731 . C730 . O732 . 120.2(6) yes
C726 . C731 . C730 . 120.0(6) yes
C726 . C731 . H7311 . 120.3 no
C730 . C731 . H7311 . 119.7 no
C730 . O732 . C733 . 124.0(9) yes
O732 . C733 . H7331 . 110.8 no
O732 . C733 . H7332 . 108.7 no
H7331 . C733 . H7332 . 109.5 no
O732 . C733 . H7333 . 108.9 no
H7331 . C733 . H7333 . 109.5 no
H7332 . C733 . H7333 . 109.5 no
O716 . Eu8 . N801 . 150.6(3) yes
O716 . Eu8 . N802 . 85.8(4) yes
N801 . Eu8 . N802 . 67.2(2) yes
O716 . Eu8 . N803 . 78.2(5) yes
N801 . Eu8 . N803 . 100.8(4) yes
N802 . Eu8 . N803 . 67.5(2) yes
O716 . Eu8 . N804 . 135.2(4) yes
N801 . Eu8 . N804 . 67.3(2) yes
N802 . Eu8 . N804 . 106.2(4) yes
N803 . Eu8 . N804 . 68.0(2) yes
O716 . Eu8 . O801 . 127.9(5) yes
N801 . Eu8 . O801 . 61.3(6) yes
N802 . Eu8 . O801 . 117.1(5) yes
N803 . Eu8 . O801 . 152.6(3) yes
N804 . Eu8 . O801 . 85.3(3) yes
O716 . Eu8 . O802 . 71.1(4) yes
N801 . Eu8 . O802 . 86.1(3) yes
N802 . Eu8 . O802 . 64.2(5) yes
N803 . Eu8 . O802 . 123.6(5) yes
N804 . Eu8 . O802 . 153.1(3) yes
O716 . Eu8 . O803 . 62.4(3) yes
N801 . Eu8 . O803 . 145.6(3) yes
N802 . Eu8 . O803 . 131.9(5) yes
N803 . Eu8 . O803 . 71.1(6) yes
N804 . Eu8 . O803 . 78.9(3) yes
O716 . Eu8 . O809 . 73.1(8) yes
N801 . Eu8 . O809 . 121.9(7) yes
N802 . Eu8 . O809 . 142.8(7) yes
N803 . Eu8 . O809 . 133.6(7) yes
N804 . Eu8 . O809 . 110.3(6) yes
O801 . Eu8 . O802 . 78.3(4) yes
O801 . Eu8 . O803 . 111.0(6) yes
O802 . Eu8 . O803 . 126.8(3) yes
O801 . Eu8 . O809 . 60.6(8) yes
O802 . Eu8 . O809 . 79.9(7) yes
O803 . Eu8 . O809 . 63.5(8) yes
Eu8 . N801 . C801 . 109.4(6) yes
Eu8 . N801 . C808 . 109.7(5) yes
C801 . N801 . C808 . 110.2(6) yes
Eu8 . N801 . C811 . 103.4(10) yes
C801 . N801 . C811 . 111.2(6) yes
C808 . N801 . C811 . 112.8(6) yes
Eu8 . N802 . C802 . 110.0(5) yes
Eu8 . N802 . C803 . 112.1(5) yes
C802 . N802 . C803 . 108.6(6) yes
Eu8 . N802 . C814 . 102.1(9) yes
C802 . N802 . C814 . 110.7(6) yes
C803 . N802 . C814 . 113.3(6) yes
Eu8 . N803 . C804 . 110.9(5) yes
Eu8 . N803 . C805 . 110.3(5) yes
C804 . N803 . C805 . 112.2(6) yes
Eu8 . N803 . C817 . 97.8(10) yes
C804 . N803 . C817 . 112.3(6) yes
C805 . N803 . C817 . 112.5(6) yes
Eu8 . N804 . C806 . 108.2(5) yes
Eu8 . N804 . C807 . 111.8(5) yes
C806 . N804 . C807 . 110.2(6) yes
Eu8 . N804 . C821 . 105.8(8) yes
C806 . N804 . C821 . 110.7(6) yes
C807 . N804 . C821 . 110.1(6) yes
Eu8 . O801 . C812 . 127.1(8) yes
Eu8 . O802 . C815 . 126.2(7) yes
Eu8 . O803 . C818 . 122.6(8) yes
Eu8 . O809 . H8091 . 133.0 no
Eu8 . O809 . H8092 . 137.1 no
H8091 . O809 . H8092 . 78.3 no
N801 . C801 . C802 . 110.4(7) yes
N801 . C801 . H8011 . 107.0 no
C802 . C801 . H8011 . 106.4 no
N801 . C801 . H8012 . 110.9 no
C802 . C801 . H8012 . 112.4 no
H8011 . C801 . H8012 . 109.5 no
N802 . C802 . C801 . 110.0(7) yes
N802 . C802 . H8021 . 109.9 no
C801 . C802 . H8021 . 110.2 no
N802 . C802 . H8022 . 110.5 no
C801 . C802 . H8022 . 106.8 no
H8021 . C802 . H8022 . 109.5 no
N802 . C803 . C804 . 115.5(7) yes
N802 . C803 . H8032 . 110.3 no
C804 . C803 . H8032 . 112.0 no
N802 . C803 . H8033 . 106.3 no
C804 . C803 . H8033 . 102.7 no
H8032 . C803 . H8033 . 109.5 no
N803 . C804 . C803 . 115.9(7) yes
N803 . C804 . H8041 . 109.3 no
C803 . C804 . H8041 . 111.1 no
N803 . C804 . H8043 . 108.1 no
C803 . C804 . H8043 . 102.7 no
H8041 . C804 . H8043 . 109.5 no
N803 . C805 . C806 . 112.1(7) yes
N803 . C805 . H8051 . 110.7 no
C806 . C805 . H8051 . 112.6 no
N803 . C805 . H8052 . 105.6 no
C806 . C805 . H8052 . 106.0 no
H8051 . C805 . H8052 . 109.5 no
N804 . C806 . C805 . 111.6(7) yes
N804 . C806 . H8061 . 109.7 no
C805 . C806 . H8061 . 109.4 no
N804 . C806 . H8062 . 110.3 no
C805 . C806 . H8062 . 106.4 no
H8061 . C806 . H8062 . 109.5 no
N804 . C807 . C808 . 112.8(7) yes
N804 . C807 . H8071 . 107.0 no
C808 . C807 . H8071 . 105.1 no
N804 . C807 . H8073 . 110.2 no
C808 . C807 . H8073 . 112.1 no
H8071 . C807 . H8073 . 109.5 no
N801 . C808 . C807 . 112.9(7) yes
N801 . C808 . H8081 . 109.6 no
C807 . C808 . H8081 . 110.3 no
N801 . C808 . H8082 . 109.4 no
C807 . C808 . H8082 . 105.1 no
H8081 . C808 . H8082 . 109.5 no
N801 . C811 . C812 . 106.4(9) yes
N801 . C811 . H8111 . 109.1 no
C812 . C811 . H8111 . 110.2 no
N801 . C811 . H8112 . 110.9 no
C812 . C811 . H8112 . 110.7 no
H8111 . C811 . H8112 . 109.5 no
C811 . C812 . O801 . 112.76(7) yes
C811 . C812 . O813 . 121.99(7) yes
O801 . C812 . O813 . 125.25(7) yes
Eu5 . O813 . C812 . 114.5(6) yes
N802 . C814 . C815 . 112.0(9) yes
N802 . C814 . H8141 . 110.6 no
C815 . C814 . H8141 . 109.7 no
N802 . C814 . H8142 . 107.2 no
C815 . C814 . H8142 . 107.7 no
H8141 . C814 . H8142 . 109.5 no
C814 . C815 . O802 . 112.76(7) yes
C814 . C815 . O816 . 121.99(7) yes
O802 . C815 . O816 . 125.25(7) yes
N803 . C817 . C818 . 126.6(10) yes
N803 . C817 . H8171 . 107.3 no
C818 . C817 . H8171 . 105.2 no
N803 . C817 . H8172 . 103.8 no
C818 . C817 . H8172 . 103.8 no
H8171 . C817 . H8172 . 109.5 no
C817 . C818 . O803 . 112.76(7) yes
C817 . C818 . O819 . 121.99(7) yes
O803 . C818 . O819 . 125.25(7) yes
N804 . C821 . C822 . 117.6(8) yes
N804 . C821 . H8212 . 107.8 no
C822 . C821 . H8212 . 106.8 no
N804 . C821 . H8213 . 106.8 no
C822 . C821 . H8213 . 108.3 no
H8212 . C821 . H8213 . 109.5 no
C821 . C822 . C823 . 120.8(14) yes
C821 . C822 . C827 . 117.0(16) yes
C823 . C822 . C827 . 122.2(15) yes
C822 . C823 . C824 . 115.3(13) yes
C822 . C823 . H8231 . 123.0 no
C824 . C823 . H8231 . 121.7 no
C823 . C824 . O820 . 119.6(9) yes
C823 . C824 . O825 . 123.3(12) yes
O820 . C824 . O825 . 117.2(8) yes
C824 . O825 . C826 . 118.3(14) yes
O825 . C826 . C827 . 125.0(13) yes
O825 . C826 . C831 . 114.8(13) yes
C827 . C826 . C831 . 120.1(6) yes
C822 . C827 . C826 . 116.0(12) yes
C822 . C827 . C828 . 124.1(13) yes
C826 . C827 . C828 . 119.9(6) yes
C827 . C828 . C829 . 120.0(6) yes
C827 . C828 . H8282 . 120.3 no
C829 . C828 . H8282 . 119.7 no
C828 . C829 . C830 . 119.9(6) yes
C828 . C829 . H8291 . 120.3 no
C830 . C829 . H8291 . 119.7 no
C829 . C830 . C831 . 120.1(5) yes
C829 . C830 . O832 . 120.1(6) yes
C831 . C830 . O832 . 119.8(6) yes
C830 . C831 . C826 . 119.9(6) yes
C830 . C831 . H8311 . 120.4 no
C826 . C831 . H8311 . 119.7 no
C830 . O832 . C833 . 124.2(8) yes
O832 . C833 . H8331 . 109.8 no
O832 . C833 . H8332 . 109.3 no
H8331 . C833 . H8332 . 109.5 no
O832 . C833 . H8333 . 109.3 no
H8331 . C833 . H8333 . 109.5 no
H8332 . C833 . H8333 . 109.5 no
loop_
_geom_hbond_atom_site_label_D
_geom_hbond_site_symmetry_D
_geom_hbond_atom_site_label_H
_geom_hbond_site_symmetry_H
_geom_hbond_atom_site_label_A
_geom_hbond_site_symmetry_A
_geom_hbond_angle_DHA
_geom_hbond_distance_DH
_geom_hbond_distance_HA
_geom_hbond_distance_DA
_geom_hbond_publ_flag
C101 . H1012 . C115 . 131 0.95 2.57 3.27(2) yes
C103 . H1032 . C118 . 130 0.95 2.30 3.00(2) yes
C106 . H1061 . O220 4_574 143 0.95 2.57 3.37(2) yes
C107 . H1071 . C112 . 131 0.95 2.44 3.15(2) yes
C121 . H1212 . C412 . 121 0.95 2.45 3.06(2) yes
C131 . H1311 . O432 2_666 148 0.95 2.57 3.41(2) yes
C204 . H2042 . O116 . 120 0.95 2.39 2.99(2) yes
C206 . H2062 . C218 . 132 0.95 2.57 3.28(2) yes
C207 . H2071 . C223 . 129 0.95 2.58 3.27(2) yes
C221 . H2212 . O203 . 129 0.95 2.30 2.99(2) yes
C301 . H3012 . C315 . 132 0.95 2.46 3.18(2) yes
C306 . H3062 . O420 4_565 139 0.95 2.59 3.36(2) yes
C307 . H3072 . C312 . 131 0.95 2.28 2.99(2) yes
C321 . H3212 . O201 . 151 0.95 2.12 2.98(2) yes
C321 . H3212 . C212 . 121 0.95 2.55 3.16(2) yes
C328 . H3281 . O313 . 143 0.95 2.43 3.24(2) yes
C331 . H3311 . O232 2_677 155 0.95 2.42 3.31(2) yes
C402 . H4022 . O719 . 168 0.95 2.59 3.52(2) yes
C407 . H4071 . C423 . 133 0.95 2.44 3.16(2) yes
C421 . H4211 . O403 . 130 0.95 2.42 3.12(2) yes
C421 . H4212 . O401 . 126 0.95 2.57 3.22(2) yes
C503 . H5031 . C518 . 131 0.95 2.41 3.12(2) yes
C505 . H5051 . O813 . 121 0.95 2.40 3.01(2) yes
C506 . H5062 . C523 . 132 0.95 2.55 3.26(2) yes
C507 . H5071 . C512 . 130 0.95 2.54 3.23(2) yes
C517 . H5172 . O813 . 121 0.95 2.15 2.77(2) yes
C521 . H5211 . O813 . 133 0.95 2.20 2.93(2) yes
C602 . H6021 . O119 . 156 0.95 2.43 3.33(2) yes
C606 . H6062 . C618 . 135 0.95 2.16 2.91(2) yes
C606 . H6062 . C628 . 133 0.95 2.54 3.26(2) yes
C614 . H6142 . C515 . 130 0.95 2.54 3.23(2) yes
C614 . H6142 . O516 . 126 0.95 1.93 2.60(2) yes
C628 . H6281 . O603 . 170 0.95 2.52 3.46(2) yes
C628 . H6281 . C618 . 155 0.95 2.42 3.30(2) yes
C628 . H6281 . O619 . 132 0.95 2.11 2.84(2) yes
C701 . H7012 . C715 . 132 0.95 2.54 3.25(2) yes
C703 . H7032 . C718 . 129 0.95 2.48 3.16(2) yes
C705 . H7053 . O613 . 125 0.95 2.55 3.19(2) yes
C706 . H7062 . O820 4_565 145 0.95 2.58 3.41(2) yes
C707 . H7072 . C712 . 130 0.95 2.48 3.17(2) yes
C721 . H7212 . O701 . 130 0.95 2.54 3.24(2) yes
C728 . H7281 . O713 . 133 0.95 2.51 3.23(2) yes
C803 . H8032 . O319 4_564 148 0.95 2.50 3.34(2) yes
C806 . H8062 . C818 . 132 0.95 2.58 3.29(2) yes
O109 . H1091 . O216 . 179 0.95 1.89 2.84(2) yes
O109 . H1092 . O402 . 179 0.95 2.09 3.04(2) yes
O209 . H2091 . O102 . 178 0.96 1.70 2.66(2) yes
O209 . H2091 . C115 . 144 0.96 2.30 3.12(2) yes
O209 . H2092 . O301 . 125 0.95 2.15 2.80(2) yes
O309 . H3091 . O202 . 179 0.95 1.98 2.93(2) yes
O309 . H3092 . O416 . 176 0.95 2.14 3.08(2) yes
O409 . H4091 . O101 . 125 0.95 2.27 2.92(2) yes
O409 . H4091 . O113 . 179 0.95 2.52 3.47(2) yes
O409 . H4092 . O302 . 179 0.96 1.65 2.61(2) yes
O409 . H4092 . C315 . 143 0.96 2.23 3.05(2) yes
O509 . H5091 . O616 . 179 0.95 2.30 3.25(2) yes
O509 . H5092 . O802 . 179 0.95 2.11 3.06(2) yes
O609 . H6092 . O701 . 179 0.95 1.80 2.75(2) yes
O609 . H6092 . C712 . 151 0.95 2.55 3.41(2) yes
O709 . H7091 . O602 . 179 0.95 1.99 2.94(2) yes
O809 . H8091 . O501 . 179 0.95 1.86 2.81(2) yes


####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_EuL-Triclinic
_database_code_depnum_ccdc_archive 'CCDC 1589836'
_audit_update_record             
;
2017-12-07 deposited with the CCDC.
2018-02-05 downloaded from the CCDC.
;
#==============================================================================
_audit_creation_date             2017-11-28
_audit_creation_method           CRYSTALS_ver_14.61_build_6156

_oxford_structure_analysis_title DIA0334a
_chemical_name_systematic        .
_chemical_melting_point          'not measured'

_refine_special_details          
; 
This was the second attempt to collect data on this 
material, using synchrotron radiation.  In addition 
to the problems seen previously, the crystals now also 
suffered radiation damage.  Several data attempts were 
made to collect data, but in each case it was not 
possible to collect a complete dataset before the 
crystals ceased to diffract and the data were still
very weak and the data were no better than those 
collected using laboratory radiation.  Again the
structure solved with two molecules in the 
asymmetric unit, however, this time the structure was
found to be triclinic and data are included here for
completeness.

The data were processed repeatedly using a variety of 
different software.  In each case, there were question-
marks over the resultant standard uncertainties as the 
data are very weak and uncertainty estimates are poor
for weak data colelcted using a photon counting detector,
especially where the peak-width is variable.  It was clear 
from plotting the I/σ(I) distribution that there was an
issue, so square-root(|I|) was used to replace σ(I) 
which gave a distribution more in-keeping with what would 
be expected.

The difference map indicated the presence of diffuse electron
density believed to be disordered solvent.  SQUEEZE was used 
leaving a void 
from which the electron density was removed.

Despite the issues surrounding data collection and 
processing, and corresponding deficiencies in the 
refinement, the results support the conclusions drawn 
in the manuscript.
;

loop_
_platon_squeeze_void_nr
_platon_squeeze_void_average_x
_platon_squeeze_void_average_y
_platon_squeeze_void_average_z
_platon_squeeze_void_volume
_platon_squeeze_void_count_electrons
_platon_squeeze_void_content
1 -0.008 0.278 0.058 3803 1304 ' '
_platon_squeeze_void_probe_radius 1.20
_platon_squeeze_details          
; 
The discrete Fourier transform of the void region were treated as 
contributions to the A and B parts of the calculated structure factors.
;


_cell_length_a                   17.4223(9)
_cell_length_b                   25.1438(15)
_cell_length_c                   33.2547(15)
_cell_angle_alpha                106.177(5)
_cell_angle_beta                 90.802(5)
_cell_angle_gamma                102.807(5)
_cell_volume                     13598.1(13)

_symmetry_cell_setting           triclinic
_symmetry_space_group_name_H-M   'P -1 '
_symmetry_space_group_name_Hall  '-P 1'
loop_
_symmetry_equiv_pos_as_xyz
x,y,z
-x,-y,-z

loop_
_atom_type_symbol
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_Cromer_Mann_a1
_atom_type_scat_Cromer_Mann_b1
_atom_type_scat_Cromer_Mann_a2
_atom_type_scat_Cromer_Mann_b2
_atom_type_scat_Cromer_Mann_a3
_atom_type_scat_Cromer_Mann_b3
_atom_type_scat_Cromer_Mann_a4
_atom_type_scat_Cromer_Mann_b4
_atom_type_scat_Cromer_Mann_c
_atom_type_scat_source
C 0.0020 0.0020 2.3100 20.8439 1.0200 10.2075 1.5886 0.5687 0.8650 51.6512
0.2156
; 
International Tables Vol C 4.2.6.8 and 6.1.1.4
and D. T. Cromer, J. Appl. Cryst. (1983), 16, 433.
;
H 0.0000 0.0000 0.4930 10.5109 0.3229 26.1257 0.1402 3.1424 0.0408 57.7998
0.0030
; 
International Tables Vol C 4.2.6.8 and 6.1.1.4
and D. T. Cromer, J. Appl. Cryst. (1983), 16, 433.
;
N 0.0040 0.0030 12.2126 0.0057 3.1322 9.8933 2.0125 28.9975 1.1663 0.5826
-11.5290
; 
International Tables Vol C 4.2.6.8 and 6.1.1.4
and D. T. Cromer, J. Appl. Cryst. (1983), 16, 433.
;
O 0.0070 0.0060 3.0485 13.2771 2.2868 5.7011 1.5463 0.3239 0.8670 32.9089
0.2508
; 
International Tables Vol C 4.2.6.8 and 6.1.1.4
and D. T. Cromer, J. Appl. Cryst. (1983), 16, 433.
;
Eu -0.5610 3.4850 24.6274 2.3879 19.0886 0.1942 13.7603 13.7546 2.9227 123.1740
2.5745
; 
International Tables Vol C 4.2.6.8 and 6.1.1.4
and D. T. Cromer, J. Appl. Cryst. (1983), 16, 433.
;


_cell_formula_units_Z            4

# Given Formula = C0.50 H0.50 Eu0.50 N0.50 O0.50 
# Dc =      0.05 Fooo =    170.00 Mu =      2.27 M =     97.49
# Found Formula = C100 H132 Eu4 N16 O40 
# Dc =      1.37 FOOO =   5664.00 Mu =     18.96 M =   2806.06

_chemical_formula_sum            'C100 H132 Eu4 N16 O40'
_chemical_formula_moiety         'C100 H132 Eu4 N16 O40'
_chemical_compound_source        .
_chemical_formula_weight         2806.06


_cell_measurement_reflns_used    27350
_cell_measurement_theta_min      1
_cell_measurement_theta_max      24
_cell_measurement_temperature    100

_exptl_crystal_description       plate
_exptl_crystal_colour            clear_pale_colourless
_exptl_crystal_size_min          0.05
_exptl_crystal_size_mid          0.10
_exptl_crystal_size_max          0.15

_exptl_crystal_density_diffrn    1.371
_exptl_crystal_density_meas      'not measured'
_exptl_crystal_density_method    'not measured'
# Non-dispersive F(000): 
_exptl_crystal_F_000             5664
_exptl_absorpt_coefficient_mu    1.896

# Sheldrick geometric approximatio 0.83 0.91 
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   'CrysAlisPro, (Agilent, 2011)'
_exptl_absorpt_correction_T_min  0.89
_exptl_absorpt_correction_T_max  0.91
_diffrn_detector                 'Photon counting pixel array (area)'
_diffrn_radiation_type           Synchrotron
_diffrn_measurement_device       'Fixed χ 3-circle diffractometer'
_diffrn_measurement_device_type  'Fluid Film Devices'
_diffrn_measurement_method       'shutterless scans'
_diffrn_measurement_specimen_support 'MiTeGen MicroMount'
_diffrn_radiation_source         'Diamond Light Source Beamline I19-1'
_diffrn_radiation_monochromator  'Silicon 111'
_diffrn_radiation_wavelength     0.6889

# If a reference occurs more than once, delete the author 
# and date from subsequent references. 
_computing_data_collection       'Diamond GDA'
_computing_cell_refinement       'DIALS 2theta refinement, DIALS'
_computing_data_reduction        
;
aimless (Evans, P. R. and Murshudov, G. N., 2013)
ccp4 (Winn, M. D. et al., 2011)
DIALS
pointless (Evans, P., 2006)
XIA2 0.4.0.438-g4431aaa (Winter, G., 2010)
;
_computing_structure_solution    'SHELXT (Sheldrick, 2015)'
_computing_structure_refinement  'CRYSTALS (Betteridge et al., 2003)'
_computing_publication_material  'CRYSTALS (Betteridge et al., 2003)'
_computing_molecular_graphics    'CAMERON (Watkin et al., 1996)'

_diffrn_standards_interval_time  .
_diffrn_standards_interval_count .
_diffrn_standards_number         0
_diffrn_standards_decay_%        .

_diffrn_ambient_temperature      100
_diffrn_reflns_number            288225
_reflns_number_total             27350
_diffrn_reflns_av_R_equivalents  0.400
# Number of reflections with Friedels Law is 27350 
# Theoretical number of reflections is about 40754 


_diffrn_reflns_theta_min         1.240
_diffrn_reflns_theta_max         17.943
_diffrn_measured_fraction_theta_max 0.696

_diffrn_reflns_theta_full        17.943
_diffrn_measured_fraction_theta_full 0.696


_diffrn_reflns_limit_h_min       -15
_diffrn_reflns_limit_h_max       15
_diffrn_reflns_limit_k_min       -22
_diffrn_reflns_limit_k_max       21
_diffrn_reflns_limit_l_min       0
_diffrn_reflns_limit_l_max       29
_reflns_limit_h_min              -15
_reflns_limit_h_max              15
_reflns_limit_k_min              -22
_reflns_limit_k_max              21
_reflns_limit_l_min              0
_reflns_limit_l_max              29

_oxford_diffrn_Wilson_B_factor   5.23
_oxford_diffrn_Wilson_scale      39.19

_atom_sites_solution_primary     direct #heavy,direct,difmap,geom,iterative
# _atom_sites_solution_secondary  difmap
_atom_sites_solution_hydrogens   difmap

_refine_diff_density_min         -1.87
_refine_diff_density_max         4.21


# The current dictionary definitions do not cover the 
# situation where the reflections used for refinement were 
# selected by a user-defined sigma threshold 


# The values actually used during refinement 
_oxford_reflns_threshold_expression_ref I>3.0\s(I)
_refine_ls_number_reflns         14186
_refine_ls_number_restraints     8786
_refine_ls_number_parameters     2881
_oxford_refine_ls_R_factor_ref   0.1613
_refine_ls_wR_factor_ref         0.1774
_refine_ls_goodness_of_fit_ref   1.1658
_refine_ls_shift/su_max          0.0013320
_refine_ls_shift/su_mean         0.0000501


# The values computed with all filters except I/sigma 
_oxford_reflns_number_all        14186
_refine_ls_R_factor_all          0.1613
_refine_ls_wR_factor_all         0.1774

# The values computed with a 2 sigma cutoff - a la SHELX 
_reflns_threshold_expression     I>2.0σ(I)
_reflns_number_gt                14186
_refine_ls_R_factor_gt           0.1613
_refine_ls_wR_factor_gt          0.1774

# choose from: rm (reference molecule of known chirality), 
# ad (anomolous dispersion - Flack), rmad (rm and ad), 
# syn (from synthesis), unk (unknown) or . (not applicable). 
_chemical_absolute_configuration .


_refine_ls_structure_factor_coef F
_refine_ls_matrix_type           full
_refine_ls_hydrogen_treatment    constr #undef, noref, refall,
# refxyz, refU, constr or mixed
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
;
 Method, part 1, Chebychev polynomial, (Watkin, 1994, Prince, 1982) 
 [weight] = 1.0/[A₀*T₀(x)+A₁*T₁(x) ... +Aₙ₋₁]*Tₙ₋₁(x)] 
 where Ai are the Chebychev coefficients listed below and x= Fcalc/Fmax 
 Method = Robust Weighting (Prince, 1982) 
 W = [weight] * [1-(deltaF/6*sigmaF)²]² 
 Ai are: 
 2.17 2.12 1.25 0.130 0.303E-01 
;

# Uequiv = arithmetic mean of Ui i.e. Ueqiv = (U1+U2+U3)/3

# Replace last . with number of unfound hydrogen atoms attached to an atom.

# ..._refinement_flags_... 
# . no refinement constraints           S special position constraint on site
# G rigid group refinement of site      R riding atom
# D distance or angle restraint on site T thermal displacement constraints
# U Uiso or Uij restraint (rigid bond)  P partial occupancy constraint


loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_occupancy
_atom_site_adp_type
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
_atom_site_attached_hydrogens
Eu1 Eu 0.79282(10) 0.67896(7) 0.60321(5) 0.0852 1.0000 Uani D U . . . .
C101 C 0.9650(8) 0.7634(5) 0.6645(4) 0.1061 1.0000 Uani D U . . . .
O101 O 0.7323(8) 0.7556(4) 0.6357(3) 0.0924 1.0000 Uani D U . . . .
N101 N 0.9017(6) 0.7772(3) 0.6421(3) 0.0972 1.0000 Uani D U . . . .
C102 C 0.9977(6) 0.7158(4) 0.6372(5) 0.1029 1.0000 Uani D U . . . .
O102 O 0.8169(6) 0.6786(4) 0.6747(2) 0.0944 1.0000 Uani D U . . . .
N102 N 0.9370(5) 0.6614(4) 0.6218(3) 0.0952 1.0000 Uani D U . . . .
C103 C 0.9626(9) 0.6229(6) 0.5845(3) 0.0967 1.0000 Uani D U . . . .
O103 O 0.7885(5) 0.5789(3) 0.5895(4) 0.0889 1.0000 Uani D U . . . .
N103 N 0.8649(6) 0.6340(4) 0.5339(2) 0.0872 1.0000 Uani D U . . . .
C104 C 0.9496(5) 0.6389(6) 0.5446(3) 0.0931 1.0000 Uani D U . . . .
N104 N 0.8313(5) 0.7502(3) 0.5539(2) 0.0871 1.0000 Uani D U . . . .
C105 C 0.8549(10) 0.6636(5) 0.5022(3) 0.0859 1.0000 Uani D U . . . .
C106 C 0.8807(9) 0.7280(5) 0.5200(4) 0.0881 1.0000 Uani D U . . . .
C107 C 0.8714(8) 0.8083(4) 0.5800(4) 0.0931 1.0000 Uani D U . . . .
C108 C 0.9340(6) 0.8082(6) 0.6119(3) 0.1021 1.0000 Uani D U . . . .
O109 O 0.6702(7) 0.6357(8) 0.6329(6) 0.0917 1.0000 Uani D U . . . .
C111 C 0.8561(7) 0.8115(6) 0.6728(3) 0.1035 1.0000 Uani D U . . . .
C112 C 0.7691(7) 0.8033(4) 0.6599(3) 0.1078 1.0000 Uani D U . . . .
O113 O 0.7375(8) 0.8441(4) 0.6738(3) 0.1499 1.0000 Uani D U . . . .
C114 C 0.9238(7) 0.6327(4) 0.6560(3) 0.0988 1.0000 Uani D U . . . .
C115 C 0.8675(6) 0.6559(4) 0.6870(2) 0.0972 1.0000 Uani D U . . . .
O116 O 0.8732(7) 0.6514(4) 0.7234(3) 0.0975 1.0000 Uani D U . . . .
C117 C 0.8219(5) 0.5726(5) 0.5188(4) 0.0884 1.0000 Uani D U . . . .
C118 C 0.8003(5) 0.5468(3) 0.5545(4) 0.0930 1.0000 Uani D U . . . .
O119 O 0.7945(5) 0.4946(4) 0.5478(4) 0.1105 1.0000 Uani D U . . . .
O120 O 0.7760(5) 0.8123(7) 0.4060(4) 0.1408 1.0000 Uani D U . . . .
C121 C 0.7537(5) 0.7524(6) 0.5341(6) 0.0890 1.0000 Uani D U . . . .
C122 C 0.7483(5) 0.7938(5) 0.5063(5) 0.0951 1.0000 Uani D U . . . .
C123 C 0.7691(5) 0.7785(5) 0.4649(5) 0.1026 1.0000 Uani D U . . . .
C124 C 0.7595(5) 0.8213(5) 0.4436(5) 0.1137 1.0000 Uani D U . . . .
O125 O 0.7350(5) 0.8684(6) 0.4607(4) 0.1151 1.0000 Uani D U . . . .
C126 C 0.7164(5) 0.8787(6) 0.5012(4) 0.1080 1.0000 Uani D U . . . .
C127 C 0.7198(5) 0.8460(5) 0.5282(5) 0.0998 1.0000 Uani D U . . . .
C128 C 0.6985(5) 0.8634(5) 0.5688(5) 0.1010 1.0000 Uani D U . . . .
C129 C 0.6733(5) 0.9136(5) 0.5824(4) 0.1094 1.0000 Uani D U . . . .
C130 C 0.6700(5) 0.9462(5) 0.5554(5) 0.1142 1.0000 Uani D U . . . .
C131 C 0.6914(5) 0.9287(6) 0.5148(4) 0.1177 1.0000 Uani D U . . . .
O132 O 0.6443(5) 0.9973(4) 0.5692(6) 0.1261 1.0000 Uani D U . . . .
C133 C 0.6228(5) 1.0138(7) 0.6108(6) 0.1287 1.0000 Uani D U . . . .
Eu2 Eu 0.81261(11) 0.66488(7) 0.78661(5) 0.0928 1.0000 Uani D U . . . .
C201 C 0.7657(10) 0.5560(6) 0.8374(4) 0.1199 1.0000 Uani D U . . . .
O201 O 0.6910(5) 0.6838(5) 0.8133(2) 0.0961 1.0000 Uani D U . . . .
N201 N 0.7368(6) 0.6079(4) 0.8395(3) 0.1083 1.0000 Uani D U . . . .
C202 C 0.7766(9) 0.5235(4) 0.7932(4) 0.1201 1.0000 Uani D U . . . .
O202 O 0.7156(6) 0.5920(4) 0.7369(3) 0.1012 1.0000 Uani D U . . . .
N202 N 0.8339(6) 0.5574(3) 0.7720(3) 0.1119 1.0000 Uani D U . . . .
C203 C 0.9157(7) 0.5567(5) 0.7828(5) 0.1211 1.0000 Uani D U . . . .
O203 O 0.9049(7) 0.7546(4) 0.7924(2) 0.1005 1.0000 Uani D U . . . .
N203 N 0.9655(4) 0.6627(4) 0.8019(3) 0.1087 1.0000 Uani D U . . . .
C204 C 0.9771(7) 0.6066(4) 0.7782(5) 0.1149 1.0000 Uani D U . . . .
N204 N 0.8668(5) 0.7137(4) 0.8688(2) 0.1063 1.0000 Uani D U . . . .
C205 C 0.9855(8) 0.6764(6) 0.8475(3) 0.1164 1.0000 Uani D U . . . .
C206 C 0.9540(6) 0.7267(5) 0.8724(4) 0.1104 1.0000 Uani D U . . . .
C207 C 0.8329(8) 0.6787(7) 0.8961(4) 0.1142 1.0000 Uani D U . . . .
C208 C 0.7483(7) 0.6465(6) 0.8829(3) 0.1094 1.0000 Uani D U . . . .
O209 O 0.7578(12) 0.7208(7) 0.7460(6) 0.0967 1.0000 Uani D U . . . .
C211 C 0.6509(7) 0.5914(5) 0.8241(2) 0.1080 1.0000 Uani D U . . . .
C212 C 0.6336(5) 0.6442(5) 0.8157(2) 0.1016 1.0000 Uani D U . . . .
O213 O 0.5631(5) 0.6464(6) 0.8117(2) 0.1067 1.0000 Uani D U . . . .
C214 C 0.8138(7) 0.5366(5) 0.7254(4) 0.1137 1.0000 Uani D U . . . .
C215 C 0.7394(6) 0.5518(4) 0.7119(2) 0.1172 1.0000 Uani D U . . . .
O216 O 0.7050(8) 0.5240(5) 0.6766(3) 0.1655 1.0000 Uani D U . . . .
C217 C 1.0130(9) 0.7085(5) 0.7853(2) 0.1124 1.0000 Uani D U . . . .
C218 C 0.9774(7) 0.7586(4) 0.7858(2) 0.1087 1.0000 Uani D U . . . .
O219 O 1.0211(7) 0.8019(5) 0.7797(2) 0.1372 1.0000 Uani D U . . . .
O220 O 0.8515(9) 0.8402(7) 1.0346(4) 0.1315 1.0000 Uani D U . . . .
C221 C 0.8379(9) 0.7679(6) 0.8789(5) 0.1092 1.0000 Uani D U . . . .
C222 C 0.8682(8) 0.8091(5) 0.9248(5) 0.1063 1.0000 Uani D U . . . .
C223 C 0.8363(8) 0.8002(6) 0.9616(4) 0.1130 1.0000 Uani D U . . . .
C224 C 0.8754(8) 0.8443(6) 1.0001(4) 0.1184 1.0000 Uani D U . . . .
O225 O 0.9345(8) 0.8880(6) 1.0004(4) 0.1214 1.0000 Uani D U . . . .
C226 C 0.9622(8) 0.8942(6) 0.9636(5) 0.1200 1.0000 Uani D U . . . .
C227 C 0.9353(7) 0.8582(6) 0.9238(5) 0.1152 1.0000 Uani D U . . . .
C228 C 0.9697(8) 0.8703(6) 0.8892(4) 0.1193 1.0000 Uani D U . . . .
C229 C 1.0310(7) 0.9178(6) 0.8943(4) 0.1314 1.0000 Uani D U . . . .
C230 C 1.0580(7) 0.9535(5) 0.9341(5) 0.1403 1.0000 Uani D U . . . .
C231 C 1.0234(8) 0.9415(6) 0.9687(4) 0.1325 1.0000 Uani D U . . . .
O232 O 1.1205(7) 1.0021(5) 0.9396(6) 0.1598 1.0000 Uani D U . . . .
C233 C 1.1549(9) 1.0134(8) 0.9037(8) 0.1716 1.0000 Uani D U . . . .
Eu3 Eu 0.49839(10) 0.69034(8) 0.77231(5) 0.0922 1.0000 Uani D U . . . .
C301 C 0.4004(7) 0.7858(5) 0.7484(5) 0.1104 1.0000 Uani D U . . . .
O301 O 0.6169(6) 0.7605(5) 0.7710(2) 0.0961 1.0000 Uani D U . . . .
N301 N 0.4728(6) 0.7944(3) 0.7756(3) 0.0986 1.0000 Uani D U . . . .
C302 C 0.3311(6) 0.7438(4) 0.7575(5) 0.1130 1.0000 Uani D U . . . .
O302 O 0.4744(8) 0.6955(4) 0.7024(2) 0.0985 1.0000 Uani D U . . . .
N302 N 0.3455(4) 0.6860(4) 0.7498(3) 0.1096 1.0000 Uani D U . . . .
C303 C 0.2911(6) 0.6519(7) 0.7721(4) 0.1205 1.0000 Uani D U . . . .
O303 O 0.4239(7) 0.5933(4) 0.7469(5) 0.1140 1.0000 Uani D U . . . .
N303 N 0.3950(5) 0.6552(4) 0.8256(3) 0.1129 1.0000 Uani D U . . . .
C304 C 0.3173(7) 0.6672(8) 0.8184(4) 0.1203 1.0000 Uani D U . . . .
N304 N 0.5206(5) 0.7639(3) 0.8519(2) 0.0933 1.0000 Uani D U . . . .
C305 C 0.4286(9) 0.6837(5) 0.8696(3) 0.1079 1.0000 Uani D U . . . .
C306 C 0.4569(8) 0.7477(5) 0.8786(4) 0.0999 1.0000 Uani D U . . . .
C307 C 0.5268(8) 0.8231(4) 0.8504(4) 0.0953 1.0000 Uani D U . . . .
C308 C 0.4660(8) 0.8272(6) 0.8193(3) 0.1007 1.0000 Uani D U . . . .
O309 O 0.5840(10) 0.6397(8) 0.7223(5) 0.1029 1.0000 Uani D U . . . .
C311 C 0.5431(6) 0.8251(7) 0.7582(2) 0.1047 1.0000 Uani D U . . . .
C312 C 0.6199(5) 0.8095(5) 0.7669(2) 0.1033 1.0000 Uani D U . . . .
O313 O 0.6831(7) 0.8460(5) 0.7698(2) 0.1255 1.0000 Uani D U . . . .
C314 C 0.3359(8) 0.6561(3) 0.7035(4) 0.1066 1.0000 Uani D U . . . .
C315 C 0.4079(7) 0.6761(4) 0.6814(2) 0.0988 1.0000 Uani D U . . . .
O316 O 0.3984(8) 0.6725(4) 0.6434(3) 0.0906 1.0000 Uani D U . . . .
C317 C 0.3864(6) 0.5919(4) 0.8159(5) 0.1288 1.0000 Uani D U . . . .
C318 C 0.4277(5) 0.5711(4) 0.7765(5) 0.1290 1.0000 Uani D U . . . .
O319 O 0.4635(6) 0.5328(4) 0.7750(6) 0.2003 1.0000 Uani D U . . . .
O320 O 0.6237(7) 0.8285(6) 1.0245(4) 0.1099 1.0000 Uani D U . . . .
C321 C 0.5984(8) 0.7602(6) 0.8705(5) 0.0935 1.0000 Uani D U . . . .
C322 C 0.6352(6) 0.8037(5) 0.9147(4) 0.0878 1.0000 Uani D U . . . .
C323 C 0.6066(7) 0.7921(5) 0.9512(4) 0.0898 1.0000 Uani D U . . . .
C324 C 0.6450(6) 0.8351(5) 0.9902(4) 0.0956 1.0000 Uani D U . . . .
O325 O 0.7008(6) 0.8806(5) 0.9906(4) 0.0977 1.0000 Uani D U . . . .
C326 C 0.7267(6) 0.8902(5) 0.9543(4) 0.0885 1.0000 Uani D U . . . .
C327 C 0.6988(6) 0.8551(5) 0.9144(5) 0.0851 1.0000 Uani D U . . . .
C328 C 0.7296(6) 0.8692(5) 0.8797(4) 0.0868 1.0000 Uani D U . . . .
C329 C 0.7885(6) 0.9182(5) 0.8848(4) 0.0975 1.0000 Uani D U . . . .
C330 C 0.8164(6) 0.9530(5) 0.9246(4) 0.0971 1.0000 Uani D U . . . .
C331 C 0.7854(6) 0.9391(5) 0.9594(4) 0.0911 1.0000 Uani D U . . . .
O332 O 0.8766(6) 1.0030(5) 0.9300(5) 0.1103 1.0000 Uani D U . . . .
C333 C 0.9067(8) 1.0162(7) 0.8938(7) 0.1207 1.0000 Uani D U . . . .
Eu4 Eu 0.46693(9) 0.68065(6) 0.58298(5) 0.0728 1.0000 Uani D U . . . .
C401 C 0.4237(7) 0.5698(6) 0.4866(3) 0.0838 1.0000 Uani D U . . . .
O401 O 0.5998(5) 0.6897(5) 0.5620(3) 0.0750 1.0000 Uani D U . . . .
N401 N 0.4922(6) 0.6184(3) 0.5046(2) 0.0789 1.0000 Uani D U . . . .
C402 C 0.3916(9) 0.5398(4) 0.5187(4) 0.0877 1.0000 Uani D U . . . .
O402 O 0.5046(8) 0.6023(3) 0.5996(3) 0.0865 1.0000 Uani D U . . . .
N402 N 0.3621(5) 0.5777(3) 0.5546(3) 0.0836 1.0000 Uani D U . . . .
C403 C 0.2824(6) 0.5832(4) 0.5447(5) 0.0886 1.0000 Uani D U . . . .
O403 O 0.4448(8) 0.7735(4) 0.6155(2) 0.0916 1.0000 Uani D U . . . .
N403 N 0.3159(4) 0.6897(4) 0.5713(3) 0.0844 1.0000 Uani D U . . . .
C404 C 0.2614(6) 0.6359(4) 0.5722(5) 0.0911 1.0000 Uani D U . . . .
N404 N 0.4478(5) 0.7305(3) 0.5216(3) 0.0794 1.0000 Uani D U . . . .
C405 C 0.3045(6) 0.7030(6) 0.5313(3) 0.0884 1.0000 Uani D U . . . .
C406 C 0.3729(6) 0.7492(5) 0.5255(5) 0.0864 1.0000 Uani D U . . . .
C407 C 0.4518(9) 0.6935(6) 0.4789(3) 0.0865 1.0000 Uani D U . . . .
C408 C 0.5088(8) 0.6557(5) 0.4767(4) 0.0841 1.0000 Uani D U . . . .
O409 O 0.5693(9) 0.7301(7) 0.6434(4) 0.0875 1.0000 Uani D U . . . .
C411 C 0.5637(6) 0.5971(5) 0.5117(3) 0.0813 1.0000 Uani D U . . . .
C412 C 0.6228(4) 0.6459(4) 0.5422(3) 0.0793 1.0000 Uani D U . . . .
O413 O 0.6919(5) 0.6408(5) 0.5464(3) 0.0826 1.0000 Uani D U . . . .
C414 C 0.3661(7) 0.5577(4) 0.5928(3) 0.0921 1.0000 Uani D U . . . .
C415 C 0.4498(7) 0.5708(4) 0.6129(2) 0.0978 1.0000 Uani D U . . . .
O416 O 0.4611(9) 0.5496(4) 0.6417(3) 0.1409 1.0000 Uani D U . . . .
C417 C 0.3041(8) 0.7380(4) 0.6075(2) 0.0991 1.0000 Uani D U . . . .
C418 C 0.3787(8) 0.7848(3) 0.6240(2) 0.1041 1.0000 Uani D U . . . .
O419 O 0.3714(9) 0.8325(4) 0.6455(3) 0.1526 1.0000 Uani D U . . . .
O420 O 0.5640(6) 0.8411(7) 0.4019(4) 0.1329 1.0000 Uani D U . . . .
C421 C 0.5171(6) 0.7818(6) 0.5323(5) 0.0914 1.0000 Uani D U . . . .
C422 C 0.5165(6) 0.8181(5) 0.4999(5) 0.1005 1.0000 Uani D U . . . .
C423 C 0.5476(6) 0.8069(5) 0.4606(5) 0.1081 1.0000 Uani D U . . . .
C424 C 0.5378(6) 0.8475(5) 0.4374(5) 0.1148 1.0000 Uani D U . . . .
O425 O 0.5032(6) 0.8904(6) 0.4518(4) 0.1132 1.0000 Uani D U . . . .
C426 C 0.4744(5) 0.8989(6) 0.4904(4) 0.1091 1.0000 Uani D U . . . .
C427 C 0.4772(5) 0.8663(5) 0.5175(5) 0.1032 1.0000 Uani D U . . . .
C428 C 0.4460(6) 0.8800(5) 0.5560(5) 0.1080 1.0000 Uani D U . . . .
C429 C 0.4114(5) 0.9260(5) 0.5673(4) 0.1147 1.0000 Uani D U . . . .
C430 C 0.4084(5) 0.9585(4) 0.5402(4) 0.1195 1.0000 Uani D U . . . .
C431 C 0.4402(6) 0.9450(5) 0.5018(4) 0.1172 1.0000 Uani D U . . . .
O432 O 0.3735(6) 1.0056(4) 0.5518(6) 0.1341 1.0000 Uani D U . . . .
C433 C 0.3420(6) 1.0185(7) 0.5913(6) 0.1429 1.0000 Uani D U . . . .
Eu5 Eu 0.00162(10) 0.69370(7) 0.10857(6) 0.0895 1.0000 Uani D U . . . .
C501 C -0.1101(8) 0.7819(5) 0.1679(4) 0.1095 1.0000 Uani D U . . . .
N501 N -0.0392(6) 0.7938(3) 0.1452(3) 0.1000 1.0000 Uani D U . . . .
O501 O 0.1154(6) 0.7700(4) 0.1381(3) 0.0918 1.0000 Uani D U . . . .
O502 O -0.0190(8) 0.6887(4) 0.1790(3) 0.1026 1.0000 Uani D U . . . .
N502 N -0.1534(4) 0.6797(4) 0.1254(3) 0.1084 1.0000 Uani D U . . . .
C502 C -0.1761(6) 0.7344(4) 0.1423(5) 0.1141 1.0000 Uani D U . . . .
N503 N -0.0999(5) 0.6491(5) 0.0382(2) 0.1056 1.0000 Uani D U . . . .
C503 C -0.2056(7) 0.6430(7) 0.0876(3) 0.1143 1.0000 Uani D U . . . .
O503 O -0.0539(5) 0.5936(3) 0.0961(5) 0.1122 1.0000 Uani D U . . . .
N504 N 0.0134(6) 0.7638(4) 0.0580(3) 0.0962 1.0000 Uani D U . . . .
C504 C -0.1799(7) 0.6571(7) 0.0478(4) 0.1148 1.0000 Uani D U . . . .
C505 C -0.0678(10) 0.6765(6) 0.0062(3) 0.1104 1.0000 Uani D U . . . .
C506 C -0.0483(9) 0.7410(5) 0.0222(4) 0.1075 1.0000 Uani D U . . . .
C507 C 0.0104(9) 0.8223(4) 0.0825(4) 0.1014 1.0000 Uani D U . . . .
C508 C -0.0513(8) 0.8236(6) 0.1140(3) 0.1037 1.0000 Uani D U . . . .
O509 O 0.0928(11) 0.6484(8) 0.1399(7) 0.1139 1.0000 Uani D U . . . .
C511 C 0.0311(6) 0.8276(7) 0.1753(4) 0.1000 1.0000 Uani D U . . . .
C512 C 0.1117(5) 0.8178(4) 0.1629(3) 0.0989 1.0000 Uani D U . . . .
O513 O 0.1712(7) 0.8573(5) 0.1779(3) 0.1230 1.0000 Uani D U . . . .
C514 C -0.1569(9) 0.6484(4) 0.1581(4) 0.1110 1.0000 Uani D U . . . .
C515 C -0.0858(7) 0.6684(4) 0.1901(3) 0.1064 1.0000 Uani D U . . . .
O516 O -0.0964(8) 0.6645(4) 0.2263(3) 0.1055 1.0000 Uani D U . . . .
C517 C -0.0990(7) 0.5874(6) 0.0259(5) 0.1194 1.0000 Uani D U . . . .
C518 C -0.0898(5) 0.5614(3) 0.0614(5) 0.1259 1.0000 Uani D U . . . .
O519 O -0.1185(5) 0.5093(4) 0.0550(5) 0.1722 1.0000 Uani D U . . . .
O520 O 0.1121(8) 0.8252(7) -0.0887(4) 0.1168 1.0000 Uani D U . . . .
C521 C 0.0938(8) 0.7651(6) 0.0411(6) 0.0992 1.0000 Uani D U . . . .
C522 C 0.1272(6) 0.8055(5) 0.0129(5) 0.0977 1.0000 Uani D U . . . .
C523 C 0.0979(7) 0.7927(5) -0.0290(4) 0.1019 1.0000 Uani D U . . . .
C524 C 0.1347(7) 0.8336(5) -0.0513(4) 0.1048 1.0000 Uani D U . . . .
O525 O 0.1908(7) 0.8791(6) -0.0327(4) 0.1000 1.0000 Uani D U . . . .
C526 C 0.2192(7) 0.8913(6) 0.0078(4) 0.0992 1.0000 Uani D U . . . .
C527 C 0.1917(6) 0.8575(5) 0.0335(4) 0.0966 1.0000 Uani D U . . . .
C528 C 0.2235(7) 0.8729(5) 0.0746(4) 0.1002 1.0000 Uani D U . . . .
C529 C 0.2829(6) 0.9217(5) 0.0899(4) 0.1016 1.0000 Uani D U . . . .
C530 C 0.3104(6) 0.9553(5) 0.0642(4) 0.1074 1.0000 Uani D U . . . .
C531 C 0.2787(7) 0.9400(5) 0.0231(4) 0.1000 1.0000 Uani D U . . . .
O532 O 0.3711(6) 1.0052(5) 0.0800(5) 0.1249 1.0000 Uani D U . . . .
C533 C 0.4018(8) 1.0191(7) 0.1222(5) 0.1231 1.0000 Uani D U . . . .
Eu6 Eu -0.02120(10) 0.66615(7) 0.28802(5) 0.0897 1.0000 Uani D U . . . .
O601 O 0.1184(4) 0.6834(5) 0.3041(2) 0.0957 1.0000 Uani D U . . . .
N601 N 0.0221(7) 0.6026(4) 0.3351(3) 0.1011 1.0000 Uani D U . . . .
C601 C -0.0362(8) 0.5479(6) 0.3285(4) 0.1094 1.0000 Uani D U . . . .
C602 C -0.0676(9) 0.5205(4) 0.2829(4) 0.1062 1.0000 Uani D U . . . .
N602 N -0.1085(5) 0.5565(3) 0.2662(3) 0.1065 1.0000 Uani D U . . . .
O602 O 0.0256(8) 0.6022(5) 0.2308(2) 0.1055 1.0000 Uani D U . . . .
C603 C -0.1897(7) 0.5524(5) 0.2786(5) 0.1131 1.0000 Uani D U . . . .
N603 N -0.1760(4) 0.6580(5) 0.3027(3) 0.1062 1.0000 Uani D U . . . .
O603 O -0.0601(8) 0.7531(4) 0.2908(2) 0.1004 1.0000 Uani D U . . . .
C604 C -0.2231(6) 0.6023(5) 0.2769(5) 0.1132 1.0000 Uani D U . . . .
N604 N -0.0430(5) 0.7052(4) 0.3711(2) 0.0998 1.0000 Uani D U . . . .
C605 C -0.1863(6) 0.6683(6) 0.3478(3) 0.1091 1.0000 Uani D U . . . .
C606 C -0.1223(5) 0.7169(6) 0.3751(4) 0.1045 1.0000 Uani D U . . . .
C607 C -0.0300(10) 0.6660(7) 0.3948(4) 0.1053 1.0000 Uani D U . . . .
C608 C 0.0352(8) 0.6362(6) 0.3798(3) 0.1010 1.0000 Uani D U . . . .
O609 O 0.0707(10) 0.7273(7) 0.2525(6) 0.1001 1.0000 Uani D U . . . .
C611 C 0.0984(8) 0.5927(5) 0.3177(3) 0.0995 1.0000 Uani D U . . . .
C612 C 0.1507(5) 0.6478(5) 0.3139(2) 0.0951 1.0000 Uani D U . . . .
O613 O 0.2234(6) 0.6560(5) 0.3211(2) 0.0918 1.0000 Uani D U . . . .
C614 C -0.1062(8) 0.5430(7) 0.2195(4) 0.1165 1.0000 Uani D U . . . .
C615 C -0.0209(8) 0.5568(5) 0.2086(3) 0.1215 1.0000 Uani D U . . . .
O616 O 0.0001(10) 0.5223(5) 0.1783(3) 0.2096 1.0000 Uani D U . . . .
C617 C -0.1965(9) 0.7048(5) 0.2876(2) 0.1123 1.0000 Uani D U . . . .
C618 C -0.1313(8) 0.7572(4) 0.2897(2) 0.1106 1.0000 Uani D U . . . .
O619 O -0.1507(8) 0.8024(5) 0.2906(2) 0.1372 1.0000 Uani D U . . . .
O620 O 0.0473(6) 0.8316(7) 0.5394(4) 0.1326 1.0000 Uani D U . . . .
C621 C 0.0197(6) 0.7602(6) 0.3847(6) 0.1014 1.0000 Uani D U . . . .
C622 C 0.0129(5) 0.8027(5) 0.4293(5) 0.1005 1.0000 Uani D U . . . .
C623 C 0.0378(6) 0.7931(5) 0.4663(5) 0.1003 1.0000 Uani D U . . . .
C624 C 0.0269(5) 0.8364(5) 0.5047(5) 0.1082 1.0000 Uani D U . . . .
O625 O -0.0034(5) 0.8799(6) 0.5039(4) 0.1082 1.0000 Uani D U . . . .
C626 C -0.0263(5) 0.8876(6) 0.4671(5) 0.1091 1.0000 Uani D U . . . .
C627 C -0.0215(5) 0.8521(5) 0.4277(5) 0.1045 1.0000 Uani D U . . . .
C628 C -0.0468(6) 0.8642(5) 0.3923(5) 0.1066 1.0000 Uani D U . . . .
C629 C -0.0771(5) 0.9118(5) 0.3965(4) 0.1093 1.0000 Uani D U . . . .
C630 C -0.0819(5) 0.9472(5) 0.4359(5) 0.1138 1.0000 Uani D U . . . .
C631 C -0.0567(5) 0.9350(6) 0.4713(4) 0.1145 1.0000 Uani D U . . . .
O632 O -0.1129(5) 0.9957(5) 0.4407(5) 0.1190 1.0000 Uani D U . . . .
C633 C -0.1381(5) 1.0082(7) 0.4046(7) 0.1214 1.0000 Uani D U . . . .
Eu7 Eu 0.31165(10) 0.70743(7) 0.27672(5) 0.0815 1.0000 Uani D U . . . .
N701 N 0.3946(6) 0.8167(3) 0.2852(3) 0.0873 1.0000 Uani D U . . . .
C701 C 0.4633(8) 0.8154(5) 0.2594(5) 0.0962 1.0000 Uani D U . . . .
O701 O 0.2289(7) 0.7723(4) 0.2773(2) 0.0855 1.0000 Uani D U . . . .
O702 O 0.3340(7) 0.7063(3) 0.2057(2) 0.0916 1.0000 Uani D U . . . .
N702 N 0.4665(5) 0.7162(4) 0.2587(3) 0.0938 1.0000 Uani D U . . . .
C702 C 0.5125(6) 0.7762(4) 0.2671(5) 0.0949 1.0000 Uani D U . . . .
C703 C 0.5062(8) 0.6855(7) 0.2817(4) 0.0987 1.0000 Uani D U . . . .
N703 N 0.3997(6) 0.6755(5) 0.3303(3) 0.0968 1.0000 Uani D U . . . .
O703 O 0.3222(5) 0.6104(3) 0.2498(5) 0.1026 1.0000 Uani D U . . . .
C704 C 0.4854(6) 0.6948(6) 0.3266(4) 0.0997 1.0000 Uani D U . . . .
N704 N 0.3284(6) 0.7770(3) 0.3575(2) 0.0843 1.0000 Uani D U . . . .
C705 C 0.3784(10) 0.6989(6) 0.3735(3) 0.0934 1.0000 Uani D U . . . .
C706 C 0.3843(9) 0.7625(5) 0.3847(4) 0.0897 1.0000 Uani D U . . . .
C707 C 0.3550(9) 0.8379(4) 0.3586(4) 0.0895 1.0000 Uani D U . . . .
C708 C 0.4202(6) 0.8472(6) 0.3299(3) 0.0861 1.0000 Uani D U . . . .
O709 O 0.1995(9) 0.6470(8) 0.2238(5) 0.0974 1.0000 Uani D U . . . .
C711 C 0.3382(6) 0.8445(6) 0.2687(2) 0.0939 1.0000 Uani D U . . . .
C712 C 0.2514(6) 0.8223(4) 0.2739(2) 0.0932 1.0000 Uani D U . . . .
O713 O 0.2058(7) 0.8543(5) 0.2747(2) 0.1203 1.0000 Uani D U . . . .
C714 C 0.4615(8) 0.6868(3) 0.2121(4) 0.0953 1.0000 Uani D U . . . .
C715 C 0.3948(7) 0.6970(3) 0.1874(2) 0.0977 1.0000 Uani D U . . . .
O716 O 0.4031(7) 0.6959(3) 0.1501(3) 0.0914 1.0000 Uani D U . . . .
C717 C 0.3753(6) 0.6117(5) 0.3172(4) 0.1132 1.0000 Uani D U . . . .
C718 C 0.3481(5) 0.5825(3) 0.2712(4) 0.1264 1.0000 Uani D U . . . .
O719 O 0.3528(6) 0.5320(4) 0.2561(5) 0.1939 1.0000 Uani D U . . . .
O720 O 0.2612(5) 0.8338(6) 0.5277(4) 0.0929 1.0000 Uani D U . . . .
C721 C 0.2475(5) 0.7681(6) 0.3744(5) 0.0812 1.0000 Uani D U . . . .
C722 C 0.2356(5) 0.8122(5) 0.4173(4) 0.0750 1.0000 Uani D U . . . .
C723 C 0.2563(5) 0.8004(5) 0.4543(4) 0.0762 1.0000 Uani D U . . . .
C724 C 0.2445(5) 0.8417(5) 0.4936(4) 0.0835 1.0000 Uani D U . . . .
O725 O 0.2161(5) 0.8869(5) 0.4944(4) 0.0870 1.0000 Uani D U . . . .
C726 C 0.1968(5) 0.8974(5) 0.4581(4) 0.0817 1.0000 Uani D U . . . .
C727 C 0.2039(5) 0.8636(4) 0.4181(4) 0.0778 1.0000 Uani D U . . . .
C728 C 0.1820(5) 0.8779(5) 0.3832(4) 0.0760 1.0000 Uani D U . . . .
C729 C 0.1533(5) 0.9262(5) 0.3880(4) 0.0849 1.0000 Uani D U . . . .
C730 C 0.1464(5) 0.9600(4) 0.4277(4) 0.0911 1.0000 Uani D U . . . .
C731 C 0.1681(5) 0.9456(5) 0.4627(4) 0.0865 1.0000 Uani D U . . . .
O732 O 0.1173(5) 1.0094(4) 0.4329(5) 0.1027 1.0000 Uani D U . . . .
C733 C 0.0955(5) 1.0235(7) 0.3968(7) 0.1168 1.0000 Uani D U . . . .
Eu8 Eu 0.32646(10) 0.68974(7) 0.08774(5) 0.0853 1.0000 Uani D U . . . .
O801 O 0.1926(4) 0.6938(5) 0.0742(3) 0.0948 1.0000 Uani D U . . . .
N801 N 0.2512(6) 0.6201(4) 0.0127(3) 0.0941 1.0000 Uani D U . . . .
C801 C 0.2848(9) 0.5693(6) -0.0022(3) 0.0985 1.0000 Uani D U . . . .
C802 C 0.2993(9) 0.5442(4) 0.0330(4) 0.0953 1.0000 Uani D U . . . .
N802 N 0.3578(6) 0.5845(3) 0.0666(3) 0.0916 1.0000 Uani D U . . . .
O802 O 0.2458(7) 0.6252(4) 0.1200(2) 0.0933 1.0000 Uani D U . . . .
C803 C 0.4393(7) 0.5860(5) 0.0552(5) 0.0996 1.0000 Uani D U . . . .
N803 N 0.4804(4) 0.6923(4) 0.0738(4) 0.0943 1.0000 Uani D U . . . .
O803 O 0.4112(7) 0.7821(4) 0.1216(2) 0.0961 1.0000 Uani D U . . . .
C804 C 0.4985(7) 0.6397(5) 0.0786(6) 0.0989 1.0000 Uani D U . . . .
N804 N 0.3715(5) 0.7289(4) 0.0211(3) 0.1016 1.0000 Uani D U . . . .
C805 C 0.4955(7) 0.6998(7) 0.0320(3) 0.1031 1.0000 Uani D U . . . .
C806 C 0.4584(6) 0.7461(6) 0.0241(5) 0.1039 1.0000 Uani D U . . . .
C807 C 0.3390(8) 0.6871(6) -0.0196(3) 0.1107 1.0000 Uani D U . . . .
C808 C 0.2565(7) 0.6524(6) -0.0183(4) 0.1054 1.0000 Uani D U . . . .
O809 O 0.2660(10) 0.7440(7) 0.1494(4) 0.0941 1.0000 Uani D U . . . .
C811 C 0.1676(8) 0.6022(5) 0.0228(4) 0.0987 1.0000 Uani D U . . . .
C812 C 0.1422(5) 0.6547(5) 0.0484(3) 0.0988 1.0000 Uani D U . . . .
O813 O 0.0724(5) 0.6573(6) 0.0427(3) 0.1057 1.0000 Uani D U . . . .
C814 C 0.3451(7) 0.5710(7) 0.1075(2) 0.0987 1.0000 Uani D U . . . .
C815 C 0.2676(6) 0.5823(4) 0.1244(2) 0.1038 1.0000 Uani D U . . . .
O816 O 0.2282(8) 0.5481(5) 0.1416(3) 0.1506 1.0000 Uani D U . . . .
C817 C 0.5254(10) 0.7432(5) 0.1078(3) 0.1013 1.0000 Uani D U . . . .
C818 C 0.4859(7) 0.7919(3) 0.1258(2) 0.1086 1.0000 Uani D U . . . .
O819 O 0.5289(8) 0.8400(4) 0.1438(3) 0.1521 1.0000 Uani D U . . . .
O820 O 0.3428(9) 0.8369(7) -0.1016(4) 0.1467 1.0000 Uani D U . . . .
C821 C 0.3361(10) 0.7800(6) 0.0287(6) 0.1129 1.0000 Uani D U . . . .
C822 C 0.3686(8) 0.8185(5) -0.0009(5) 0.1196 1.0000 Uani D U . . . .
C823 C 0.3331(8) 0.8055(6) -0.0415(5) 0.1294 1.0000 Uani D U . . . .
C824 C 0.3704(8) 0.8448(6) -0.0651(5) 0.1299 1.0000 Uani D U . . . .
O825 O 0.4318(8) 0.8878(6) -0.0492(4) 0.1303 1.0000 Uani D U . . . .
C826 C 0.4642(8) 0.8989(6) -0.0095(4) 0.1232 1.0000 Uani D U . . . .
C827 C 0.4380(7) 0.8675(5) 0.0178(5) 0.1193 1.0000 Uani D U . . . .
C828 C 0.4753(8) 0.8823(6) 0.0577(5) 0.1262 1.0000 Uani D U . . . .
C829 C 0.5390(8) 0.9288(6) 0.0703(4) 0.1330 1.0000 Uani D U . . . .
C830 C 0.5652(7) 0.9603(5) 0.0429(5) 0.1375 1.0000 Uani D U . . . .
C831 C 0.5278(8) 0.9455(6) 0.0031(4) 0.1348 1.0000 Uani D U . . . .
O832 O 0.6304(7) 1.0077(5) 0.0557(6) 0.1458 1.0000 Uani D U . . . .
C833 C 0.6669(9) 1.0218(7) 0.0968(6) 0.1622 1.0000 Uani D U . . . .
H1011 H 1.0067 0.7966 0.6740 0.1098 1.0000 Uiso R . . . . .
H1012 H 0.9436 0.7526 0.6880 0.1098 1.0000 Uiso R . . . . .
H1021 H 1.0375 0.7094 0.6538 0.1086 1.0000 Uiso R . . . . .
H1022 H 1.0202 0.7269 0.6140 0.1086 1.0000 Uiso R . . . . .
H1031 H 1.0174 0.6258 0.5895 0.1063 1.0000 Uiso R . . . . .
H1032 H 0.9342 0.5849 0.5814 0.1063 1.0000 Uiso R . . . . .
H1041 H 0.9784 0.6768 0.5477 0.1036 1.0000 Uiso R . . . . .
H1042 H 0.9683 0.6134 0.5222 0.1036 1.0000 Uiso R . . . . .
H1051 H 0.8870 0.6518 0.4801 0.0981 1.0000 Uiso R . . . . .
H1052 H 0.8012 0.6527 0.4914 0.0981 1.0000 Uiso R . . . . .
H1061 H 0.9346 0.7390 0.5305 0.0990 1.0000 Uiso R . . . . .
H1062 H 0.8743 0.7443 0.4979 0.0990 1.0000 Uiso R . . . . .
H1071 H 0.8331 0.8266 0.5941 0.1027 1.0000 Uiso R . . . . .
H1072 H 0.8960 0.8288 0.5617 0.1027 1.0000 Uiso R . . . . .
H1081 H 0.9580 0.8465 0.6271 0.1074 1.0000 Uiso R . . . . .
H1082 H 0.9727 0.7904 0.5977 0.1074 1.0000 Uiso R . . . . .
H1111 H 0.8697 0.8094 0.7000 0.1122 1.0000 Uiso R . . . . .
H1112 H 0.8734 0.8497 0.6719 0.1122 1.0000 Uiso R . . . . .
H1142 H 0.9728 0.6376 0.6711 0.1070 1.0000 Uiso R . . . . .
H1141 H 0.9019 0.5933 0.6433 0.1070 1.0000 Uiso R . . . . .
H1171 H 0.8542 0.5516 0.5014 0.0993 1.0000 Uiso R . . . . .
H1172 H 0.7746 0.5699 0.5030 0.0993 1.0000 Uiso R . . . . .
H1211 H 0.7228 0.7641 0.5567 0.0992 1.0000 Uiso R . . . . .
H1212 H 0.7295 0.7145 0.5179 0.0992 1.0000 Uiso R . . . . .
H1231 H 0.7868 0.7450 0.4521 0.1078 1.0000 Uiso R . . . . .
H1281 H 0.7008 0.8412 0.5875 0.1056 1.0000 Uiso R . . . . .
H1291 H 0.6585 0.9258 0.6102 0.1109 1.0000 Uiso R . . . . .
H1311 H 0.6891 0.9510 0.4961 0.1177 1.0000 Uiso R . . . . .
H1333 H 0.6064 1.0486 0.6174 0.1330 1.0000 Uiso R . . . . .
H1332 H 0.6674 1.0177 0.6291 0.1330 1.0000 Uiso R . . . . .
H1331 H 0.5809 0.9843 0.6142 0.1330 1.0000 Uiso R . . . . .
H2011 H 0.8147 0.5678 0.8540 0.1242 1.0000 Uiso R . . . . .
H2012 H 0.7283 0.5323 0.8493 0.1242 1.0000 Uiso R . . . . .
H2021 H 0.7962 0.4919 0.7952 0.1249 1.0000 Uiso R . . . . .
H2022 H 0.7272 0.5102 0.7770 0.1249 1.0000 Uiso R . . . . .
H2031 H 0.9208 0.5552 0.8109 0.1252 1.0000 Uiso R . . . . .
H2032 H 0.9258 0.5232 0.7642 0.1252 1.0000 Uiso R . . . . .
H2041 H 1.0271 0.6036 0.7879 0.1206 1.0000 Uiso R . . . . .
H2042 H 0.9773 0.6049 0.7493 0.1206 1.0000 Uiso R . . . . .
H2051 H 1.0413 0.6852 0.8526 0.1186 1.0000 Uiso R . . . . .
H2052 H 0.9629 0.6440 0.8564 0.1186 1.0000 Uiso R . . . . .
H2061 H 0.9709 0.7352 0.9013 0.1144 1.0000 Uiso R . . . . .
H2062 H 0.9748 0.7587 0.8627 0.1144 1.0000 Uiso R . . . . .
H2071 H 0.8354 0.7035 0.9237 0.1168 1.0000 Uiso R . . . . .
H2072 H 0.8627 0.6513 0.8961 0.1168 1.0000 Uiso R . . . . .
H2081 H 0.7293 0.6255 0.9019 0.1171 1.0000 Uiso R . . . . .
H2082 H 0.7181 0.6739 0.8836 0.1171 1.0000 Uiso R . . . . .
H2111 H 0.6189 0.5807 0.8448 0.1181 1.0000 Uiso R . . . . .
H2112 H 0.6417 0.5607 0.7990 0.1181 1.0000 Uiso R . . . . .
H2141 H 0.8569 0.5523 0.7118 0.1196 1.0000 Uiso R . . . . .
H2142 H 0.8049 0.4962 0.7168 0.1196 1.0000 Uiso R . . . . .
H2171 H 1.0609 0.7240 0.8027 0.1153 1.0000 Uiso R . . . . .
H2172 H 1.0242 0.6912 0.7574 0.1153 1.0000 Uiso R . . . . .
H2211 H 0.8617 0.7901 0.8615 0.1098 1.0000 Uiso R . . . . .
H2212 H 0.7821 0.7595 0.8739 0.1098 1.0000 Uiso R . . . . .
H2231 H 0.7940 0.7689 0.9615 0.1105 1.0000 Uiso R . . . . .
H2281 H 0.9515 0.8459 0.8617 0.1194 1.0000 Uiso R . . . . .
H2291 H 1.0548 0.9261 0.8705 0.1310 1.0000 Uiso R . . . . .
H2311 H 1.0418 0.9659 0.9961 0.1332 1.0000 Uiso R . . . . .
H2331 H 1.1965 1.0468 0.9103 0.1646 1.0000 Uiso R . . . . .
H2332 H 1.1747 0.9814 0.8895 0.1646 1.0000 Uiso R . . . . .
H2333 H 1.1144 1.0173 0.8861 0.1646 1.0000 Uiso R . . . . .
H3011 H 0.3867 0.8215 0.7531 0.1118 1.0000 Uiso R . . . . .
H3012 H 0.4113 0.7726 0.7199 0.1118 1.0000 Uiso R . . . . .
H3021 H 0.3200 0.7571 0.7859 0.1147 1.0000 Uiso R . . . . .
H3022 H 0.2865 0.7408 0.7395 0.1147 1.0000 Uiso R . . . . .
H3031 H 0.2398 0.6581 0.7691 0.1237 1.0000 Uiso R . . . . .
H3032 H 0.2897 0.6127 0.7599 0.1237 1.0000 Uiso R . . . . .
H3041 H 0.3214 0.7068 0.8305 0.1219 1.0000 Uiso R . . . . .
H3042 H 0.2791 0.6463 0.8318 0.1219 1.0000 Uiso R . . . . .
H3051 H 0.3889 0.6763 0.8879 0.1145 1.0000 Uiso R . . . . .
H3052 H 0.4718 0.6686 0.8748 0.1145 1.0000 Uiso R . . . . .
H3061 H 0.4772 0.7636 0.9071 0.1053 1.0000 Uiso R . . . . .
H3062 H 0.4136 0.7629 0.8738 0.1053 1.0000 Uiso R . . . . .
H3071 H 0.5205 0.8458 0.8777 0.1013 1.0000 Uiso R . . . . .
H3072 H 0.5778 0.8372 0.8424 0.1013 1.0000 Uiso R . . . . .
H3081 H 0.4724 0.8661 0.8201 0.1045 1.0000 Uiso R . . . . .
H3082 H 0.4151 0.8134 0.8274 0.1045 1.0000 Uiso R . . . . .
H3111 H 0.5500 0.8650 0.7702 0.1084 1.0000 Uiso R . . . . .
H3112 H 0.5327 0.8157 0.7287 0.1084 1.0000 Uiso R . . . . .
H3141 H 0.2906 0.6629 0.6914 0.1151 1.0000 Uiso R . . . . .
H3142 H 0.3291 0.6164 0.6995 0.1151 1.0000 Uiso R . . . . .
H3171 H 0.4079 0.5835 0.8392 0.1305 1.0000 Uiso R . . . . .
H3172 H 0.3319 0.5736 0.8106 0.1305 1.0000 Uiso R . . . . .
H3211 H 0.5929 0.7222 0.8716 0.0992 1.0000 Uiso R . . . . .
H3212 H 0.6375 0.7684 0.8521 0.0992 1.0000 Uiso R . . . . .
H3231 H 0.5664 0.7595 0.9509 0.0992 1.0000 Uiso R . . . . .
H3281 H 0.7108 0.8454 0.8521 0.0917 1.0000 Uiso R . . . . .
H3291 H 0.8101 0.9281 0.8611 0.0974 1.0000 Uiso R . . . . .
H3311 H 0.8041 0.9629 0.9870 0.1012 1.0000 Uiso R . . . . .
H3333 H 0.9467 1.0506 0.9005 0.1312 1.0000 Uiso R . . . . .
H3332 H 0.8641 1.0197 0.8773 0.1312 1.0000 Uiso R . . . . .
H3331 H 0.9277 0.9855 0.8784 0.1312 1.0000 Uiso R . . . . .
H4011 H 0.3830 0.5832 0.4762 0.0906 1.0000 Uiso R . . . . .
H4012 H 0.4408 0.5435 0.4642 0.0906 1.0000 Uiso R . . . . .
H4021 H 0.4324 0.5265 0.5293 0.0917 1.0000 Uiso R . . . . .
H4022 H 0.3494 0.5083 0.5052 0.0917 1.0000 Uiso R . . . . .
H4031 H 0.2462 0.5505 0.5479 0.0928 1.0000 Uiso R . . . . .
H4032 H 0.2784 0.5836 0.5163 0.0928 1.0000 Uiso R . . . . .
H4041 H 0.2612 0.6340 0.6003 0.0960 1.0000 Uiso R . . . . .
H4042 H 0.2099 0.6362 0.5626 0.0960 1.0000 Uiso R . . . . .
H4051 H 0.2571 0.7159 0.5317 0.0935 1.0000 Uiso R . . . . .
H4052 H 0.2997 0.6695 0.5085 0.0935 1.0000 Uiso R . . . . .
H4061 H 0.3786 0.7824 0.5486 0.0922 1.0000 Uiso R . . . . .
H4062 H 0.3610 0.7576 0.5003 0.0922 1.0000 Uiso R . . . . .
H4071 H 0.4684 0.7176 0.4616 0.0909 1.0000 Uiso R . . . . .
H4072 H 0.4010 0.6697 0.4683 0.0909 1.0000 Uiso R . . . . .
H4081 H 0.5604 0.6795 0.4849 0.0905 1.0000 Uiso R . . . . .
H4082 H 0.5070 0.6324 0.4486 0.0905 1.0000 Uiso R . . . . .
H4111 H 0.5494 0.5658 0.5230 0.0921 1.0000 Uiso R . . . . .
H4112 H 0.5866 0.5855 0.4859 0.0921 1.0000 Uiso R . . . . .
H4141 H 0.3337 0.5753 0.6125 0.0958 1.0000 Uiso R . . . . .
H4142 H 0.3467 0.5176 0.5850 0.0958 1.0000 Uiso R . . . . .
H4171 H 0.2860 0.7225 0.6296 0.1042 1.0000 Uiso R . . . . .
H4172 H 0.2650 0.7541 0.5985 0.1042 1.0000 Uiso R . . . . .
H4211 H 0.5106 0.8067 0.5587 0.0971 1.0000 Uiso R . . . . .
H4212 H 0.5653 0.7705 0.5339 0.0971 1.0000 Uiso R . . . . .
H4231 H 0.5719 0.7761 0.4498 0.1077 1.0000 Uiso R . . . . .
H4281 H 0.4477 0.8578 0.5747 0.1089 1.0000 Uiso R . . . . .
H4291 H 0.3899 0.9357 0.5937 0.1157 1.0000 Uiso R . . . . .
H4311 H 0.4386 0.9672 0.4831 0.1181 1.0000 Uiso R . . . . .
H4332 H 0.3201 1.0509 0.5965 0.1450 1.0000 Uiso R . . . . .
H4333 H 0.3836 1.0252 0.6122 0.1450 1.0000 Uiso R . . . . .
H4331 H 0.3022 0.9863 0.5922 0.1450 1.0000 Uiso R . . . . .
H5011 H -0.1285 0.8158 0.1772 0.1191 1.0000 Uiso R . . . . .
H5012 H -0.0957 0.7709 0.1915 0.1191 1.0000 Uiso R . . . . .
H5021 H -0.1918 0.7460 0.1192 0.1228 1.0000 Uiso R . . . . .
H5022 H -0.2193 0.7288 0.1590 0.1228 1.0000 Uiso R . . . . .
H5031 H -0.2576 0.6483 0.0914 0.1269 1.0000 Uiso R . . . . .
H5032 H -0.2054 0.6045 0.0854 0.1269 1.0000 Uiso R . . . . .
H5041 H -0.1813 0.6953 0.0499 0.1263 1.0000 Uiso R . . . . .
H5042 H -0.2156 0.6319 0.0252 0.1263 1.0000 Uiso R . . . . .
H5051 H -0.1058 0.6642 -0.0172 0.1221 1.0000 Uiso R . . . . .
H5052 H -0.0208 0.6648 -0.0022 0.1221 1.0000 Uiso R . . . . .
H5061 H -0.0291 0.7560 0.0001 0.1170 1.0000 Uiso R . . . . .
H5062 H -0.0952 0.7528 0.0307 0.1170 1.0000 Uiso R . . . . .
H5071 H -0.0022 0.8413 0.0632 0.1094 1.0000 Uiso R . . . . .
H5072 H 0.0610 0.8415 0.0966 0.1094 1.0000 Uiso R . . . . .
H5081 H -0.0488 0.8623 0.1286 0.1118 1.0000 Uiso R . . . . .
H5082 H -0.1021 0.8064 0.0997 0.1118 1.0000 Uiso R . . . . .
H5111 H 0.0335 0.8669 0.1794 0.1129 1.0000 Uiso R . . . . .
H5112 H 0.0225 0.8189 0.2012 0.1129 1.0000 Uiso R . . . . .
H5141 H -0.2015 0.6546 0.1733 0.1223 1.0000 Uiso R . . . . .
H5142 H -0.1637 0.6089 0.1445 0.1223 1.0000 Uiso R . . . . .
H5171 H -0.1473 0.5667 0.0099 0.1289 1.0000 Uiso R . . . . .
H5172 H -0.0563 0.5828 0.0088 0.1289 1.0000 Uiso R . . . . .
H5211 H 0.1314 0.7785 0.0648 0.1090 1.0000 Uiso R . . . . .
H5212 H 0.0946 0.7270 0.0264 0.1090 1.0000 Uiso R . . . . .
H5231 H 0.0573 0.7599 -0.0421 0.1080 1.0000 Uiso R . . . . .
H5281 H 0.2053 0.8504 0.0927 0.1056 1.0000 Uiso R . . . . .
H5291 H 0.3055 0.9330 0.1180 0.1093 1.0000 Uiso R . . . . .
H5311 H 0.2970 0.9625 0.0049 0.1064 1.0000 Uiso R . . . . .
H5331 H 0.4421 1.0533 0.1297 0.1315 1.0000 Uiso R . . . . .
H5333 H 0.3597 1.0236 0.1397 0.1315 1.0000 Uiso R . . . . .
H5332 H 0.4227 0.9887 0.1256 0.1315 1.0000 Uiso R . . . . .
H6012 H -0.0784 0.5544 0.3456 0.1206 1.0000 Uiso R . . . . .
H6011 H -0.0106 0.5228 0.3372 0.1206 1.0000 Uiso R . . . . .
H6022 H -0.1039 0.4855 0.2812 0.1213 1.0000 Uiso R . . . . .
H6021 H -0.0256 0.5134 0.2658 0.1213 1.0000 Uiso R . . . . .
H6031 H -0.1895 0.5503 0.3067 0.1251 1.0000 Uiso R . . . . .
H6032 H -0.2223 0.5184 0.2606 0.1251 1.0000 Uiso R . . . . .
H6041 H -0.2740 0.5968 0.2871 0.1253 1.0000 Uiso R . . . . .
H6042 H -0.2275 0.6025 0.2485 0.1253 1.0000 Uiso R . . . . .
H6051 H -0.2357 0.6781 0.3529 0.1202 1.0000 Uiso R . . . . .
H6052 H -0.1867 0.6343 0.3551 0.1202 1.0000 Uiso R . . . . .
H6061 H -0.1225 0.7510 0.3682 0.1137 1.0000 Uiso R . . . . .
H6062 H -0.1330 0.7216 0.4037 0.1137 1.0000 Uiso R . . . . .
H6071 H -0.0173 0.6873 0.4234 0.1146 1.0000 Uiso R . . . . .
H6072 H -0.0769 0.6371 0.3922 0.1146 1.0000 Uiso R . . . . .
H6081 H 0.0825 0.6650 0.3834 0.1122 1.0000 Uiso R . . . . .
H6082 H 0.0409 0.6116 0.3961 0.1122 1.0000 Uiso R . . . . .
H6111 H 0.1252 0.5798 0.3368 0.1120 1.0000 Uiso R . . . . .
H6112 H 0.0884 0.5646 0.2912 0.1120 1.0000 Uiso R . . . . .
H6141 H -0.1373 0.5640 0.2096 0.1263 1.0000 Uiso R . . . . .
H6142 H -0.1279 0.5034 0.2073 0.1263 1.0000 Uiso R . . . . .
H6171 H -0.2360 0.7178 0.3044 0.1215 1.0000 Uiso R . . . . .
H6172 H -0.2178 0.6882 0.2593 0.1215 1.0000 Uiso R . . . . .
H6211 H 0.0157 0.7813 0.3654 0.1117 1.0000 Uiso R . . . . .
H6212 H 0.0699 0.7512 0.3840 0.1117 1.0000 Uiso R . . . . .
H6231 H 0.0594 0.7618 0.4669 0.1121 1.0000 Uiso R . . . . .
H6281 H -0.0438 0.8400 0.3651 0.1142 1.0000 Uiso R . . . . .
H6291 H -0.0947 0.9203 0.3724 0.1173 1.0000 Uiso R . . . . .
H6311 H -0.0596 0.9592 0.4986 0.1169 1.0000 Uiso R . . . . .
H6332 H -0.1577 1.0417 0.4107 0.1247 1.0000 Uiso R . . . . .
H6333 H -0.0944 1.0123 0.3880 0.1247 1.0000 Uiso R . . . . .
H6331 H -0.1785 0.9764 0.3895 0.1247 1.0000 Uiso R . . . . .
H7012 H 0.4957 0.8529 0.2655 0.1001 1.0000 Uiso R . . . . .
H7011 H 0.4443 0.8024 0.2306 0.1001 1.0000 Uiso R . . . . .
H7022 H 0.5319 0.7894 0.2958 0.1013 1.0000 Uiso R . . . . .
H7021 H 0.5556 0.7772 0.2499 0.1013 1.0000 Uiso R . . . . .
H7032 H 0.5618 0.6980 0.2814 0.1081 1.0000 Uiso R . . . . .
H7031 H 0.4900 0.6460 0.2673 0.1081 1.0000 Uiso R . . . . .
H7042 H 0.5023 0.7342 0.3412 0.1082 1.0000 Uiso R . . . . .
H7041 H 0.5124 0.6738 0.3392 0.1082 1.0000 Uiso R . . . . .
H7051 H 0.4137 0.6918 0.3923 0.1063 1.0000 Uiso R . . . . .
H7052 H 0.3258 0.6805 0.3764 0.1063 1.0000 Uiso R . . . . .
H7061 H 0.3734 0.7760 0.4132 0.1029 1.0000 Uiso R . . . . .
H7062 H 0.4366 0.7808 0.3811 0.1029 1.0000 Uiso R . . . . .
H7071 H 0.3740 0.8597 0.3865 0.0977 1.0000 Uiso R . . . . .
H7072 H 0.3107 0.8498 0.3502 0.0977 1.0000 Uiso R . . . . .
H7081 H 0.4356 0.8869 0.3327 0.0951 1.0000 Uiso R . . . . .
H7082 H 0.4642 0.8348 0.3380 0.0951 1.0000 Uiso R . . . . .
H7111 H 0.3526 0.8841 0.2830 0.0989 1.0000 Uiso R . . . . .
H7112 H 0.3436 0.8388 0.2396 0.0989 1.0000 Uiso R . . . . .
H7141 H 0.5101 0.7013 0.2019 0.1027 1.0000 Uiso R . . . . .
H7142 H 0.4541 0.6469 0.2074 0.1027 1.0000 Uiso R . . . . .
H7171 H 0.3453 0.6017 0.3388 0.1200 1.0000 Uiso R . . . . .
H7172 H 0.4225 0.5986 0.3164 0.1200 1.0000 Uiso R . . . . .
H7211 H 0.2098 0.7696 0.3541 0.0963 1.0000 Uiso R . . . . .
H7212 H 0.2363 0.7310 0.3780 0.0963 1.0000 Uiso R . . . . .
H7231 H 0.2764 0.7681 0.4539 0.0928 1.0000 Uiso R . . . . .
H7281 H 0.1866 0.8552 0.3557 0.0882 1.0000 Uiso R . . . . .
H7291 H 0.1384 0.9368 0.3642 0.0930 1.0000 Uiso R . . . . .
H7311 H 0.1634 0.9683 0.4902 0.0947 1.0000 Uiso R . . . . .
H7331 H 0.0766 1.0573 0.4034 0.1229 1.0000 Uiso R . . . . .
H7333 H 0.1408 1.0283 0.3814 0.1229 1.0000 Uiso R . . . . .
H7332 H 0.0555 0.9926 0.3803 0.1229 1.0000 Uiso R . . . . .
H8012 H 0.3330 0.5796 -0.0142 0.1056 1.0000 Uiso R . . . . .
H8011 H 0.2480 0.5412 -0.0230 0.1056 1.0000 Uiso R . . . . .
H8022 H 0.2513 0.5344 0.0453 0.1029 1.0000 Uiso R . . . . .
H8021 H 0.3183 0.5109 0.0216 0.1029 1.0000 Uiso R . . . . .
H8032 H 0.4397 0.5815 0.0259 0.1033 1.0000 Uiso R . . . . .
H8031 H 0.4542 0.5547 0.0613 0.1033 1.0000 Uiso R . . . . .
H8042 H 0.5479 0.6375 0.0673 0.1056 1.0000 Uiso R . . . . .
H8041 H 0.5028 0.6418 0.1075 0.1056 1.0000 Uiso R . . . . .
H8052 H 0.5511 0.7118 0.0315 0.1109 1.0000 Uiso R . . . . .
H8051 H 0.4763 0.6649 0.0107 0.1109 1.0000 Uiso R . . . . .
H8062 H 0.4756 0.7805 0.0462 0.1119 1.0000 Uiso R . . . . .
H8061 H 0.4739 0.7525 -0.0018 0.1119 1.0000 Uiso R . . . . .
H8071 H 0.3378 0.7073 -0.0397 0.1161 1.0000 Uiso R . . . . .
H8072 H 0.3726 0.6616 -0.0277 0.1161 1.0000 Uiso R . . . . .
H8081 H 0.2222 0.6777 -0.0116 0.1116 1.0000 Uiso R . . . . .
H8082 H 0.2399 0.6261 -0.0452 0.1116 1.0000 Uiso R . . . . .
H8111 H 0.1351 0.5861 -0.0028 0.1055 1.0000 Uiso R . . . . .
H8112 H 0.1626 0.5749 0.0381 0.1055 1.0000 Uiso R . . . . .
H8141 H 0.3877 0.5941 0.1272 0.1041 1.0000 Uiso R . . . . .
H8142 H 0.3444 0.5320 0.1034 0.1041 1.0000 Uiso R . . . . .
H8171 H 0.5726 0.7586 0.0969 0.1125 1.0000 Uiso R . . . . .
H8172 H 0.5383 0.7292 0.1302 0.1125 1.0000 Uiso R . . . . .
H8211 H 0.3504 0.8031 0.0568 0.1185 1.0000 Uiso R . . . . .
H8212 H 0.2803 0.7673 0.0243 0.1185 1.0000 Uiso R . . . . .
H8231 H 0.2892 0.7742 -0.0527 0.1254 1.0000 Uiso R . . . . .
H8281 H 0.4576 0.8605 0.0764 0.1231 1.0000 Uiso R . . . . .
H8291 H 0.5649 0.9392 0.0976 0.1288 1.0000 Uiso R . . . . .
H8311 H 0.5454 0.9674 -0.0156 0.1286 1.0000 Uiso R . . . . .
H8331 H 0.7099 1.0543 0.1029 0.1590 1.0000 Uiso R . . . . .
H8332 H 0.6281 1.0288 0.1161 0.1590 1.0000 Uiso R . . . . .
H8333 H 0.6851 0.9898 0.0991 0.1590 1.0000 Uiso R . . . . .
H1092 H 0.6789 0.6061 0.6437 0.1006 1.0000 Uiso R . . . . .
H1091 H 0.6169 0.6243 0.6214 0.1006 1.0000 Uiso R . . . . .
H2092 H 0.7778 0.7051 0.7201 0.1095 1.0000 Uiso R . . . . .
H2091 H 0.7375 0.7541 0.7526 0.1095 1.0000 Uiso R . . . . .
H3092 H 0.6270 0.6242 0.7274 0.1106 1.0000 Uiso R . . . . .
H3091 H 0.5482 0.6145 0.6998 0.1106 1.0000 Uiso R . . . . .
H4092 H 0.6144 0.7584 0.6578 0.0955 1.0000 Uiso R . . . . .
H4091 H 0.5367 0.7191 0.6637 0.0955 1.0000 Uiso R . . . . .
H5092 H 0.0680 0.6162 0.1486 0.1216 1.0000 Uiso R . . . . .
H5091 H 0.1422 0.6398 0.1331 0.1216 1.0000 Uiso R . . . . .
H6092 H 0.0807 0.7368 0.2270 0.1116 1.0000 Uiso R . . . . .
H6091 H 0.1250 0.7430 0.2618 0.1116 1.0000 Uiso R . . . . .
H7092 H 0.1448 0.6324 0.2254 0.1024 1.0000 Uiso R . . . . .
H7091 H 0.2091 0.6179 0.2006 0.1024 1.0000 Uiso R . . . . .
H8092 H 0.2169 0.7530 0.1449 0.1041 1.0000 Uiso R . . . . .
H8091 H 0.2575 0.7510 0.1783 0.1041 1.0000 Uiso R . . . . .

_refine_ls_extinction_method     None
_oxford_refine_ls_scale          0.05342(12)
loop_
_geom_bond_atom_site_label_1
_geom_bond_site_symmetry_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_2
_geom_bond_distance
_geom_bond_publ_flag
Eu1 . O101 . 2.402(7) yes
Eu1 . N101 . 2.728(6) yes
Eu1 . O102 . 2.412(7) yes
Eu1 . N102 . 2.736(6) yes
Eu1 . O103 . 2.411(7) yes
Eu1 . N103 . 2.725(6) yes
Eu1 . N104 . 2.737(6) yes
Eu1 . O109 . 2.519(7) yes
Eu1 . O413 . 2.394(11) yes
C101 . N101 . 1.477(6) yes
C101 . C102 . 1.514(7) yes
C101 . H1011 . 0.950 no
C101 . H1012 . 0.950 no
O101 . C112 . 1.266(5) yes
N101 . C108 . 1.481(7) yes
N101 . C111 . 1.502(7) yes
C102 . N102 . 1.484(7) yes
C102 . H1021 . 0.950 no
C102 . H1022 . 0.950 no
O102 . C115 . 1.270(5) yes
N102 . C103 . 1.487(7) yes
N102 . C114 . 1.504(7) yes
C103 . C104 . 1.517(7) yes
C103 . H1031 . 0.950 no
C103 . H1032 . 0.950 no
O103 . C118 . 1.268(5) yes
N103 . C104 . 1.485(7) yes
N103 . C105 . 1.478(7) yes
N103 . C117 . 1.497(7) yes
C104 . H1041 . 0.950 no
C104 . H1042 . 0.950 no
N104 . C106 . 1.487(7) yes
N104 . C107 . 1.483(7) yes
N104 . C121 . 1.513(6) yes
C105 . C106 . 1.521(7) yes
C105 . H1051 . 0.950 no
C105 . H1052 . 0.950 no
C106 . H1061 . 0.950 no
C106 . H1062 . 0.950 no
C107 . C108 . 1.513(7) yes
C107 . H1071 . 0.950 no
C107 . H1072 . 0.950 no
C108 . H1081 . 0.950 no
C108 . H1082 . 0.950 no
O109 . H1092 . 0.950 no
O109 . H1091 . 0.950 no
C111 . C112 . 1.522(5) yes
C111 . H1111 . 0.950 no
C111 . H1112 . 0.950 no
C112 . O113 . 1.251(5) yes
C114 . C115 . 1.520(5) yes
C114 . H1142 . 0.950 no
C114 . H1141 . 0.950 no
C115 . O116 . 1.252(5) yes
O116 . Eu2 . 2.338(11) yes
C117 . C118 . 1.520(5) yes
C117 . H1171 . 0.950 no
C117 . H1172 . 0.950 no
C118 . O119 . 1.249(5) yes
O120 . C124 . 1.256(7) yes
C121 . C122 . 1.588(7) yes
C121 . H1211 . 0.950 no
C121 . H1212 . 0.950 no
C122 . C123 . 1.399(7) yes
C122 . C127 . 1.506(7) yes
C123 . C124 . 1.480(7) yes
C123 . H1231 . 0.950 no
C124 . O125 . 1.329(7) yes
O125 . C126 . 1.358(7) yes
C126 . C127 . 1.382(6) yes
C126 . C131 . 1.382(6) yes
C127 . C128 . 1.383(6) yes
C128 . C129 . 1.385(6) yes
C128 . H1281 . 0.950 no
C129 . C130 . 1.382(6) yes
C129 . H1291 . 0.950 no
C130 . C131 . 1.383(6) yes
C130 . O132 . 1.413(5) yes
C131 . H1311 . 0.950 no
O132 . C133 . 1.413(5) yes
C133 . H1333 . 0.950 no
C133 . H1332 . 0.950 no
C133 . H1331 . 0.950 no
Eu2 . O201 . 2.401(7) yes
Eu2 . N201 . 2.743(7) yes
Eu2 . O202 . 2.411(7) yes
Eu2 . N202 . 2.719(6) yes
Eu2 . O203 . 2.419(7) yes
Eu2 . N203 . 2.719(6) yes
Eu2 . N204 . 2.724(6) yes
Eu2 . O209 . 2.515(7) yes
C201 . N201 . 1.485(7) yes
C201 . C202 . 1.509(7) yes
C201 . H2011 . 0.950 no
C201 . H2012 . 0.950 no
O201 . C212 . 1.267(5) yes
N201 . C208 . 1.481(7) yes
N201 . C211 . 1.502(7) yes
C202 . N202 . 1.481(6) yes
C202 . H2021 . 0.950 no
C202 . H2022 . 0.950 no
O202 . C215 . 1.269(5) yes
N202 . C203 . 1.469(7) yes
N202 . C214 . 1.501(7) yes
C203 . C204 . 1.502(7) yes
C203 . H2031 . 0.950 no
C203 . H2032 . 0.950 no
O203 . C218 . 1.271(5) yes
N203 . C204 . 1.470(6) yes
N203 . C205 . 1.478(7) yes
N203 . C217 . 1.504(7) yes
C204 . H2041 . 0.950 no
C204 . H2042 . 0.950 no
N204 . C206 . 1.478(7) yes
N204 . C207 . 1.474(7) yes
N204 . C221 . 1.510(6) yes
C205 . C206 . 1.525(7) yes
C205 . H2051 . 0.950 no
C205 . H2052 . 0.950 no
C206 . H2061 . 0.950 no
C206 . H2062 . 0.950 no
C207 . C208 . 1.508(7) yes
C207 . H2071 . 0.950 no
C207 . H2072 . 0.950 no
C208 . H2081 . 0.950 no
C208 . H2082 . 0.950 no
O209 . H2092 . 0.950 no
O209 . H2091 . 0.950 no
C211 . C212 . 1.520(5) yes
C211 . H2111 . 0.950 no
C211 . H2112 . 0.950 no
C212 . O213 . 1.248(5) yes
O213 . Eu3 . 2.351(12) yes
C214 . C215 . 1.525(5) yes
C214 . H2141 . 0.950 no
C214 . H2142 . 0.950 no
C215 . O216 . 1.251(5) yes
C217 . C218 . 1.519(5) yes
C217 . H2171 . 0.950 no
C217 . H2172 . 0.950 no
C218 . O219 . 1.251(5) yes
O220 . C224 . 1.251(7) yes
C221 . C222 . 1.592(7) yes
C221 . H2211 . 0.950 no
C221 . H2212 . 0.950 no
C222 . C223 . 1.405(7) yes
C222 . C227 . 1.508(7) yes
C223 . C224 . 1.477(7) yes
C223 . H2231 . 0.950 no
C224 . O225 . 1.326(7) yes
O225 . C226 . 1.357(7) yes
C226 . C227 . 1.385(6) yes
C226 . C231 . 1.379(6) yes
C227 . C228 . 1.385(6) yes
C228 . C229 . 1.382(6) yes
C228 . H2281 . 0.950 no
C229 . C230 . 1.382(6) yes
C229 . H2291 . 0.950 no
C230 . C231 . 1.383(6) yes
C230 . O232 . 1.413(5) yes
C231 . H2311 . 0.950 no
O232 . C233 . 1.412(5) yes
C233 . H2331 . 0.950 no
C233 . H2332 . 0.950 no
C233 . H2333 . 0.950 no
Eu3 . O301 . 2.409(7) yes
Eu3 . N301 . 2.723(7) yes
Eu3 . O302 . 2.401(7) yes
Eu3 . N302 . 2.727(6) yes
Eu3 . O303 . 2.402(6) yes
Eu3 . N303 . 2.725(7) yes
Eu3 . N304 . 2.738(6) yes
Eu3 . O309 . 2.518(7) yes
C301 . N301 . 1.481(7) yes
C301 . C302 . 1.513(7) yes
C301 . H3011 . 0.950 no
C301 . H3012 . 0.950 no
O301 . C312 . 1.267(5) yes
N301 . C308 . 1.479(7) yes
N301 . C311 . 1.509(7) yes
C302 . N302 . 1.481(7) yes
C302 . H3021 . 0.950 no
C302 . H3022 . 0.950 no
O302 . C315 . 1.265(5) yes
N302 . C303 . 1.483(7) yes
N302 . C314 . 1.503(7) yes
C303 . C304 . 1.516(7) yes
C303 . H3031 . 0.950 no
C303 . H3032 . 0.950 no
O303 . C318 . 1.266(5) yes
N303 . C304 . 1.481(7) yes
N303 . C305 . 1.483(7) yes
N303 . C317 . 1.504(7) yes
C304 . H3041 . 0.950 no
C304 . H3042 . 0.950 no
N304 . C306 . 1.489(7) yes
N304 . C307 . 1.485(7) yes
N304 . C321 . 1.515(6) yes
C305 . C306 . 1.514(7) yes
C305 . H3051 . 0.950 no
C305 . H3052 . 0.950 no
C306 . H3061 . 0.950 no
C306 . H3062 . 0.950 no
C307 . C308 . 1.510(7) yes
C307 . H3071 . 0.950 no
C307 . H3072 . 0.950 no
C308 . H3081 . 0.950 no
C308 . H3082 . 0.950 no
O309 . H3092 . 0.950 no
O309 . H3091 . 0.950 no
C311 . C312 . 1.521(5) yes
C311 . H3111 . 0.950 no
C311 . H3112 . 0.950 no
C312 . O313 . 1.251(5) yes
C314 . C315 . 1.522(5) yes
C314 . H3141 . 0.950 no
C314 . H3142 . 0.950 no
C315 . O316 . 1.248(5) yes
O316 . Eu4 . 2.386(11) yes
C317 . C318 . 1.521(5) yes
C317 . H3171 . 0.950 no
C317 . H3172 . 0.950 no
C318 . O319 . 1.250(5) yes
O320 . C324 . 1.250(7) yes
C321 . C322 . 1.592(7) yes
C321 . H3211 . 0.950 no
C321 . H3212 . 0.950 no
C322 . C323 . 1.399(7) yes
C322 . C327 . 1.508(7) yes
C323 . C324 . 1.471(7) yes
C323 . H3231 . 0.950 no
C324 . O325 . 1.326(7) yes
O325 . C326 . 1.357(7) yes
C326 . C327 . 1.383(6) yes
C326 . C331 . 1.381(6) yes
C327 . C328 . 1.382(6) yes
C328 . C329 . 1.385(6) yes
C328 . H3281 . 0.950 no
C329 . C330 . 1.381(6) yes
C329 . H3291 . 0.950 no
C330 . C331 . 1.384(6) yes
C330 . O332 . 1.413(5) yes
C331 . H3311 . 0.950 no
O332 . C333 . 1.413(5) yes
C333 . H3333 . 0.950 no
C333 . H3332 . 0.950 no
C333 . H3331 . 0.950 no
Eu4 . O401 . 2.409(7) yes
Eu4 . N401 . 2.740(6) yes
Eu4 . O402 . 2.406(7) yes
Eu4 . N402 . 2.724(6) yes
Eu4 . O403 . 2.403(7) yes
Eu4 . N403 . 2.722(6) yes
Eu4 . N404 . 2.727(6) yes
Eu4 . O409 . 2.508(7) yes
C401 . N401 . 1.484(7) yes
C401 . C402 . 1.515(7) yes
C401 . H4011 . 0.950 no
C401 . H4012 . 0.950 no
O401 . C412 . 1.266(5) yes
N401 . C408 . 1.480(6) yes
N401 . C411 . 1.500(6) yes
C402 . N402 . 1.482(6) yes
C402 . H4021 . 0.950 no
C402 . H4022 . 0.950 no
O402 . C415 . 1.267(5) yes
N402 . C403 . 1.467(7) yes
N402 . C414 . 1.497(6) yes
C403 . C404 . 1.508(7) yes
C403 . H4031 . 0.950 no
C403 . H4032 . 0.950 no
O403 . C418 . 1.264(5) yes
N403 . C404 . 1.478(6) yes
N403 . C405 . 1.482(7) yes
N403 . C417 . 1.507(7) yes
C404 . H4041 . 0.950 no
C404 . H4042 . 0.950 no
N404 . C406 . 1.479(7) yes
N404 . C407 . 1.479(7) yes
N404 . C421 . 1.514(6) yes
C405 . C406 . 1.523(7) yes
C405 . H4051 . 0.950 no
C405 . H4052 . 0.950 no
C406 . H4061 . 0.950 no
C406 . H4062 . 0.950 no
C407 . C408 . 1.509(7) yes
C407 . H4071 . 0.950 no
C407 . H4072 . 0.950 no
C408 . H4081 . 0.950 no
C408 . H4082 . 0.950 no
O409 . H4092 . 0.950 no
O409 . H4091 . 0.950 no
C411 . C412 . 1.520(5) yes
C411 . H4111 . 0.950 no
C411 . H4112 . 0.950 no
C412 . O413 . 1.249(5) yes
C414 . C415 . 1.523(5) yes
C414 . H4141 . 0.950 no
C414 . H4142 . 0.950 no
C415 . O416 . 1.251(5) yes
C417 . C418 . 1.521(5) yes
C417 . H4171 . 0.950 no
C417 . H4172 . 0.950 no
C418 . O419 . 1.248(5) yes
O420 . C424 . 1.252(7) yes
C421 . C422 . 1.595(7) yes
C421 . H4211 . 0.950 no
C421 . H4212 . 0.950 no
C422 . C423 . 1.399(7) yes
C422 . C427 . 1.506(7) yes
C423 . C424 . 1.478(7) yes
C423 . H4231 . 0.950 no
C424 . O425 . 1.327(7) yes
O425 . C426 . 1.364(7) yes
C426 . C427 . 1.384(6) yes
C426 . C431 . 1.382(6) yes
C427 . C428 . 1.381(6) yes
C428 . C429 . 1.384(6) yes
C428 . H4281 . 0.950 no
C429 . C430 . 1.381(6) yes
C429 . H4291 . 0.950 no
C430 . C431 . 1.383(6) yes
C430 . O432 . 1.413(5) yes
C431 . H4311 . 0.950 no
O432 . C433 . 1.413(5) yes
C433 . H4332 . 0.950 no
C433 . H4333 . 0.950 no
C433 . H4331 . 0.950 no
Eu5 . N501 . 2.728(7) yes
Eu5 . O501 . 2.406(7) yes
Eu5 . O502 . 2.407(7) yes
Eu5 . N502 . 2.732(7) yes
Eu5 . N503 . 2.720(7) yes
Eu5 . O503 . 2.403(7) yes
Eu5 . N504 . 2.734(7) yes
Eu5 . O509 . 2.515(7) yes
Eu5 . C517 . 3.386(17) yes
Eu5 . O813 . 2.570(12) yes
C501 . N501 . 1.473(6) yes
C501 . C502 . 1.507(7) yes
C501 . H5011 . 0.950 no
C501 . H5012 . 0.950 no
N501 . C508 . 1.477(7) yes
N501 . C511 . 1.502(7) yes
O501 . C512 . 1.269(5) yes
O502 . C515 . 1.268(5) yes
N502 . C502 . 1.477(7) yes
N502 . C503 . 1.485(7) yes
N502 . C514 . 1.502(7) yes
C502 . H5021 . 0.950 no
C502 . H5022 . 0.950 no
N503 . C504 . 1.477(7) yes
N503 . C505 . 1.474(7) yes
N503 . C517 . 1.494(7) yes
C503 . C504 . 1.513(7) yes
C503 . H5031 . 0.950 no
C503 . H5032 . 0.950 no
O503 . C518 . 1.268(5) yes
N504 . C506 . 1.486(7) yes
N504 . C507 . 1.483(7) yes
N504 . C521 . 1.513(6) yes
C504 . H5041 . 0.950 no
C504 . H5042 . 0.950 no
C505 . C506 . 1.517(7) yes
C505 . H5051 . 0.950 no
C505 . H5052 . 0.950 no
C506 . H5061 . 0.950 no
C506 . H5062 . 0.950 no
C507 . C508 . 1.511(7) yes
C507 . H5071 . 0.950 no
C507 . H5072 . 0.950 no
C508 . H5081 . 0.950 no
C508 . H5082 . 0.950 no
O509 . H5092 . 0.950 no
O509 . H5091 . 0.950 no
C511 . C512 . 1.522(5) yes
C511 . H5111 . 0.950 no
C511 . H5112 . 0.950 no
C512 . O513 . 1.250(5) yes
C514 . C515 . 1.519(5) yes
C514 . H5141 . 0.950 no
C514 . H5142 . 0.950 no
C515 . O516 . 1.249(5) yes
O516 . Eu6 . 2.405(12) yes
C517 . C518 . 1.524(5) yes
C517 . H5171 . 0.950 no
C517 . H5172 . 0.950 no
C518 . O519 . 1.250(5) yes
O520 . C524 . 1.244(7) yes
C521 . C522 . 1.592(7) yes
C521 . H5211 . 0.950 no
C521 . H5212 . 0.950 no
C522 . C523 . 1.402(7) yes
C522 . C527 . 1.507(7) yes
C523 . C524 . 1.473(7) yes
C523 . H5231 . 0.950 no
C524 . O525 . 1.319(7) yes
O525 . C526 . 1.355(7) yes
C526 . C527 . 1.384(6) yes
C526 . C531 . 1.382(6) yes
C527 . C528 . 1.383(6) yes
C528 . C529 . 1.382(6) yes
C528 . H5281 . 0.950 no
C529 . C530 . 1.383(6) yes
C529 . H5291 . 0.950 no
C530 . C531 . 1.383(6) yes
C530 . O532 . 1.413(5) yes
C531 . H5311 . 0.950 no
O532 . C533 . 1.415(5) yes
C533 . H5331 . 0.950 no
C533 . H5333 . 0.950 no
C533 . H5332 . 0.950 no
Eu6 . O601 . 2.399(7) yes
Eu6 . N601 . 2.734(7) yes
Eu6 . N602 . 2.727(7) yes
Eu6 . O602 . 2.406(7) yes
Eu6 . N603 . 2.720(7) yes
Eu6 . O603 . 2.407(7) yes
Eu6 . N604 . 2.724(7) yes
Eu6 . O609 . 2.511(7) yes
O601 . C612 . 1.267(5) yes
N601 . C601 . 1.475(7) yes
N601 . C608 . 1.475(7) yes
N601 . C611 . 1.501(7) yes
C601 . C602 . 1.518(7) yes
C601 . H6012 . 0.950 no
C601 . H6011 . 0.950 no
C602 . N602 . 1.478(7) yes
C602 . H6022 . 0.950 no
C602 . H6021 . 0.950 no
N602 . C603 . 1.470(7) yes
N602 . C614 . 1.497(7) yes
O602 . C615 . 1.269(5) yes
C603 . C604 . 1.506(7) yes
C603 . H6031 . 0.950 no
C603 . H6032 . 0.950 no
N603 . C604 . 1.474(6) yes
N603 . C605 . 1.472(7) yes
N603 . C617 . 1.508(7) yes
O603 . C618 . 1.269(5) yes
C604 . H6041 . 0.950 no
C604 . H6042 . 0.950 no
N604 . C606 . 1.474(7) yes
N604 . C607 . 1.472(7) yes
N604 . C621 . 1.510(6) yes
C605 . C606 . 1.520(7) yes
C605 . H6051 . 0.950 no
C605 . H6052 . 0.950 no
C606 . H6061 . 0.950 no
C606 . H6062 . 0.950 no
C607 . C608 . 1.513(7) yes
C607 . H6071 . 0.950 no
C607 . H6072 . 0.950 no
C608 . H6081 . 0.950 no
C608 . H6082 . 0.950 no
O609 . H6092 . 0.950 no
O609 . H6091 . 0.950 no
C611 . C612 . 1.520(5) yes
C611 . H6111 . 0.950 no
C611 . H6112 . 0.950 no
C612 . O613 . 1.246(5) yes
O613 . Eu7 . 2.541(12) yes
C614 . C615 . 1.524(5) yes
C614 . H6141 . 0.950 no
C614 . H6142 . 0.950 no
C615 . O616 . 1.250(5) yes
C617 . C618 . 1.521(5) yes
C617 . H6171 . 0.950 no
C617 . H6172 . 0.950 no
C618 . O619 . 1.249(5) yes
O620 . C624 . 1.249(7) yes
C621 . C622 . 1.591(7) yes
C621 . H6211 . 0.950 no
C621 . H6212 . 0.950 no
C622 . C623 . 1.399(7) yes
C622 . C627 . 1.506(7) yes
C623 . C624 . 1.474(7) yes
C623 . H6231 . 0.950 no
C624 . O625 . 1.321(7) yes
O625 . C626 . 1.358(7) yes
C626 . C627 . 1.381(6) yes
C626 . C631 . 1.380(6) yes
C627 . C628 . 1.385(6) yes
C628 . C629 . 1.384(6) yes
C628 . H6281 . 0.950 no
C629 . C630 . 1.380(6) yes
C629 . H6291 . 0.950 no
C630 . C631 . 1.386(6) yes
C630 . O632 . 1.411(5) yes
C631 . H6311 . 0.950 no
O632 . C633 . 1.411(5) yes
C633 . H6332 . 0.950 no
C633 . H6333 . 0.950 no
C633 . H6331 . 0.950 no
Eu7 . N701 . 2.742(7) yes
Eu7 . O701 . 2.401(7) yes
Eu7 . O702 . 2.392(7) yes
Eu7 . N702 . 2.746(7) yes
Eu7 . N703 . 2.726(7) yes
Eu7 . O703 . 2.403(7) yes
Eu7 . N704 . 2.737(7) yes
Eu7 . O709 . 2.514(7) yes
Eu7 . C717 . 3.432(17) yes
Eu7 . C718 . 3.297(9) yes
N701 . C701 . 1.482(6) yes
N701 . C708 . 1.482(7) yes
N701 . C711 . 1.501(7) yes
C701 . C702 . 1.511(7) yes
C701 . H7012 . 0.950 no
C701 . H7011 . 0.950 no
O701 . C712 . 1.267(5) yes
O702 . C715 . 1.263(5) yes
N702 . C702 . 1.490(7) yes
N702 . C703 . 1.488(7) yes
N702 . C714 . 1.510(7) yes
C702 . H7022 . 0.950 no
C702 . H7021 . 0.950 no
C703 . C704 . 1.510(7) yes
C703 . H7032 . 0.950 no
C703 . H7031 . 0.950 no
N703 . C704 . 1.482(7) yes
N703 . C705 . 1.481(7) yes
N703 . C717 . 1.499(7) yes
O703 . C718 . 1.268(5) yes
C704 . H7042 . 0.950 no
C704 . H7041 . 0.950 no
N704 . C706 . 1.489(7) yes
N704 . C707 . 1.489(7) yes
N704 . C721 . 1.518(6) yes
C705 . C706 . 1.516(7) yes
C705 . H7051 . 0.950 no
C705 . H7052 . 0.950 no
C706 . H7061 . 0.950 no
C706 . H7062 . 0.950 no
C707 . C708 . 1.513(7) yes
C707 . H7071 . 0.950 no
C707 . H7072 . 0.950 no
C708 . H7081 . 0.950 no
C708 . H7082 . 0.950 no
O709 . H7092 . 0.950 no
O709 . H7091 . 0.950 no
C711 . C712 . 1.521(5) yes
C711 . H7111 . 0.950 no
C711 . H7112 . 0.950 no
C712 . O713 . 1.248(5) yes
C714 . C715 . 1.520(5) yes
C714 . H7141 . 0.950 no
C714 . H7142 . 0.950 no
C715 . O716 . 1.246(5) yes
O716 . Eu8 . 2.399(11) yes
C717 . C718 . 1.519(5) yes
C717 . H7171 . 0.950 no
C717 . H7172 . 0.950 no
C718 . O719 . 1.251(5) yes
O720 . C724 . 1.244(6) yes
C721 . C722 . 1.593(7) yes
C721 . H7211 . 0.950 no
C721 . H7212 . 0.950 no
C722 . C723 . 1.403(7) yes
C722 . C727 . 1.509(7) yes
C723 . C724 . 1.475(7) yes
C723 . H7231 . 0.950 no
C724 . O725 . 1.330(7) yes
O725 . C726 . 1.361(7) yes
C726 . C727 . 1.389(6) yes
C726 . C731 . 1.380(6) yes
C727 . C728 . 1.378(6) yes
C728 . C729 . 1.383(6) yes
C728 . H7281 . 0.950 no
C729 . C730 . 1.381(6) yes
C729 . H7291 . 0.950 no
C730 . C731 . 1.384(6) yes
C730 . O732 . 1.412(5) yes
C731 . H7311 . 0.950 no
O732 . C733 . 1.412(5) yes
C733 . H7331 . 0.950 no
C733 . H7333 . 0.950 no
C733 . H7332 . 0.950 no
Eu8 . O801 . 2.398(7) yes
Eu8 . N801 . 2.732(7) yes
Eu8 . N802 . 2.721(7) yes
Eu8 . O802 . 2.400(7) yes
Eu8 . O803 . 2.411(7) yes
Eu8 . N804 . 2.726(7) yes
Eu8 . O809 . 2.512(7) yes
O801 . C812 . 1.265(5) yes
N801 . C801 . 1.486(7) yes
N801 . C808 . 1.473(7) yes
N801 . C811 . 1.497(7) yes
C801 . C802 . 1.518(7) yes
C801 . H8012 . 0.950 no
C801 . H8011 . 0.950 no
C802 . N802 . 1.481(6) yes
C802 . H8022 . 0.950 no
C802 . H8021 . 0.950 no
N802 . C803 . 1.470(7) yes
N802 . C814 . 1.496(7) yes
O802 . C815 . 1.265(5) yes
C803 . C804 . 1.506(7) yes
C803 . H8032 . 0.950 no
C803 . H8031 . 0.950 no
N803 . C804 . 1.475(6) yes
N803 . C805 . 1.472(7) yes
N803 . C817 . 1.503(7) yes
O803 . C818 . 1.268(5) yes
C804 . H8042 . 0.950 no
C804 . H8041 . 0.950 no
N804 . C806 . 1.473(7) yes
N804 . C807 . 1.475(7) yes
N804 . C821 . 1.507(6) yes
C805 . C806 . 1.532(7) yes
C805 . H8052 . 0.950 no
C805 . H8051 . 0.950 no
C806 . H8062 . 0.950 no
C806 . H8061 . 0.950 no
C807 . C808 . 1.515(7) yes
C807 . H8071 . 0.950 no
C807 . H8072 . 0.950 no
C808 . H8081 . 0.950 no
C808 . H8082 . 0.950 no
O809 . H8092 . 0.950 no
O809 . H8091 . 0.950 no
C811 . C812 . 1.521(5) yes
C811 . H8111 . 0.950 no
C811 . H8112 . 0.950 no
C812 . O813 . 1.246(5) yes
C814 . C815 . 1.523(5) yes
C814 . H8141 . 0.950 no
C814 . H8142 . 0.950 no
C815 . O816 . 1.248(5) yes
C817 . C818 . 1.521(5) yes
C817 . H8171 . 0.950 no
C817 . H8172 . 0.950 no
C818 . O819 . 1.250(5) yes
O820 . C824 . 1.247(7) yes
C821 . C822 . 1.591(8) yes
C821 . H8211 . 0.950 no
C821 . H8212 . 0.950 no
C822 . C823 . 1.397(7) yes
C822 . C827 . 1.502(7) yes
C823 . C824 . 1.475(7) yes
C823 . H8231 . 0.950 no
C824 . O825 . 1.322(7) yes
O825 . C826 . 1.358(7) yes
C826 . C827 . 1.381(6) yes
C826 . C831 . 1.383(6) yes
C827 . C828 . 1.383(6) yes
C828 . C829 . 1.383(6) yes
C828 . H8281 . 0.950 no
C829 . C830 . 1.383(6) yes
C829 . H8291 . 0.950 no
C830 . C831 . 1.383(6) yes
C830 . O832 . 1.413(5) yes
C831 . H8311 . 0.950 no
O832 . C833 . 1.413(5) yes
C833 . H8331 . 0.950 no
C833 . H8332 . 0.950 no
C833 . H8333 . 0.950 no
loop_
_geom_angle_atom_site_label_1
_geom_angle_site_symmetry_1
_geom_angle_atom_site_label_2
_geom_angle_site_symmetry_2
_geom_angle_atom_site_label_3
_geom_angle_site_symmetry_3
_geom_angle
_geom_angle_publ_flag
O101 . Eu1 . N101 . 67.8(4) yes
O101 . Eu1 . O102 . 83.2(4) yes
N101 . Eu1 . O102 . 73.0(3) yes
O101 . Eu1 . N102 . 130.1(4) yes
N101 . Eu1 . N102 . 66.6(2) yes
O102 . Eu1 . N102 . 65.1(4) yes
O101 . Eu1 . O103 . 146.3(4) yes
N101 . Eu1 . O103 . 134.5(3) yes
O102 . Eu1 . O103 . 82.0(4) yes
N102 . Eu1 . O103 . 68.4(3) yes
O101 . Eu1 . N103 . 143.6(3) yes
N101 . Eu1 . N103 . 102.2(3) yes
O102 . Eu1 . N103 . 128.9(4) yes
N102 . Eu1 . N103 . 66.62(19) yes
O103 . Eu1 . N103 . 65.5(4) yes
O101 . Eu1 . N104 . 77.6(3) yes
N101 . Eu1 . N104 . 66.61(19) yes
O102 . Eu1 . N104 . 139.3(3) yes
N102 . Eu1 . N104 . 101.6(3) yes
O103 . Eu1 . N104 . 131.0(4) yes
O101 . Eu1 . O109 . 73.4(5) yes
N101 . Eu1 . O109 . 126.7(5) yes
O102 . Eu1 . O109 . 67.3(5) yes
N102 . Eu1 . O109 . 121.4(5) yes
O103 . Eu1 . O109 . 73.0(5) yes
O101 . Eu1 . O413 . 92.1(4) yes
N101 . Eu1 . O413 . 140.7(3) yes
O102 . Eu1 . O413 . 140.2(3) yes
N102 . Eu1 . O413 . 136.9(3) yes
O103 . Eu1 . O413 . 80.5(3) yes
N103 . Eu1 . N104 . 66.7(2) yes
N103 . Eu1 . O109 . 130.2(5) yes
N104 . Eu1 . O109 . 137.0(5) yes
N103 . Eu1 . O413 . 73.8(3) yes
N104 . Eu1 . O413 . 76.5(3) yes
O109 . Eu1 . O413 . 73.5(5) yes
N101 . C101 . C102 . 112.9(6) yes
N101 . C101 . H1011 . 108.5 no
C102 . C101 . H1011 . 108.7 no
N101 . C101 . H1012 . 107.6 no
C102 . C101 . H1012 . 109.7 no
H1011 . C101 . H1012 . 109.5 no
Eu1 . O101 . C112 . 124.4(6) yes
C101 . N101 . Eu1 . 109.1(5) yes
C101 . N101 . C108 . 111.3(6) yes
Eu1 . N101 . C108 . 111.5(5) yes
C101 . N101 . C111 . 110.5(5) yes
Eu1 . N101 . C111 . 104.0(8) yes
C108 . N101 . C111 . 110.2(6) yes
C101 . C102 . N102 . 112.6(6) yes
C101 . C102 . H1021 . 107.7 no
N102 . C102 . H1021 . 107.4 no
C101 . C102 . H1022 . 109.7 no
N102 . C102 . H1022 . 109.9 no
H1021 . C102 . H1022 . 109.5 no
Eu1 . O102 . C115 . 124.8(5) yes
C102 . N102 . Eu1 . 111.9(4) yes
C102 . N102 . C103 . 110.4(6) yes
Eu1 . N102 . C103 . 110.4(4) yes
C102 . N102 . C114 . 109.8(6) yes
Eu1 . N102 . C114 . 104.8(7) yes
C103 . N102 . C114 . 109.5(5) yes
N102 . C103 . C104 . 112.3(6) yes
N102 . C103 . H1031 . 107.9 no
C104 . C103 . H1031 . 108.6 no
N102 . C103 . H1032 . 108.9 no
C104 . C103 . H1032 . 109.7 no
H1031 . C103 . H1032 . 109.5 no
Eu1 . O103 . C118 . 124.5(5) yes
Eu1 . N103 . C104 . 111.2(5) yes
Eu1 . N103 . C105 . 108.6(5) yes
C104 . N103 . C105 . 111.2(6) yes
Eu1 . N103 . C117 . 104.7(8) yes
C104 . N103 . C117 . 110.1(6) yes
C105 . N103 . C117 . 110.8(5) yes
C103 . C104 . N103 . 112.1(6) yes
C103 . C104 . H1041 . 109.6 no
N103 . C104 . H1041 . 109.2 no
C103 . C104 . H1042 . 108.1 no
N103 . C104 . H1042 . 108.2 no
H1041 . C104 . H1042 . 109.5 no
Eu1 . N104 . C106 . 111.7(4) yes
Eu1 . N104 . C107 . 110.3(5) yes
C106 . N104 . C107 . 111.0(6) yes
Eu1 . N104 . C121 . 105.8(7) yes
C106 . N104 . C121 . 108.9(6) yes
C107 . N104 . C121 . 109.0(5) yes
N103 . C105 . C106 . 112.3(6) yes
N103 . C105 . H1051 . 107.7 no
C106 . C105 . H1051 . 108.3 no
N103 . C105 . H1052 . 109.0 no
C106 . C105 . H1052 . 110.0 no
H1051 . C105 . H1052 . 109.5 no
C105 . C106 . N104 . 111.7(7) yes
C105 . C106 . H1061 . 110.1 no
N104 . C106 . H1061 . 109.7 no
C105 . C106 . H1062 . 108.0 no
N104 . C106 . H1062 . 107.8 no
H1061 . C106 . H1062 . 109.5 no
N104 . C107 . C108 . 112.9(6) yes
N104 . C107 . H1071 . 109.2 no
C108 . C107 . H1071 . 109.2 no
N104 . C107 . H1072 . 107.8 no
C108 . C107 . H1072 . 108.3 no
H1071 . C107 . H1072 . 109.5 no
C107 . C108 . N101 . 112.8(6) yes
C107 . C108 . H1081 . 108.7 no
N101 . C108 . H1081 . 108.5 no
C107 . C108 . H1082 . 109.2 no
N101 . C108 . H1082 . 108.1 no
H1081 . C108 . H1082 . 109.5 no
Eu1 . O109 . H1092 . 110.7 no
Eu1 . O109 . H1091 . 129.5 no
H1092 . O109 . H1091 . 106.4 no
N101 . C111 . C112 . 116.5(8) yes
N101 . C111 . H1111 . 107.8 no
C112 . C111 . H1111 . 117.9 no
N101 . C111 . H1112 . 106.2 no
C112 . C111 . H1112 . 97.7 no
H1111 . C111 . H1112 . 109.5 no
C111 . C112 . O101 . 118.65(6) yes
C111 . C112 . O113 . 118.15(6) yes
O101 . C112 . O113 . 123.20(6) yes
N102 . C114 . C115 . 112.9(7) yes
N102 . C114 . H1142 . 109.6 no
C115 . C114 . H1142 . 108.4 no
N102 . C114 . H1141 . 108.1 no
C115 . C114 . H1141 . 108.3 no
H1142 . C114 . H1141 . 109.5 no
C114 . C115 . O102 . 118.64(6) yes
C114 . C115 . O116 . 118.15(6) yes
O102 . C115 . O116 . 123.21(6) yes
C115 . O116 . Eu2 . 142.9(5) yes
N103 . C117 . C118 . 112.8(7) yes
N103 . C117 . H1171 . 109.0 no
C118 . C117 . H1171 . 108.7 no
N103 . C117 . H1172 . 108.3 no
C118 . C117 . H1172 . 108.4 no
H1171 . C117 . H1172 . 109.5 no
C117 . C118 . O103 . 118.64(6) yes
C117 . C118 . O119 . 118.15(6) yes
O103 . C118 . O119 . 123.21(6) yes
N104 . C121 . C122 . 122.5(8) yes
N104 . C121 . H1211 . 105.9 no
C122 . C121 . H1211 . 103.7 no
N104 . C121 . H1212 . 106.6 no
C122 . C121 . H1212 . 108.2 no
H1211 . C121 . H1212 . 109.5 no
C121 . C122 . C123 . 118.2(12) yes
C121 . C122 . C127 . 114.9(13) yes
C123 . C122 . C127 . 126.9(13) yes
C122 . C123 . C124 . 110.9(12) yes
C122 . C123 . H1231 . 124.5 no
C124 . C123 . H1231 . 124.6 no
C123 . C124 . O120 . 117.1(8) yes
C123 . C124 . O125 . 125.8(10) yes
O120 . C124 . O125 . 117.1(8) yes
C124 . O125 . C126 . 118.0(13) yes
O125 . C126 . C127 . 128.2(12) yes
O125 . C126 . C131 . 111.7(12) yes
C127 . C126 . C131 . 120.1(5) yes
C122 . C127 . C126 . 110.3(11) yes
C122 . C127 . C128 . 129.6(11) yes
C126 . C127 . C128 . 120.1(5) yes
C127 . C128 . C129 . 119.8(6) yes
C127 . C128 . H1281 . 120.5 no
C129 . C128 . H1281 . 119.7 no
C128 . C129 . C130 . 119.9(5) yes
C128 . C129 . H1291 . 120.4 no
C130 . C129 . H1291 . 119.7 no
C129 . C130 . C131 . 120.2(5) yes
C129 . C130 . O132 . 120.1(6) yes
C131 . C130 . O132 . 119.8(6) yes
C130 . C131 . C126 . 119.9(5) yes
C130 . C131 . H1311 . 120.5 no
C126 . C131 . H1311 . 119.7 no
C130 . O132 . C133 . 118.2(7) yes
O132 . C133 . H1333 . 112.5 no
O132 . C133 . H1332 . 107.8 no
H1333 . C133 . H1332 . 109.5 no
O132 . C133 . H1331 . 108.0 no
H1333 . C133 . H1331 . 109.5 no
H1332 . C133 . H1331 . 109.5 no
O116 . Eu2 . O201 . 139.1(4) yes
O116 . Eu2 . N201 . 142.8(3) yes
O201 . Eu2 . N201 . 59.5(4) yes
O116 . Eu2 . O202 . 76.0(3) yes
O201 . Eu2 . O202 . 78.0(4) yes
N201 . Eu2 . O202 . 80.2(3) yes
O116 . Eu2 . N202 . 77.5(3) yes
O201 . Eu2 . N202 . 118.3(4) yes
N201 . Eu2 . N202 . 66.6(2) yes
O202 . Eu2 . N202 . 65.0(4) yes
O116 . Eu2 . O203 . 74.6(3) yes
O201 . Eu2 . O203 . 108.8(4) yes
N201 . Eu2 . O203 . 137.7(3) yes
O202 . Eu2 . O203 . 140.4(3) yes
N202 . Eu2 . O203 . 131.4(4) yes
O116 . Eu2 . N203 . 71.1(3) yes
O201 . Eu2 . N203 . 149.0(3) yes
N201 . Eu2 . N203 . 101.9(3) yes
O202 . Eu2 . N203 . 126.2(4) yes
N202 . Eu2 . N203 . 67.1(2) yes
O116 . Eu2 . N204 . 133.9(3) yes
O201 . Eu2 . N204 . 82.2(3) yes
N201 . Eu2 . N204 . 66.5(2) yes
O202 . Eu2 . N204 . 146.5(3) yes
N202 . Eu2 . N204 . 102.6(3) yes
O116 . Eu2 . O209 . 73.8(6) yes
O201 . Eu2 . O209 . 70.1(6) yes
N201 . Eu2 . O209 . 128.0(6) yes
O202 . Eu2 . O209 . 77.5(5) yes
N202 . Eu2 . O209 . 137.1(5) yes
O203 . Eu2 . N203 . 66.6(4) yes
O203 . Eu2 . N204 . 71.8(3) yes
N203 . Eu2 . N204 . 67.13(19) yes
O203 . Eu2 . O209 . 69.2(5) yes
N203 . Eu2 . O209 . 129.0(6) yes
N204 . Eu2 . O209 . 120.3(5) yes
N201 . C201 . C202 . 112.8(6) yes
N201 . C201 . H2011 . 107.4 no
C202 . C201 . H2011 . 109.9 no
N201 . C201 . H2012 . 107.7 no
C202 . C201 . H2012 . 109.5 no
H2011 . C201 . H2012 . 109.5 no
Eu2 . O201 . C212 . 121.9(5) yes
C201 . N201 . Eu2 . 111.0(5) yes
C201 . N201 . C208 . 110.9(6) yes
Eu2 . N201 . C208 . 109.5(5) yes
C201 . N201 . C211 . 109.8(6) yes
Eu2 . N201 . C211 . 105.5(7) yes
C208 . N201 . C211 . 110.1(5) yes
C201 . C202 . N202 . 113.3(7) yes
C201 . C202 . H2021 . 106.5 no
N202 . C202 . H2021 . 108.2 no
C201 . C202 . H2022 . 109.8 no
N202 . C202 . H2022 . 109.4 no
H2021 . C202 . H2022 . 109.5 no
Eu2 . O202 . C215 . 117.5(5) yes
C202 . N202 . Eu2 . 111.4(4) yes
C202 . N202 . C203 . 111.9(6) yes
Eu2 . N202 . C203 . 112.6(4) yes
C202 . N202 . C214 . 110.0(5) yes
Eu2 . N202 . C214 . 99.0(7) yes
C203 . N202 . C214 . 111.4(6) yes
N202 . C203 . C204 . 114.8(7) yes
N202 . C203 . H2031 . 109.4 no
C204 . C203 . H2031 . 108.5 no
N202 . C203 . H2032 . 106.8 no
C204 . C203 . H2032 . 107.7 no
H2031 . C203 . H2032 . 109.5 no
Eu2 . O203 . C218 . 123.1(6) yes
Eu2 . N203 . C204 . 108.5(5) yes
Eu2 . N203 . C205 . 110.3(5) yes
C204 . N203 . C205 . 112.9(6) yes
Eu2 . N203 . C217 . 104.7(8) yes
C204 . N203 . C217 . 110.3(5) yes
C205 . N203 . C217 . 109.8(6) yes
C203 . C204 . N203 . 114.8(6) yes
C203 . C204 . H2041 . 108.2 no
N203 . C204 . H2041 . 107.6 no
C203 . C204 . H2042 . 108.6 no
N203 . C204 . H2042 . 108.2 no
H2041 . C204 . H2042 . 109.5 no
Eu2 . N204 . C206 . 109.3(5) yes
Eu2 . N204 . C207 . 112.8(5) yes
C206 . N204 . C207 . 111.8(6) yes
Eu2 . N204 . C221 . 101.6(7) yes
C206 . N204 . C221 . 110.6(6) yes
C207 . N204 . C221 . 110.3(6) yes
N203 . C205 . C206 . 111.9(6) yes
N203 . C205 . H2051 . 108.7 no
C206 . C205 . H2051 . 109.3 no
N203 . C205 . H2052 . 108.7 no
C206 . C205 . H2052 . 108.8 no
H2051 . C205 . H2052 . 109.5 no
C205 . C206 . N204 . 111.9(6) yes
C205 . C206 . H2061 . 108.8 no
N204 . C206 . H2061 . 107.6 no
C205 . C206 . H2062 . 108.8 no
N204 . C206 . H2062 . 110.3 no
H2061 . C206 . H2062 . 109.5 no
N204 . C207 . C208 . 114.0(7) yes
N204 . C207 . H2071 . 107.5 no
C208 . C207 . H2071 . 108.6 no
N204 . C207 . H2072 . 110.0 no
C208 . C207 . H2072 . 107.2 no
H2071 . C207 . H2072 . 109.5 no
C207 . C208 . N201 . 113.3(7) yes
C207 . C208 . H2081 . 110.2 no
N201 . C208 . H2081 . 109.6 no
C207 . C208 . H2082 . 107.3 no
N201 . C208 . H2082 . 106.8 no
H2081 . C208 . H2082 . 109.5 no
Eu2 . O209 . H2092 . 96.5 no
Eu2 . O209 . H2091 . 136.4 no
H2092 . O209 . H2091 . 125.0 no
N201 . C211 . C212 . 105.4(7) yes
N201 . C211 . H2111 . 110.8 no
C212 . C211 . H2111 . 110.6 no
N201 . C211 . H2112 . 110.1 no
C212 . C211 . H2112 . 110.4 no
H2111 . C211 . H2112 . 109.5 no
C211 . C212 . O201 . 118.64(6) yes
C211 . C212 . O213 . 118.15(6) yes
O201 . C212 . O213 . 123.21(6) yes
C212 . O213 . Eu3 . 132.2(5) yes
N202 . C214 . C215 . 113.1(8) yes
N202 . C214 . H2141 . 109.1 no
C215 . C214 . H2141 . 109.2 no
N202 . C214 . H2142 . 108.2 no
C215 . C214 . H2142 . 107.7 no
H2141 . C214 . H2142 . 109.5 no
C214 . C215 . O202 . 118.65(6) yes
C214 . C215 . O216 . 118.15(6) yes
O202 . C215 . O216 . 123.20(6) yes
N203 . C217 . C218 . 117.0(8) yes
N203 . C217 . H2171 . 106.6 no
C218 . C217 . H2171 . 106.0 no
N203 . C217 . H2172 . 108.1 no
C218 . C217 . H2172 . 109.5 no
H2171 . C217 . H2172 . 109.5 no
C217 . C218 . O203 . 118.65(6) yes
C217 . C218 . O219 . 118.14(6) yes
O203 . C218 . O219 . 123.21(6) yes
N204 . C221 . C222 . 113.1(8) yes
N204 . C221 . H2211 . 108.5 no
C222 . C221 . H2211 . 102.4 no
N204 . C221 . H2212 . 110.5 no
C222 . C221 . H2212 . 112.5 no
H2211 . C221 . H2212 . 109.5 no
C221 . C222 . C223 . 123.7(13) yes
C221 . C222 . C227 . 111.8(14) yes
C223 . C222 . C227 . 124.5(13) yes
C222 . C223 . C224 . 112.9(11) yes
C222 . C223 . H2231 . 123.1 no
C224 . C223 . H2231 . 124.0 no
C223 . C224 . O220 . 117.9(8) yes
C223 . C224 . O225 . 124.3(11) yes
O220 . C224 . O225 . 117.8(8) yes
C224 . O225 . C226 . 119.8(13) yes
O225 . C226 . C227 . 126.3(12) yes
O225 . C226 . C231 . 113.5(12) yes
C227 . C226 . C231 . 120.2(5) yes
C222 . C227 . C226 . 112.3(11) yes
C222 . C227 . C228 . 128.1(11) yes
C226 . C227 . C228 . 119.6(5) yes
C227 . C228 . C229 . 120.1(6) yes
C227 . C228 . H2281 . 120.1 no
C229 . C228 . H2281 . 119.7 no
C228 . C229 . C230 . 120.2(5) yes
C228 . C229 . H2291 . 120.2 no
C230 . C229 . H2291 . 119.6 no
C229 . C230 . C231 . 119.7(5) yes
C229 . C230 . O232 . 120.5(6) yes
C231 . C230 . O232 . 119.8(6) yes
C230 . C231 . C226 . 120.2(5) yes
C230 . C231 . H2311 . 120.2 no
C226 . C231 . H2311 . 119.7 no
C230 . O232 . C233 . 118.7(7) yes
O232 . C233 . H2331 . 113.0 no
O232 . C233 . H2332 . 107.7 no
H2331 . C233 . H2332 . 109.5 no
O232 . C233 . H2333 . 107.6 no
H2331 . C233 . H2333 . 109.5 no
H2332 . C233 . H2333 . 109.5 no
O213 . Eu3 . O301 . 93.1(5) yes
O213 . Eu3 . N301 . 140.4(3) yes
O301 . Eu3 . N301 . 66.3(4) yes
O213 . Eu3 . O302 . 143.1(3) yes
O301 . Eu3 . O302 . 82.2(4) yes
N301 . Eu3 . O302 . 70.3(3) yes
O213 . Eu3 . N302 . 136.1(4) yes
O301 . Eu3 . N302 . 129.5(4) yes
N301 . Eu3 . N302 . 67.0(2) yes
O302 . Eu3 . N302 . 64.9(4) yes
O213 . Eu3 . O303 . 78.9(5) yes
O301 . Eu3 . O303 . 148.1(5) yes
N301 . Eu3 . O303 . 135.9(4) yes
O302 . Eu3 . O303 . 86.0(4) yes
N302 . Eu3 . O303 . 69.4(4) yes
O213 . Eu3 . N303 . 72.5(3) yes
O301 . Eu3 . N303 . 142.1(3) yes
N301 . Eu3 . N303 . 102.6(3) yes
O302 . Eu3 . N303 . 129.9(4) yes
N302 . Eu3 . N303 . 66.9(2) yes
O213 . Eu3 . N304 . 75.8(3) yes
O301 . Eu3 . N304 . 76.0(3) yes
N301 . Eu3 . N304 . 66.76(19) yes
O302 . Eu3 . N304 . 136.7(3) yes
N302 . Eu3 . N304 . 101.9(3) yes
O213 . Eu3 . O309 . 74.9(5) yes
O301 . Eu3 . O309 . 73.2(6) yes
N301 . Eu3 . O309 . 125.0(6) yes
O302 . Eu3 . O309 . 68.8(5) yes
N302 . Eu3 . O309 . 122.3(5) yes
O303 . Eu3 . N303 . 64.9(4) yes
O303 . Eu3 . N304 . 129.9(4) yes
N303 . Eu3 . N304 . 66.6(2) yes
O303 . Eu3 . O309 . 74.9(6) yes
N303 . Eu3 . O309 . 131.9(6) yes
N304 . Eu3 . O309 . 135.6(5) yes
N301 . C301 . C302 . 112.7(6) yes
N301 . C301 . H3011 . 108.2 no
C302 . C301 . H3011 . 108.4 no
N301 . C301 . H3012 . 108.6 no
C302 . C301 . H3012 . 109.3 no
H3011 . C301 . H3012 . 109.5 no
Eu3 . O301 . C312 . 125.9(6) yes
C301 . N301 . Eu3 . 108.4(5) yes
C301 . N301 . C308 . 111.3(6) yes
Eu3 . N301 . C308 . 111.0(5) yes
C301 . N301 . C311 . 109.6(5) yes
Eu3 . N301 . C311 . 106.5(8) yes
C308 . N301 . C311 . 109.8(6) yes
C301 . C302 . N302 . 112.8(6) yes
C301 . C302 . H3021 . 109.3 no
N302 . C302 . H3021 . 109.0 no
C301 . C302 . H3022 . 108.5 no
N302 . C302 . H3022 . 107.7 no
H3021 . C302 . H3022 . 109.5 no
Eu3 . O302 . C315 . 124.0(5) yes
C302 . N302 . Eu3 . 111.6(4) yes
C302 . N302 . C303 . 111.2(6) yes
Eu3 . N302 . C303 . 110.2(5) yes
C302 . N302 . C314 . 109.9(6) yes
Eu3 . N302 . C314 . 103.7(7) yes
C303 . N302 . C314 . 110.0(5) yes
N302 . C303 . C304 . 112.3(6) yes
N302 . C303 . H3031 . 108.8 no
C304 . C303 . H3031 . 109.4 no
N302 . C303 . H3032 . 108.8 no
C304 . C303 . H3032 . 108.1 no
H3031 . C303 . H3032 . 109.5 no
Eu3 . O303 . C318 . 106.7(6) yes
Eu3 . N303 . C304 . 110.6(5) yes
Eu3 . N303 . C305 . 109.2(5) yes
C304 . N303 . C305 . 111.1(6) yes
Eu3 . N303 . C317 . 106.1(7) yes
C304 . N303 . C317 . 109.8(6) yes
C305 . N303 . C317 . 109.8(6) yes
C303 . C304 . N303 . 112.5(6) yes
C303 . C304 . H3041 . 108.2 no
N303 . C304 . H3041 . 108.4 no
C303 . C304 . H3042 . 109.4 no
N303 . C304 . H3042 . 108.9 no
H3041 . C304 . H3042 . 109.5 no
Eu3 . N304 . C306 . 112.2(4) yes
Eu3 . N304 . C307 . 110.4(4) yes
C306 . N304 . C307 . 110.4(6) yes
Eu3 . N304 . C321 . 106.0(7) yes
C306 . N304 . C321 . 108.9(6) yes
C307 . N304 . C321 . 108.8(5) yes
N303 . C305 . C306 . 112.7(6) yes
N303 . C305 . H3051 . 108.6 no
C306 . C305 . H3051 . 108.4 no
N303 . C305 . H3052 . 108.7 no
C306 . C305 . H3052 . 108.9 no
H3051 . C305 . H3052 . 109.5 no
C305 . C306 . N304 . 112.5(7) yes
C305 . C306 . H3061 . 109.0 no
N304 . C306 . H3061 . 108.0 no
C305 . C306 . H3062 . 108.9 no
N304 . C306 . H3062 . 108.9 no
H3061 . C306 . H3062 . 109.5 no
N304 . C307 . C308 . 112.8(6) yes
N304 . C307 . H3071 . 108.4 no
C308 . C307 . H3071 . 109.4 no
N304 . C307 . H3072 . 108.6 no
C308 . C307 . H3072 . 108.2 no
H3071 . C307 . H3072 . 109.5 no
C307 . C308 . N301 . 113.2(6) yes
C307 . C308 . H3081 . 108.8 no
N301 . C308 . H3081 . 108.0 no
C307 . C308 . H3082 . 108.1 no
N301 . C308 . H3082 . 109.2 no
H3081 . C308 . H3082 . 109.5 no
Eu3 . O309 . H3092 . 130.9 no
Eu3 . O309 . H3091 . 104.5 no
H3092 . O309 . H3091 . 112.0 no
N301 . C311 . C312 . 113.9(8) yes
N301 . C311 . H3111 . 109.1 no
C312 . C311 . H3111 . 108.1 no
N301 . C311 . H3112 . 108.2 no
C312 . C311 . H3112 . 108.0 no
H3111 . C311 . H3112 . 109.5 no
C311 . C312 . O301 . 118.64(6) yes
C311 . C312 . O313 . 118.15(6) yes
O301 . C312 . O313 . 123.21(6) yes
N302 . C314 . C315 . 112.0(7) yes
N302 . C314 . H3141 . 109.2 no
C315 . C314 . H3141 . 109.3 no
N302 . C314 . H3142 . 108.8 no
C315 . C314 . H3142 . 108.0 no
H3141 . C314 . H3142 . 109.5 no
C314 . C315 . O302 . 118.65(6) yes
C314 . C315 . O316 . 118.15(6) yes
O302 . C315 . O316 . 123.20(6) yes
C315 . O316 . Eu4 . 143.5(5) yes
N303 . C317 . C318 . 109.3(9) yes
N303 . C317 . H3171 . 109.7 no
C318 . C317 . H3171 . 111.2 no
N303 . C317 . H3172 . 108.6 no
C318 . C317 . H3172 . 108.5 no
H3171 . C317 . H3172 . 109.5 no
C317 . C318 . O303 . 118.65(6) yes
C317 . C318 . O319 . 118.15(6) yes
O303 . C318 . O319 . 123.20(6) yes
N304 . C321 . C322 . 119.3(7) yes
N304 . C321 . H3211 . 107.4 no
C322 . C321 . H3211 . 110.0 no
N304 . C321 . H3212 . 107.4 no
C322 . C321 . H3212 . 103.1 no
H3211 . C321 . H3212 . 109.5 no
C321 . C322 . C323 . 118.4(12) yes
C321 . C322 . C327 . 117.5(13) yes
C323 . C322 . C327 . 124.1(12) yes
C322 . C323 . C324 . 113.6(11) yes
C322 . C323 . H3231 . 123.1 no
C324 . C323 . H3231 . 123.3 no
C323 . C324 . O320 . 118.5(8) yes
C323 . C324 . O325 . 123.2(10) yes
O320 . C324 . O325 . 118.3(8) yes
C324 . O325 . C326 . 121.2(12) yes
O325 . C326 . C327 . 125.0(11) yes
O325 . C326 . C331 . 115.0(11) yes
C327 . C326 . C331 . 120.0(5) yes
C322 . C327 . C326 . 112.9(10) yes
C322 . C327 . C328 . 127.1(10) yes
C326 . C327 . C328 . 119.9(5) yes
C327 . C328 . C329 . 120.0(6) yes
C327 . C328 . H3281 . 120.6 no
C329 . C328 . H3281 . 119.4 no
C328 . C329 . C330 . 120.0(5) yes
C328 . C329 . H3291 . 120.7 no
C330 . C329 . H3291 . 119.4 no
C329 . C330 . C331 . 120.0(5) yes
C329 . C330 . O332 . 120.1(6) yes
C331 . C330 . O332 . 119.8(6) yes
C330 . C331 . C326 . 120.0(5) yes
C330 . C331 . H3311 . 120.6 no
C326 . C331 . H3311 . 119.4 no
C330 . O332 . C333 . 118.4(7) yes
O332 . C333 . H3333 . 112.4 no
O332 . C333 . H3332 . 107.9 no
H3333 . C333 . H3332 . 109.5 no
O332 . C333 . H3331 . 108.0 no
H3333 . C333 . H3331 . 109.5 no
H3332 . C333 . H3331 . 109.5 no
O316 . Eu4 . O401 . 138.3(3) yes
O316 . Eu4 . N401 . 142.2(3) yes
O401 . Eu4 . N401 . 60.8(4) yes
O316 . Eu4 . O402 . 76.2(3) yes
O401 . Eu4 . O402 . 77.7(4) yes
N401 . Eu4 . O402 . 79.7(3) yes
O316 . Eu4 . N402 . 76.8(3) yes
O401 . Eu4 . N402 . 118.9(3) yes
N401 . Eu4 . N402 . 66.54(19) yes
O402 . Eu4 . N402 . 64.1(4) yes
O316 . Eu4 . O403 . 74.5(3) yes
O401 . Eu4 . O403 . 109.7(4) yes
N401 . Eu4 . O403 . 137.5(3) yes
O402 . Eu4 . O403 . 141.7(3) yes
N402 . Eu4 . O403 . 130.2(4) yes
O316 . Eu4 . N403 . 70.5(3) yes
O401 . Eu4 . N403 . 150.3(3) yes
N401 . Eu4 . N403 . 101.9(3) yes
O402 . Eu4 . N403 . 125.4(4) yes
N402 . Eu4 . N403 . 66.96(19) yes
O316 . Eu4 . N404 . 133.6(3) yes
O401 . Eu4 . N404 . 83.4(3) yes
N401 . Eu4 . N404 . 66.34(19) yes
O402 . Eu4 . N404 . 146.0(3) yes
N402 . Eu4 . N404 . 102.4(2) yes
O316 . Eu4 . O409 . 75.8(5) yes
O401 . Eu4 . O409 . 67.1(5) yes
N401 . Eu4 . O409 . 126.3(5) yes
O402 . Eu4 . O409 . 77.5(5) yes
N402 . Eu4 . O409 . 137.0(5) yes
O403 . Eu4 . N403 . 65.4(4) yes
O403 . Eu4 . N404 . 71.5(3) yes
N403 . Eu4 . N404 . 67.11(19) yes
O403 . Eu4 . O409 . 71.9(5) yes
N403 . Eu4 . O409 . 130.9(5) yes
N404 . Eu4 . O409 . 120.5(5) yes
N401 . C401 . C402 . 112.3(6) yes
N401 . C401 . H4011 . 109.2 no
C402 . C401 . H4011 . 109.1 no
N401 . C401 . H4012 . 107.7 no
C402 . C401 . H4012 . 109.0 no
H4011 . C401 . H4012 . 109.5 no
Eu4 . O401 . C412 . 120.2(5) yes
C401 . N401 . Eu4 . 111.0(5) yes
C401 . N401 . C408 . 111.0(6) yes
Eu4 . N401 . C408 . 109.9(5) yes
C401 . N401 . C411 . 110.2(6) yes
Eu4 . N401 . C411 . 104.2(6) yes
C408 . N401 . C411 . 110.3(5) yes
C401 . C402 . N402 . 112.5(6) yes
C401 . C402 . H4021 . 109.1 no
N402 . C402 . H4021 . 108.4 no
C401 . C402 . H4022 . 108.5 no
N402 . C402 . H4022 . 108.9 no
H4021 . C402 . H4022 . 109.5 no
Eu4 . O402 . C415 . 114.1(5) yes
C402 . N402 . Eu4 . 110.7(4) yes
C402 . N402 . C403 . 112.2(6) yes
Eu4 . N402 . C403 . 112.4(4) yes
C402 . N402 . C414 . 110.3(5) yes
Eu4 . N402 . C414 . 98.9(7) yes
C403 . N402 . C414 . 111.6(6) yes
N402 . C403 . C404 . 114.4(6) yes
N402 . C403 . H4031 . 107.3 no
C404 . C403 . H4031 . 108.8 no
N402 . C403 . H4032 . 108.1 no
C404 . C403 . H4032 . 108.6 no
H4031 . C403 . H4032 . 109.5 no
Eu4 . O403 . C418 . 125.9(5) yes
Eu4 . N403 . C404 . 108.7(5) yes
Eu4 . N403 . C405 . 110.2(5) yes
C404 . N403 . C405 . 111.8(6) yes
Eu4 . N403 . C417 . 106.5(7) yes
C404 . N403 . C417 . 109.9(5) yes
C405 . N403 . C417 . 109.5(6) yes
C403 . C404 . N403 . 113.9(6) yes
C403 . C404 . H4041 . 108.7 no
N403 . C404 . H4041 . 108.7 no
C403 . C404 . H4042 . 107.8 no
N403 . C404 . H4042 . 108.2 no
H4041 . C404 . H4042 . 109.5 no
Eu4 . N404 . C406 . 109.5(5) yes
Eu4 . N404 . C407 . 113.2(4) yes
C406 . N404 . C407 . 111.2(6) yes
Eu4 . N404 . C421 . 102.6(7) yes
C406 . N404 . C421 . 110.0(6) yes
C407 . N404 . C421 . 110.0(6) yes
N403 . C405 . C406 . 111.8(6) yes
N403 . C405 . H4051 . 108.0 no
C406 . C405 . H4051 . 109.0 no
N403 . C405 . H4052 . 109.3 no
C406 . C405 . H4052 . 109.2 no
H4051 . C405 . H4052 . 109.5 no
C405 . C406 . N404 . 112.1(6) yes
C405 . C406 . H4061 . 109.3 no
N404 . C406 . H4061 . 109.8 no
C405 . C406 . H4062 . 108.3 no
N404 . C406 . H4062 . 107.9 no
H4061 . C406 . H4062 . 109.5 no
N404 . C407 . C408 . 113.7(7) yes
N404 . C407 . H4071 . 107.5 no
C408 . C407 . H4071 . 108.3 no
N404 . C407 . H4072 . 109.8 no
C408 . C407 . H4072 . 107.9 no
H4071 . C407 . H4072 . 109.5 no
C407 . C408 . N401 . 113.6(6) yes
C407 . C408 . H4081 . 108.1 no
N401 . C408 . H4081 . 108.0 no
C407 . C408 . H4082 . 109.1 no
N401 . C408 . H4082 . 108.5 no
H4081 . C408 . H4082 . 109.5 no
Eu4 . O409 . H4092 . 154.6 no
Eu4 . O409 . H4091 . 94.4 no
H4092 . O409 . H4091 . 108.2 no
N401 . C411 . C412 . 107.9(7) yes
N401 . C411 . H4111 . 110.1 no
C412 . C411 . H4111 . 110.3 no
N401 . C411 . H4112 . 109.8 no
C412 . C411 . H4112 . 109.3 no
H4111 . C411 . H4112 . 109.5 no
C411 . C412 . O401 . 118.64(6) yes
C411 . C412 . O413 . 118.15(6) yes
O401 . C412 . O413 . 123.20(6) yes
C412 . O413 . Eu1 . 133.2(5) yes
N402 . C414 . C415 . 113.1(7) yes
N402 . C414 . H4141 . 108.4 no
C415 . C414 . H4141 . 109.9 no
N402 . C414 . H4142 . 108.7 no
C415 . C414 . H4142 . 107.2 no
H4141 . C414 . H4142 . 109.5 no
C414 . C415 . O402 . 118.65(6) yes
C414 . C415 . O416 . 118.15(6) yes
O402 . C415 . O416 . 123.20(6) yes
N403 . C417 . C418 . 113.9(7) yes
N403 . C417 . H4171 . 107.6 no
C418 . C417 . H4171 . 108.5 no
N403 . C417 . H4172 . 108.5 no
C418 . C417 . H4172 . 108.8 no
H4171 . C417 . H4172 . 109.5 no
C417 . C418 . O403 . 118.65(6) yes
C417 . C418 . O419 . 118.15(6) yes
O403 . C418 . O419 . 123.20(6) yes
N404 . C421 . C422 . 110.8(7) yes
N404 . C421 . H4211 . 108.5 no
C422 . C421 . H4211 . 104.8 no
N404 . C421 . H4212 . 110.6 no
C422 . C421 . H4212 . 112.5 no
H4211 . C421 . H4212 . 109.5 no
C421 . C422 . C423 . 125.3(12) yes
C421 . C422 . C427 . 110.1(13) yes
C423 . C422 . C427 . 124.6(13) yes
C422 . C423 . C424 . 113.0(11) yes
C422 . C423 . H4231 . 123.6 no
C424 . C423 . H4231 . 123.4 no
C423 . C424 . O420 . 117.7(8) yes
C423 . C424 . O425 . 124.3(10) yes
O420 . C424 . O425 . 118.0(8) yes
C424 . O425 . C426 . 119.6(13) yes
O425 . C426 . C427 . 126.1(12) yes
O425 . C426 . C431 . 114.1(12) yes
C427 . C426 . C431 . 119.9(5) yes
C422 . C427 . C426 . 112.5(11) yes
C422 . C427 . C428 . 127.6(11) yes
C426 . C427 . C428 . 119.9(5) yes
C427 . C428 . C429 . 120.1(6) yes
C427 . C428 . H4281 . 120.4 no
C429 . C428 . H4281 . 119.5 no
C428 . C429 . C430 . 120.0(5) yes
C428 . C429 . H4291 . 120.5 no
C430 . C429 . H4291 . 119.5 no
C429 . C430 . C431 . 119.9(5) yes
C429 . C430 . O432 . 120.1(6) yes
C431 . C430 . O432 . 120.0(6) yes
C430 . C431 . C426 . 120.2(5) yes
C430 . C431 . H4311 . 120.3 no
C426 . C431 . H4311 . 119.5 no
C430 . O432 . C433 . 118.6(7) yes
O432 . C433 . H4332 . 112.8 no
O432 . C433 . H4333 . 107.6 no
H4332 . C433 . H4333 . 109.5 no
O432 . C433 . H4331 . 108.0 no
H4332 . C433 . H4331 . 109.5 no
H4333 . C433 . H4331 . 109.5 no
N501 . Eu5 . O501 . 68.1(4) yes
N501 . Eu5 . O502 . 77.6(3) yes
O501 . Eu5 . O502 . 87.2(4) yes
N501 . Eu5 . N502 . 66.7(2) yes
O501 . Eu5 . N502 . 131.5(4) yes
O502 . Eu5 . N502 . 67.1(4) yes
N501 . Eu5 . N503 . 102.3(3) yes
O501 . Eu5 . N503 . 140.7(3) yes
O502 . Eu5 . N503 . 129.2(4) yes
N502 . Eu5 . N503 . 66.8(2) yes
N501 . Eu5 . O503 . 137.8(3) yes
O501 . Eu5 . O503 . 144.5(4) yes
O502 . Eu5 . O503 . 78.8(4) yes
N502 . Eu5 . O503 . 72.0(3) yes
N503 . Eu5 . O503 . 67.9(5) yes
N501 . Eu5 . N504 . 66.6(2) yes
O501 . Eu5 . N504 . 74.7(3) yes
O502 . Eu5 . N504 . 143.8(3) yes
N502 . Eu5 . N504 . 102.0(3) yes
N503 . Eu5 . N504 . 66.8(2) yes
N501 . Eu5 . O509 . 127.3(6) yes
O501 . Eu5 . O509 . 75.5(6) yes
O502 . Eu5 . O509 . 63.5(6) yes
N502 . Eu5 . O509 . 121.2(6) yes
N503 . Eu5 . O509 . 129.6(6) yes
N501 . Eu5 . C517 . 126.1(3) yes
O501 . Eu5 . C517 . 150.4(3) yes
O502 . Eu5 . C517 . 119.7(3) yes
N502 . Eu5 . C517 . 74.6(2) yes
N503 . Eu5 . C517 . 25.5(2) yes
N501 . Eu5 . O813 . 134.1(3) yes
O501 . Eu5 . O813 . 91.1(4) yes
O502 . Eu5 . O813 . 144.3(3) yes
N502 . Eu5 . O813 . 133.7(3) yes
N503 . Eu5 . O813 . 68.0(3) yes
O503 . Eu5 . N504 . 132.5(4) yes
O503 . Eu5 . O509 . 69.0(6) yes
N504 . Eu5 . O509 . 136.8(6) yes
O503 . Eu5 . C517 . 45.3(3) yes
N504 . Eu5 . C517 . 87.3(2) yes
O509 . Eu5 . C517 . 104.4(5) yes
O503 . Eu5 . O813 . 82.1(4) yes
N504 . Eu5 . O813 . 68.6(3) yes
O509 . Eu5 . O813 . 81.5(6) yes
C517 . Eu5 . O813 . 60.1(3) yes
N501 . C501 . C502 . 114.2(6) yes
N501 . C501 . H5011 . 108.4 no
C502 . C501 . H5011 . 109.4 no
N501 . C501 . H5012 . 108.4 no
C502 . C501 . H5012 . 107.0 no
H5011 . C501 . H5012 . 109.5 no
C501 . N501 . Eu5 . 108.7(5) yes
C501 . N501 . C508 . 112.1(6) yes
Eu5 . N501 . C508 . 111.4(5) yes
C501 . N501 . C511 . 110.9(5) yes
Eu5 . N501 . C511 . 103.2(8) yes
C508 . N501 . C511 . 110.2(6) yes
Eu5 . O501 . C512 . 123.8(6) yes
Eu5 . O502 . C515 . 123.0(6) yes
Eu5 . N502 . C502 . 112.6(5) yes
Eu5 . N502 . C503 . 110.7(5) yes
C502 . N502 . C503 . 111.2(6) yes
Eu5 . N502 . C514 . 101.9(8) yes
C502 . N502 . C514 . 110.7(6) yes
C503 . N502 . C514 . 109.3(5) yes
C501 . C502 . N502 . 114.0(6) yes
C501 . C502 . H5021 . 107.0 no
N502 . C502 . H5021 . 108.0 no
C501 . C502 . H5022 . 109.5 no
N502 . C502 . H5022 . 108.7 no
H5021 . C502 . H5022 . 109.5 no
Eu5 . N503 . C504 . 110.7(5) yes
Eu5 . N503 . C505 . 108.1(5) yes
C504 . N503 . C505 . 112.1(6) yes
Eu5 . N503 . C517 . 103.1(9) yes
C504 . N503 . C517 . 111.0(6) yes
C505 . N503 . C517 . 111.5(6) yes
N502 . C503 . C504 . 112.7(6) yes
N502 . C503 . H5031 . 108.7 no
C504 . C503 . H5031 . 108.1 no
N502 . C503 . H5032 . 107.8 no
C504 . C503 . H5032 . 110.0 no
H5031 . C503 . H5032 . 109.5 no
Eu5 . O503 . C518 . 123.3(6) yes
Eu5 . N504 . C506 . 111.9(5) yes
Eu5 . N504 . C507 . 111.0(5) yes
C506 . N504 . C507 . 110.8(6) yes
Eu5 . N504 . C521 . 104.9(7) yes
C506 . N504 . C521 . 109.1(6) yes
C507 . N504 . C521 . 109.0(6) yes
C503 . C504 . N503 . 113.0(6) yes
C503 . C504 . H5041 . 110.0 no
N503 . C504 . H5041 . 109.1 no
C503 . C504 . H5042 . 107.9 no
N503 . C504 . H5042 . 107.4 no
H5041 . C504 . H5042 . 109.5 no
N503 . C505 . C506 . 112.8(7) yes
N503 . C505 . H5051 . 108.3 no
C506 . C505 . H5051 . 109.1 no
N503 . C505 . H5052 . 108.6 no
C506 . C505 . H5052 . 108.4 no
H5051 . C505 . H5052 . 109.5 no
C505 . C506 . N504 . 112.4(7) yes
C505 . C506 . H5061 . 108.8 no
N504 . C506 . H5061 . 108.0 no
C505 . C506 . H5062 . 108.5 no
N504 . C506 . H5062 . 109.6 no
H5061 . C506 . H5062 . 109.5 no
N504 . C507 . C508 . 113.2(6) yes
N504 . C507 . H5071 . 107.6 no
C508 . C507 . H5071 . 108.0 no
N504 . C507 . H5072 . 108.8 no
C508 . C507 . H5072 . 109.6 no
H5071 . C507 . H5072 . 109.5 no
C507 . C508 . N501 . 113.3(6) yes
C507 . C508 . H5081 . 108.0 no
N501 . C508 . H5081 . 108.0 no
C507 . C508 . H5082 . 109.5 no
N501 . C508 . H5082 . 108.5 no
H5081 . C508 . H5082 . 109.5 no
Eu5 . O509 . H5092 . 115.8 no
Eu5 . O509 . H5091 . 133.9 no
H5092 . O509 . H5091 . 100.7 no
N501 . C511 . C512 . 117.5(8) yes
N501 . C511 . H5111 . 107.9 no
C512 . C511 . H5111 . 107.1 no
N501 . C511 . H5112 . 107.2 no
C512 . C511 . H5112 . 107.5 no
H5111 . C511 . H5112 . 109.5 no
C511 . C512 . O501 . 118.65(6) yes
C511 . C512 . O513 . 118.15(6) yes
O501 . C512 . O513 . 123.21(6) yes
N502 . C514 . C515 . 115.2(8) yes
N502 . C514 . H5141 . 107.0 no
C515 . C514 . H5141 . 106.7 no
N502 . C514 . H5142 . 109.1 no
C515 . C514 . H5142 . 109.1 no
H5141 . C514 . H5142 . 109.5 no
C514 . C515 . O502 . 118.65(6) yes
C514 . C515 . O516 . 118.14(6) yes
O502 . C515 . O516 . 123.21(6) yes
C515 . O516 . Eu6 . 139.4(5) yes
N503 . C517 . Eu5 . 51.5(7) yes
N503 . C517 . C518 . 116.7(8) yes
Eu5 . C517 . C518 . 72.8(4) yes
N503 . C517 . H5171 . 107.8 no
Eu5 . C517 . H5171 . 150.2 no
C518 . C517 . H5171 . 107.5 no
N503 . C517 . H5172 . 107.5 no
Eu5 . C517 . H5172 . 98.3 no
C518 . C517 . H5172 . 107.7 no
H5171 . C517 . H5172 . 109.5 no
C517 . C518 . O503 . 118.65(6) yes
C517 . C518 . O519 . 118.15(6) yes
O503 . C518 . O519 . 123.20(6) yes
N504 . C521 . C522 . 121.2(8) yes
N504 . C521 . H5211 . 106.8 no
C522 . C521 . H5211 . 102.8 no
N504 . C521 . H5212 . 107.2 no
C522 . C521 . H5212 . 109.0 no
H5211 . C521 . H5212 . 109.5 no
C521 . C522 . C523 . 121.2(12) yes
C521 . C522 . C527 . 116.8(13) yes
C523 . C522 . C527 . 122.1(12) yes
C522 . C523 . C524 . 115.3(11) yes
C522 . C523 . H5231 . 122.4 no
C524 . C523 . H5231 . 122.3 no
C523 . C524 . O520 . 119.1(8) yes
C523 . C524 . O525 . 121.7(10) yes
O520 . C524 . O525 . 119.1(8) yes
C524 . O525 . C526 . 122.9(13) yes
O525 . C526 . C527 . 123.3(11) yes
O525 . C526 . C531 . 116.8(11) yes
C527 . C526 . C531 . 119.9(5) yes
C522 . C527 . C526 . 114.8(10) yes
C522 . C527 . C528 . 125.3(11) yes
C526 . C527 . C528 . 119.9(5) yes
C527 . C528 . C529 . 120.1(6) yes
C527 . C528 . H5281 . 121.2 no
C529 . C528 . H5281 . 118.7 no
C528 . C529 . C530 . 119.9(5) yes
C528 . C529 . H5291 . 121.4 no
C530 . C529 . H5291 . 118.7 no
C529 . C530 . C531 . 120.0(5) yes
C529 . C530 . O532 . 119.8(6) yes
C531 . C530 . O532 . 120.2(6) yes
C530 . C531 . C526 . 120.1(5) yes
C530 . C531 . H5311 . 121.3 no
C526 . C531 . H5311 . 118.6 no
C530 . O532 . C533 . 118.1(7) yes
O532 . C533 . H5331 . 111.6 no
O532 . C533 . H5333 . 108.2 no
H5331 . C533 . H5333 . 109.5 no
O532 . C533 . H5332 . 108.6 no
H5331 . C533 . H5332 . 109.5 no
H5333 . C533 . H5332 . 109.5 no
O516 . Eu6 . O601 . 131.5(4) yes
O516 . Eu6 . N601 . 145.8(3) yes
O601 . Eu6 . N601 . 65.2(4) yes
O516 . Eu6 . N602 . 80.0(3) yes
O601 . Eu6 . N602 . 118.4(4) yes
N601 . Eu6 . N602 . 66.6(2) yes
O516 . Eu6 . O602 . 75.1(3) yes
O601 . Eu6 . O602 . 74.0(4) yes
N601 . Eu6 . O602 . 84.6(3) yes
N602 . Eu6 . O602 . 65.6(4) yes
O516 . Eu6 . N603 . 69.6(4) yes
O601 . Eu6 . N603 . 157.8(3) yes
N601 . Eu6 . N603 . 101.7(4) yes
N602 . Eu6 . N603 . 66.9(2) yes
O602 . Eu6 . N603 . 124.3(4) yes
O516 . Eu6 . O603 . 64.7(3) yes
O601 . Eu6 . O603 . 111.3(5) yes
N601 . Eu6 . O603 . 144.6(3) yes
N602 . Eu6 . O603 . 130.1(4) yes
O602 . Eu6 . O603 . 129.7(3) yes
O516 . Eu6 . N604 . 131.0(3) yes
O601 . Eu6 . N604 . 90.8(3) yes
N601 . Eu6 . N604 . 66.6(2) yes
N602 . Eu6 . N604 . 102.9(3) yes
O602 . Eu6 . N604 . 151.1(3) yes
O516 . Eu6 . O609 . 74.5(6) yes
O601 . Eu6 . O609 . 61.3(6) yes
N601 . Eu6 . O609 . 125.8(6) yes
N602 . Eu6 . O609 . 136.0(5) yes
O602 . Eu6 . O609 . 73.5(6) yes
N603 . Eu6 . O603 . 68.3(5) yes
N603 . Eu6 . N604 . 67.2(2) yes
O603 . Eu6 . N604 . 78.5(3) yes
N603 . Eu6 . O609 . 131.8(6) yes
O603 . Eu6 . O609 . 67.7(6) yes
N604 . Eu6 . O609 . 120.9(5) yes
Eu6 . O601 . C612 . 123.1(6) yes
Eu6 . N601 . C601 . 111.6(5) yes
Eu6 . N601 . C608 . 109.6(5) yes
C601 . N601 . C608 . 112.2(6) yes
Eu6 . N601 . C611 . 101.7(8) yes
C601 . N601 . C611 . 110.4(6) yes
C608 . N601 . C611 . 110.9(5) yes
N601 . C601 . C602 . 112.8(6) yes
N601 . C601 . H6012 . 108.4 no
C602 . C601 . H6012 . 110.2 no
N601 . C601 . H6011 . 107.5 no
C602 . C601 . H6011 . 108.5 no
H6012 . C601 . H6011 . 109.5 no
C601 . C602 . N602 . 112.7(6) yes
C601 . C602 . H6022 . 107.6 no
N602 . C602 . H6022 . 109.0 no
C601 . C602 . H6021 . 110.2 no
N602 . C602 . H6021 . 107.9 no
H6022 . C602 . H6021 . 109.5 no
C602 . N602 . Eu6 . 110.3(5) yes
C602 . N602 . C603 . 112.4(6) yes
Eu6 . N602 . C603 . 112.4(5) yes
C602 . N602 . C614 . 110.8(6) yes
Eu6 . N602 . C614 . 98.7(8) yes
C603 . N602 . C614 . 111.5(6) yes
Eu6 . O602 . C615 . 120.5(6) yes
N602 . C603 . C604 . 114.2(7) yes
N602 . C603 . H6031 . 107.5 no
C604 . C603 . H6031 . 108.3 no
N602 . C603 . H6032 . 108.1 no
C604 . C603 . H6032 . 109.2 no
H6031 . C603 . H6032 . 109.5 no
Eu6 . N603 . C604 . 109.2(5) yes
Eu6 . N603 . C605 . 110.8(5) yes
C604 . N603 . C605 . 112.9(6) yes
Eu6 . N603 . C617 . 103.6(8) yes
C604 . N603 . C617 . 109.7(5) yes
C605 . N603 . C617 . 110.2(6) yes
Eu6 . O603 . C618 . 123.9(6) yes
C603 . C604 . N603 . 114.4(6) yes
C603 . C604 . H6041 . 107.8 no
N603 . C604 . H6041 . 107.6 no
C603 . C604 . H6042 . 108.3 no
N603 . C604 . H6042 . 109.3 no
H6041 . C604 . H6042 . 109.5 no
Eu6 . N604 . C606 . 108.9(5) yes
Eu6 . N604 . C607 . 112.4(5) yes
C606 . N604 . C607 . 112.3(6) yes
Eu6 . N604 . C621 . 101.8(7) yes
C606 . N604 . C621 . 110.2(6) yes
C607 . N604 . C621 . 110.6(6) yes
N603 . C605 . C606 . 112.7(6) yes
N603 . C605 . H6051 . 108.0 no
C606 . C605 . H6051 . 108.0 no
N603 . C605 . H6052 . 108.9 no
C606 . C605 . H6052 . 109.7 no
H6051 . C605 . H6052 . 109.5 no
C605 . C606 . N604 . 112.7(6) yes
C605 . C606 . H6061 . 109.7 no
N604 . C606 . H6061 . 109.7 no
C605 . C606 . H6062 . 108.4 no
N604 . C606 . H6062 . 106.9 no
H6061 . C606 . H6062 . 109.5 no
N604 . C607 . C608 . 114.0(7) yes
N604 . C607 . H6071 . 108.1 no
C608 . C607 . H6071 . 108.8 no
N604 . C607 . H6072 . 109.6 no
C608 . C607 . H6072 . 106.8 no
H6071 . C607 . H6072 . 109.5 no
C607 . C608 . N601 . 113.3(7) yes
C607 . C608 . H6081 . 107.0 no
N601 . C608 . H6081 . 108.4 no
C607 . C608 . H6082 . 110.2 no
N601 . C608 . H6082 . 108.4 no
H6081 . C608 . H6082 . 109.5 no
Eu6 . O609 . H6092 . 145.5 no
Eu6 . O609 . H6091 . 122.8 no
H6092 . O609 . H6091 . 89.2 no
N601 . C611 . C612 . 110.7(8) yes
N601 . C611 . H6111 . 108.0 no
C612 . C611 . H6111 . 108.0 no
N601 . C611 . H6112 . 110.3 no
C612 . C611 . H6112 . 110.3 no
H6111 . C611 . H6112 . 109.5 no
C611 . C612 . O601 . 118.65(6) yes
C611 . C612 . O613 . 118.15(6) yes
O601 . C612 . O613 . 123.20(6) yes
C612 . O613 . Eu7 . 117.3(5) yes
N602 . C614 . C615 . 109.5(7) yes
N602 . C614 . H6141 . 108.6 no
C615 . C614 . H6141 . 112.1 no
N602 . C614 . H6142 . 108.7 no
C615 . C614 . H6142 . 108.4 no
H6141 . C614 . H6142 . 109.5 no
C614 . C615 . O602 . 118.65(6) yes
C614 . C615 . O616 . 118.15(6) yes
O602 . C615 . O616 . 123.20(6) yes
N603 . C617 . C618 . 118.3(8) yes
N603 . C617 . H6171 . 106.7 no
C618 . C617 . H6171 . 106.7 no
N603 . C617 . H6172 . 107.0 no
C618 . C617 . H6172 . 108.4 no
H6171 . C617 . H6172 . 109.5 no
C617 . C618 . O603 . 118.65(6) yes
C617 . C618 . O619 . 118.15(6) yes
O603 . C618 . O619 . 123.20(6) yes
N604 . C621 . C622 . 116.5(8) yes
N604 . C621 . H6211 . 108.3 no
C622 . C621 . H6211 . 104.4 no
N604 . C621 . H6212 . 108.4 no
C622 . C621 . H6212 . 109.7 no
H6211 . C621 . H6212 . 109.5 no
C621 . C622 . C623 . 120.6(13) yes
C621 . C622 . C627 . 114.9(14) yes
C623 . C622 . C627 . 124.5(13) yes
C622 . C623 . C624 . 113.4(11) yes
C622 . C623 . H6231 . 123.7 no
C624 . C623 . H6231 . 122.9 no
C623 . C624 . O620 . 118.2(8) yes
C623 . C624 . O625 . 123.0(11) yes
O620 . C624 . O625 . 118.7(8) yes
C624 . O625 . C626 . 121.4(13) yes
O625 . C626 . C627 . 124.9(12) yes
O625 . C626 . C631 . 114.9(12) yes
C627 . C626 . C631 . 120.2(5) yes
C622 . C627 . C626 . 112.7(11) yes
C622 . C627 . C628 . 127.4(11) yes
C626 . C627 . C628 . 119.9(5) yes
C627 . C628 . C629 . 120.0(6) yes
C627 . C628 . H6281 . 120.4 no
C629 . C628 . H6281 . 119.6 no
C628 . C629 . C630 . 120.1(5) yes
C628 . C629 . H6291 . 120.4 no
C630 . C629 . H6291 . 119.5 no
C629 . C630 . C631 . 119.9(5) yes
C629 . C630 . O632 . 120.7(6) yes
C631 . C630 . O632 . 119.5(6) yes
C630 . C631 . C626 . 120.1(5) yes
C630 . C631 . H6311 . 120.3 no
C626 . C631 . H6311 . 119.6 no
C630 . O632 . C633 . 119.3(7) yes
O632 . C633 . H6332 . 113.5 no
O632 . C633 . H6333 . 107.8 no
H6332 . C633 . H6333 . 109.5 no
O632 . C633 . H6331 . 107.0 no
H6332 . C633 . H6331 . 109.5 no
H6333 . C633 . H6331 . 109.5 no
O613 . Eu7 . N701 . 136.6(3) yes
O613 . Eu7 . O701 . 93.3(4) yes
N701 . Eu7 . O701 . 66.5(4) yes
O613 . Eu7 . O702 . 142.8(3) yes
N701 . Eu7 . O702 . 77.2(3) yes
O701 . Eu7 . O702 . 87.8(4) yes
O613 . Eu7 . N702 . 134.0(3) yes
N701 . Eu7 . N702 . 66.0(2) yes
O701 . Eu7 . N702 . 129.4(4) yes
O702 . Eu7 . N702 . 65.8(4) yes
O613 . Eu7 . N703 . 69.3(3) yes
N701 . Eu7 . N703 . 101.6(3) yes
O701 . Eu7 . N703 . 140.7(3) yes
O702 . Eu7 . N703 . 127.6(4) yes
N702 . Eu7 . N703 . 66.4(2) yes
O613 . Eu7 . O703 . 76.4(3) yes
N701 . Eu7 . O703 . 141.1(3) yes
O701 . Eu7 . O703 . 144.7(4) yes
O702 . Eu7 . O703 . 81.4(4) yes
N702 . Eu7 . O703 . 75.7(3) yes
O613 . Eu7 . N704 . 71.3(3) yes
N701 . Eu7 . N704 . 66.45(19) yes
O701 . Eu7 . N704 . 74.4(3) yes
O702 . Eu7 . N704 . 143.5(3) yes
N702 . Eu7 . N704 . 101.3(3) yes
O613 . Eu7 . O709 . 78.3(5) yes
N701 . Eu7 . O709 . 128.7(5) yes
O701 . Eu7 . O709 . 77.6(5) yes
O702 . Eu7 . O709 . 65.6(5) yes
N702 . Eu7 . O709 . 121.8(5) yes
O613 . Eu7 . C717 . 59.9(3) yes
N701 . Eu7 . C717 . 125.1(3) yes
O701 . Eu7 . C717 . 151.4(3) yes
O702 . Eu7 . C717 . 119.2(3) yes
N702 . Eu7 . C717 . 74.6(2) yes
O613 . Eu7 . C718 . 68.0(3) yes
N701 . Eu7 . C718 . 138.4(3) yes
O701 . Eu7 . C718 . 155.1(4) yes
O702 . Eu7 . C718 . 97.3(3) yes
N702 . Eu7 . C718 . 74.1(2) yes
N703 . Eu7 . O703 . 67.2(5) yes
N703 . Eu7 . N704 . 66.7(2) yes
O703 . Eu7 . N704 . 130.5(4) yes
N703 . Eu7 . O709 . 128.8(5) yes
O703 . Eu7 . O709 . 67.3(6) yes
N704 . Eu7 . O709 . 136.9(5) yes
N703 . Eu7 . C717 . 25.0(2) yes
O703 . Eu7 . C717 . 44.4(3) yes
N704 . Eu7 . C717 . 86.6(2) yes
O709 . Eu7 . C717 . 104.0(5) yes
N703 . Eu7 . C718 . 49.4(3) yes
O703 . Eu7 . C718 . 18.4(2) yes
N704 . Eu7 . C718 . 112.4(3) yes
O709 . Eu7 . C718 . 82.3(5) yes
C717 . Eu7 . C718 . 26.00(13) yes
Eu7 . N701 . C701 . 109.4(5) yes
Eu7 . N701 . C708 . 110.5(5) yes
C701 . N701 . C708 . 111.0(6) yes
Eu7 . N701 . C711 . 105.5(8) yes
C701 . N701 . C711 . 110.1(5) yes
C708 . N701 . C711 . 110.2(6) yes
N701 . C701 . C702 . 113.2(6) yes
N701 . C701 . H7012 . 108.9 no
C702 . C701 . H7012 . 108.9 no
N701 . C701 . H7011 . 108.5 no
C702 . C701 . H7011 . 107.9 no
H7012 . C701 . H7011 . 109.5 no
Eu7 . O701 . C712 . 125.9(6) yes
Eu7 . O702 . C715 . 125.7(6) yes
Eu7 . N702 . C702 . 113.3(4) yes
Eu7 . N702 . C703 . 111.0(4) yes
C702 . N702 . C703 . 110.1(6) yes
Eu7 . N702 . C714 . 104.1(8) yes
C702 . N702 . C714 . 109.0(6) yes
C703 . N702 . C714 . 109.2(5) yes
C701 . C702 . N702 . 112.9(6) yes
C701 . C702 . H7022 . 107.9 no
N702 . C702 . H7022 . 107.7 no
C701 . C702 . H7021 . 109.5 no
N702 . C702 . H7021 . 109.3 no
H7022 . C702 . H7021 . 109.5 no
N702 . C703 . C704 . 112.9(6) yes
N702 . C703 . H7032 . 108.9 no
C704 . C703 . H7032 . 109.1 no
N702 . C703 . H7031 . 107.5 no
C704 . C703 . H7031 . 108.9 no
H7032 . C703 . H7031 . 109.5 no
Eu7 . N703 . C704 . 111.5(5) yes
Eu7 . N703 . C705 . 108.2(5) yes
C704 . N703 . C705 . 111.5(6) yes
Eu7 . N703 . C717 . 104.9(8) yes
C704 . N703 . C717 . 110.3(6) yes
C705 . N703 . C717 . 110.2(5) yes
Eu7 . O703 . C718 . 124.9(6) yes
C703 . C704 . N703 . 113.0(6) yes
C703 . C704 . H7042 . 108.9 no
N703 . C704 . H7042 . 109.1 no
C703 . C704 . H7041 . 108.2 no
N703 . C704 . H7041 . 108.2 no
H7042 . C704 . H7041 . 109.5 no
Eu7 . N704 . C706 . 111.8(4) yes
Eu7 . N704 . C707 . 110.9(5) yes
C706 . N704 . C707 . 109.9(6) yes
Eu7 . N704 . C721 . 107.0(7) yes
C706 . N704 . C721 . 108.7(6) yes
C707 . N704 . C721 . 108.5(5) yes
N703 . C705 . C706 . 112.3(6) yes
N703 . C705 . H7051 . 107.8 no
C706 . C705 . H7051 . 109.1 no
N703 . C705 . H7052 . 109.8 no
C706 . C705 . H7052 . 108.4 no
H7051 . C705 . H7052 . 109.5 no
C705 . C706 . N704 . 112.2(7) yes
C705 . C706 . H7061 . 109.3 no
N704 . C706 . H7061 . 108.9 no
C705 . C706 . H7062 . 108.3 no
N704 . C706 . H7062 . 108.5 no
H7061 . C706 . H7062 . 109.5 no
N704 . C707 . C708 . 112.2(6) yes
N704 . C707 . H7071 . 108.5 no
C708 . C707 . H7071 . 108.8 no
N704 . C707 . H7072 . 108.1 no
C708 . C707 . H7072 . 109.8 no
H7071 . C707 . H7072 . 109.5 no
C707 . C708 . N701 . 112.5(6) yes
C707 . C708 . H7081 . 108.0 no
N701 . C708 . H7081 . 108.1 no
C707 . C708 . H7082 . 109.8 no
N701 . C708 . H7082 . 109.0 no
H7081 . C708 . H7082 . 109.5 no
Eu7 . O709 . H7092 . 134.4 no
Eu7 . O709 . H7091 . 119.6 no
H7092 . O709 . H7091 . 99.6 no
N701 . C711 . C712 . 115.6(8) yes
N701 . C711 . H7111 . 107.8 no
C712 . C711 . H7111 . 108.3 no
N701 . C711 . H7112 . 108.2 no
C712 . C711 . H7112 . 107.3 no
H7111 . C711 . H7112 . 109.5 no
C711 . C712 . O701 . 118.65(6) yes
C711 . C712 . O713 . 118.15(6) yes
O701 . C712 . O713 . 123.20(6) yes
N702 . C714 . C715 . 113.4(7) yes
N702 . C714 . H7141 . 107.6 no
C715 . C714 . H7141 . 108.4 no
N702 . C714 . H7142 . 109.8 no
C715 . C714 . H7142 . 108.2 no
H7141 . C714 . H7142 . 109.5 no
C714 . C715 . O702 . 118.65(6) yes
C714 . C715 . O716 . 118.15(6) yes
O702 . C715 . O716 . 123.20(6) yes
C715 . O716 . Eu8 . 140.2(5) yes
N703 . C717 . Eu7 . 50.2(6) yes
N703 . C717 . C718 . 116.7(8) yes
Eu7 . C717 . C718 . 72.1(3) yes
N703 . C717 . H7171 . 106.2 no
Eu7 . C717 . H7171 . 114.5 no
C718 . C717 . H7171 . 120.9 no
N703 . C717 . H7172 . 106.6 no
Eu7 . C717 . H7172 . 134.4 no
C718 . C717 . H7172 . 95.4 no
H7171 . C717 . H7172 . 109.5 no
C717 . C718 . O703 . 118.65(6) yes
C717 . C718 . Eu7 . 81.9(4) yes
O703 . C718 . Eu7 . 36.7(4) yes
C717 . C718 . O719 . 118.15(6) yes
O703 . C718 . O719 . 123.21(6) yes
Eu7 . C718 . O719 . 159.9(4) yes
N704 . C721 . C722 . 117.8(7) yes
N704 . C721 . H7211 . 108.5 no
C722 . C721 . H7211 . 106.0 no
N704 . C721 . H7212 . 106.5 no
C722 . C721 . H7212 . 108.4 no
H7211 . C721 . H7212 . 109.5 no
C721 . C722 . C723 . 116.1(11) yes
C721 . C722 . C727 . 121.8(12) yes
C723 . C722 . C727 . 122.0(11) yes
C722 . C723 . C724 . 115.1(10) yes
C722 . C723 . H7231 . 122.0 no
C724 . C723 . H7231 . 122.9 no
C723 . C724 . O720 . 118.7(8) yes
C723 . C724 . O725 . 123.0(10) yes
O720 . C724 . O725 . 118.3(8) yes
C724 . O725 . C726 . 120.6(12) yes
O725 . C726 . C727 . 124.7(10) yes
O725 . C726 . C731 . 115.5(10) yes
C727 . C726 . C731 . 119.7(5) yes
C722 . C727 . C726 . 114.4(9) yes
C722 . C727 . C728 . 125.5(10) yes
C726 . C727 . C728 . 120.0(5) yes
C727 . C728 . C729 . 120.2(5) yes
C727 . C728 . H7281 . 120.9 no
C729 . C728 . H7281 . 118.9 no
C728 . C729 . C730 . 119.8(5) yes
C728 . C729 . H7291 . 121.1 no
C730 . C729 . H7291 . 119.1 no
C729 . C730 . C731 . 120.1(5) yes
C729 . C730 . O732 . 120.3(6) yes
C731 . C730 . O732 . 119.6(6) yes
C730 . C731 . C726 . 120.1(5) yes
C730 . C731 . H7311 . 120.9 no
C726 . C731 . H7311 . 118.9 no
C730 . O732 . C733 . 118.8(7) yes
O732 . C733 . H7331 . 112.7 no
O732 . C733 . H7333 . 107.6 no
H7331 . C733 . H7333 . 109.5 no
O732 . C733 . H7332 . 108.1 no
H7331 . C733 . H7332 . 109.5 no
H7333 . C733 . H7332 . 109.5 no
O716 . Eu8 . O801 . 133.3(4) yes
O716 . Eu8 . N801 . 145.9(3) yes
O801 . Eu8 . N801 . 63.8(4) yes
O716 . Eu8 . N802 . 79.6(3) yes
O801 . Eu8 . N802 . 116.8(4) yes
N801 . Eu8 . N802 . 66.7(2) yes
O716 . Eu8 . O802 . 74.6(3) yes
O801 . Eu8 . O802 . 73.7(4) yes
N801 . Eu8 . O802 . 86.8(3) yes
N802 . Eu8 . O802 . 66.6(4) yes
O716 . Eu8 . O803 . 64.7(3) yes
O801 . Eu8 . O803 . 112.8(5) yes
N801 . Eu8 . O803 . 144.0(3) yes
N802 . Eu8 . O803 . 130.4(4) yes
O802 . Eu8 . O803 . 128.0(3) yes
O716 . Eu8 . N804 . 129.6(3) yes
O801 . Eu8 . N804 . 91.1(3) yes
N801 . Eu8 . N804 . 66.6(2) yes
N802 . Eu8 . N804 . 103.2(3) yes
O802 . Eu8 . N804 . 153.3(3) yes
O716 . Eu8 . O809 . 72.6(5) yes
O801 . Eu8 . O809 . 64.7(5) yes
N801 . Eu8 . O809 . 127.5(5) yes
N802 . Eu8 . O809 . 132.9(5) yes
O802 . Eu8 . O809 . 69.8(6) yes
O803 . Eu8 . N804 . 77.9(3) yes
O803 . Eu8 . O809 . 68.3(5) yes
N804 . Eu8 . O809 . 123.8(5) yes
Eu8 . O801 . C812 . 124.5(6) yes
Eu8 . N801 . C801 . 110.8(5) yes
Eu8 . N801 . C808 . 109.5(5) yes
C801 . N801 . C808 . 111.4(6) yes
Eu8 . N801 . C811 . 103.7(8) yes
C801 . N801 . C811 . 109.9(6) yes
C808 . N801 . C811 . 111.3(5) yes
N801 . C801 . C802 . 112.1(6) yes
N801 . C801 . H8012 . 109.3 no
C802 . C801 . H8012 . 109.6 no
N801 . C801 . H8011 . 107.9 no
C802 . C801 . H8011 . 108.4 no
H8012 . C801 . H8011 . 109.5 no
C801 . C802 . N802 . 112.4(6) yes
C801 . C802 . H8022 . 109.6 no
N802 . C802 . H8022 . 107.9 no
C801 . C802 . H8021 . 108.5 no
N802 . C802 . H8021 . 108.9 no
H8022 . C802 . H8021 . 109.5 no
C802 . N802 . Eu8 . 110.5(5) yes
C802 . N802 . C803 . 111.9(6) yes
Eu8 . N802 . C803 . 112.3(5) yes
C802 . N802 . C814 . 110.6(6) yes
Eu8 . N802 . C814 . 99.3(8) yes
C803 . N802 . C814 . 111.6(6) yes
Eu8 . O802 . C815 . 121.0(6) yes
N802 . C803 . C804 . 114.3(7) yes
N802 . C803 . H8032 . 107.8 no
C804 . C803 . H8032 . 109.3 no
N802 . C803 . H8031 . 107.6 no
C804 . C803 . H8031 . 108.2 no
H8032 . C803 . H8031 . 109.5 no
C804 . N803 . C805 . 112.7(6) yes
C804 . N803 . C817 . 110.4(5) yes
C805 . N803 . C817 . 110.8(6) yes
Eu8 . O803 . C818 . 124.0(6) yes
C803 . C804 . N803 . 114.2(6) yes
C803 . C804 . H8042 . 107.3 no
N803 . C804 . H8042 . 106.8 no
C803 . C804 . H8041 . 109.3 no
N803 . C804 . H8041 . 109.7 no
H8042 . C804 . H8041 . 109.5 no
Eu8 . N804 . C806 . 108.5(5) yes
Eu8 . N804 . C807 . 112.5(5) yes
C806 . N804 . C807 . 112.2(6) yes
Eu8 . N804 . C821 . 101.7(8) yes
C806 . N804 . C821 . 111.0(6) yes
C807 . N804 . C821 . 110.5(6) yes
N803 . C805 . C806 . 111.6(6) yes
N803 . C805 . H8052 . 107.4 no
C806 . C805 . H8052 . 107.7 no
N803 . C805 . H8051 . 110.6 no
C806 . C805 . H8051 . 110.0 no
H8052 . C805 . H8051 . 109.5 no
C805 . C806 . N804 . 111.4(6) yes
C805 . C806 . H8062 . 110.0 no
N804 . C806 . H8062 . 108.8 no
C805 . C806 . H8061 . 109.2 no
N804 . C806 . H8061 . 107.9 no
H8062 . C806 . H8061 . 109.5 no
N804 . C807 . C808 . 113.4(7) yes
N804 . C807 . H8071 . 108.0 no
C808 . C807 . H8071 . 108.9 no
N804 . C807 . H8072 . 108.8 no
C808 . C807 . H8072 . 108.3 no
H8071 . C807 . H8072 . 109.5 no
C807 . C808 . N801 . 113.5(7) yes
C807 . C808 . H8081 . 108.3 no
N801 . C808 . H8081 . 108.8 no
C807 . C808 . H8082 . 108.6 no
N801 . C808 . H8082 . 108.1 no
H8081 . C808 . H8082 . 109.5 no
Eu8 . O809 . H8092 . 119.2 no
Eu8 . O809 . H8091 . 147.2 no
H8092 . O809 . H8091 . 88.6 no
N801 . C811 . C812 . 108.5(8) yes
N801 . C811 . H8111 . 108.4 no
C812 . C811 . H8111 . 109.1 no
N801 . C811 . H8112 . 111.2 no
C812 . C811 . H8112 . 110.2 no
H8111 . C811 . H8112 . 109.5 no
C811 . C812 . O801 . 118.65(6) yes
C811 . C812 . O813 . 118.15(6) yes
O801 . C812 . O813 . 123.20(6) yes
Eu5 . O813 . C812 . 116.9(5) yes
N802 . C814 . C815 . 112.1(8) yes
N802 . C814 . H8141 . 108.3 no
C815 . C814 . H8141 . 109.2 no
N802 . C814 . H8142 . 108.8 no
C815 . C814 . H8142 . 109.0 no
H8141 . C814 . H8142 . 109.5 no
C814 . C815 . O802 . 118.65(6) yes
C814 . C815 . O816 . 118.15(6) yes
O802 . C815 . O816 . 123.20(6) yes
N803 . C817 . C818 . 118.5(8) yes
N803 . C817 . H8171 . 107.5 no
C818 . C817 . H8171 . 107.0 no
N803 . C817 . H8172 . 106.2 no
C818 . C817 . H8172 . 108.0 no
H8171 . C817 . H8172 . 109.5 no
C817 . C818 . O803 . 118.64(6) yes
C817 . C818 . O819 . 118.15(6) yes
O803 . C818 . O819 . 123.21(6) yes
N804 . C821 . C822 . 111.8(8) yes
N804 . C821 . H8211 . 109.2 no
C822 . C821 . H8211 . 107.0 no
N804 . C821 . H8212 . 108.9 no
C822 . C821 . H8212 . 110.5 no
H8211 . C821 . H8212 . 109.5 no
C821 . C822 . C823 . 120.0(13) yes
C821 . C822 . C827 . 115.6(14) yes
C823 . C822 . C827 . 124.4(14) yes
C822 . C823 . C824 . 113.4(12) yes
C822 . C823 . H8231 . 123.1 no
C824 . C823 . H8231 . 123.5 no
C823 . C824 . O820 . 118.4(8) yes
C823 . C824 . O825 . 122.9(11) yes
O820 . C824 . O825 . 118.6(8) yes
C824 . O825 . C826 . 121.5(14) yes
O825 . C826 . C827 . 124.7(12) yes
O825 . C826 . C831 . 115.4(12) yes
C827 . C826 . C831 . 119.9(5) yes
C822 . C827 . C826 . 113.0(11) yes
C822 . C827 . C828 . 126.8(12) yes
C826 . C827 . C828 . 120.3(5) yes
C827 . C828 . C829 . 119.9(6) yes
C827 . C828 . H8281 . 120.3 no
C829 . C828 . H8281 . 119.9 no
C828 . C829 . C830 . 119.8(5) yes
C828 . C829 . H8291 . 120.2 no
C830 . C829 . H8291 . 119.9 no
C829 . C830 . C831 . 120.3(5) yes
C829 . C830 . O832 . 119.9(6) yes
C831 . C830 . O832 . 119.8(6) yes
C826 . C831 . C830 . 119.9(5) yes
C826 . C831 . H8311 . 119.9 no
C830 . C831 . H8311 . 120.3 no
C830 . O832 . C833 . 118.3(7) yes
O832 . C833 . H8331 . 112.9 no
O832 . C833 . H8332 . 108.1 no
H8331 . C833 . H8332 . 109.5 no
O832 . C833 . H8333 . 107.4 no
H8331 . C833 . H8333 . 109.5 no
H8332 . C833 . H8333 . 109.5 no
loop_
_geom_hbond_atom_site_label_D
_geom_hbond_site_symmetry_D
_geom_hbond_atom_site_label_H
_geom_hbond_site_symmetry_H
_geom_hbond_atom_site_label_A
_geom_hbond_site_symmetry_A
_geom_hbond_angle_DHA
_geom_hbond_distance_DH
_geom_hbond_distance_HA
_geom_hbond_distance_DA
_geom_hbond_publ_flag
C101 . H1012 . C115 . 126 0.95 2.49 3.143(18) yes
C103 . H1032 . C118 . 125 0.95 2.37 3.019(18) yes
C106 . H1062 . C123 . 139 0.95 2.54 3.321(18) yes
C121 . H1212 . C412 . 125 0.95 2.55 3.186(18) yes
C121 . H1212 . O413 . 123 0.95 2.28 2.916(18) yes
C131 . H1311 . O432 2_676 157 0.95 2.52 3.419(18) yes
C202 . H2021 . O816 2_666 121 0.95 2.58 3.174(18) yes
C202 . H2022 . C718 2_666 136 0.95 2.49 3.244(18) yes
C202 . H2022 . O719 2_666 163 0.95 1.71 2.635(18) yes
C206 . H2062 . C218 . 126 0.95 2.56 3.208(18) yes
C207 . H2071 . C223 . 142 0.95 2.40 3.208(18) yes
C211 . H2112 . O719 2_666 162 0.95 2.55 3.470(18) yes
C221 . H2211 . O203 . 127 0.95 2.42 3.080(18) yes
C221 . H2211 . C228 . 120 0.95 2.39 2.981(18) yes
C221 . H2212 . O201 . 130 0.95 2.58 3.265(18) yes
C301 . H3012 . C315 . 126 0.95 2.39 3.055(18) yes
C306 . H3061 . C323 . 140 0.95 2.52 3.304(18) yes
C306 . H3062 . O820 1_556 147 0.95 2.42 3.256(18) yes
C307 . H3072 . C312 . 124 0.95 2.57 3.209(18) yes
C321 . H3211 . C212 . 125 0.95 2.53 3.173(18) yes
C321 . H3211 . O213 . 121 0.95 2.30 2.909(18) yes
C331 . H3311 . O232 2_777 159 0.95 2.58 3.487(18) yes
C403 . H4032 . O119 2_666 129 0.95 2.55 3.234(18) yes
C406 . H4061 . C418 . 126 0.95 2.49 3.141(18) yes
C406 . H4061 . C428 . 130 0.95 2.42 3.119(18) yes
C407 . H4071 . C423 . 144 0.95 2.37 3.188(18) yes
C421 . H4211 . O403 . 124 0.95 2.47 3.095(18) yes
C503 . H5032 . C518 . 123 0.95 2.53 3.150(18) yes
C505 . H5052 . O813 . 124 0.95 2.26 2.904(18) yes
C506 . H5061 . C523 . 141 0.95 2.52 3.310(18) yes
C506 . H5062 . O220 1_454 136 0.95 2.54 3.289(18) yes
C521 . H5211 . O501 . 129 0.95 2.52 3.207(18) yes
C521 . H5212 . C812 . 131 0.95 2.43 3.142(18) yes
C521 . H5212 . O813 . 132 0.95 1.94 2.668(18) yes
C531 . H5311 . O832 2_675 159 0.95 2.59 3.496(18) yes
C607 . H6071 . C623 . 137 0.95 2.60 3.359(18) yes
C614 . H6141 . O516 . 121 0.95 2.37 2.967(18) yes
C631 . H6311 . O732 2_576 156 0.95 2.50 3.389(18) yes
C701 . H7011 . C715 . 125 0.95 2.58 3.223(18) yes
C705 . H7052 . O613 . 122 0.95 2.40 3.004(18) yes
C706 . H7061 . C723 . 138 0.95 2.56 3.332(18) yes
C706 . H7062 . O420 . 157 0.95 2.36 3.257(18) yes
C706 . H7062 . C424 . 127 0.95 2.50 3.168(18) yes
C707 . H7072 . C712 . 124 0.95 2.57 3.204(18) yes
C721 . H7211 . O601 . 125 0.95 2.53 3.165(18) yes
C721 . H7211 . O701 . 129 0.95 2.60 3.273(18) yes
C731 . H7311 . O632 2_576 162 0.95 2.47 3.391(18) yes
C801 . H8011 . O519 2_565 155 0.95 2.40 3.282(18) yes
C806 . H8062 . C818 . 127 0.95 2.58 3.247(18) yes
C806 . H8062 . C828 . 136 0.95 2.48 3.236(18) yes
C807 . H8071 . C823 . 139 0.95 2.50 3.278(18) yes
C811 . H8111 . O519 2_565 129 0.95 2.49 3.181(18) yes
O109 . H1091 . O402 . 178 0.95 1.98 2.927(18) yes
O209 . H2092 . O102 . 178 0.95 1.69 2.637(18) yes
O209 . H2092 . C115 . 146 0.95 2.31 3.142(18) yes
O209 . H2091 . O301 . 127 0.95 2.23 2.897(18) yes
O309 . H3092 . O202 . 179 0.95 1.95 2.905(18) yes
O309 . H3091 . O416 . 178 0.95 2.40 3.349(18) yes
O409 . H4092 . O101 . 120 0.95 2.20 2.799(18) yes
O409 . H4091 . O302 . 178 0.95 1.83 2.784(18) yes
O409 . H4091 . C315 . 149 0.95 2.42 3.273(18) yes
O509 . H5091 . O802 . 178 0.95 1.95 2.900(18) yes
O609 . H6091 . O701 . 178 0.95 1.81 2.755(18) yes
O609 . H6091 . C712 . 152 0.95 2.56 3.430(18) yes
O709 . H7092 . O602 . 178 0.95 2.08 3.025(18) yes
O709 . H7091 . O816 . 177 0.95 2.32 3.273(18) yes
O809 . H8092 . O501 . 177 0.95 1.94 2.884(18) yes


####################################################################### 
# 
# This file contains crystal structure data downloaded from the 
# Cambridge Structural Database (CSD) hosted by the Cambridge 
# Crystallographic Data Centre (CCDC).
# 
# Full information about CCDC data access policies and citation 
# guidelines are available at http://www.ccdc.cam.ac.uk/access/V1 
# 
# Audit and citation data items may have been added by the CCDC. 
# Please retain this information to preserve the provenance of 
# this file and to allow appropriate attribution of the data. 
# 
#######################################################################

data_EuL-Orthorhombic
_database_code_depnum_ccdc_archive 'CCDC 1589837'
_audit_update_record             
;
2017-12-07 deposited with the CCDC.
2018-02-05 downloaded from the CCDC.
;
#==============================================================================
_audit_creation_date             2017-11-27
_audit_creation_method           CRYSTALS_ver_14.61_build_6156

_oxford_structure_analysis_title 6769ROD
_chemical_name_systematic        .
_chemical_melting_point          'not measured'

_refine_special_details          
; 
This was the third and final attempt to collect data on 
this material, using a state of the art laboratory 
instrument provided by the instrument manufacturer.  
The data were still very weak and exhibited streaks and 
additional non-Bragg features.  The structure still
solved however, this time with only one molecule in 
the asymmetric unit and in the orthorhombic system.
It was possible to identify a number of partial triflate
anions, which had not been visible in the previous 
structures.  Despite this, most were unstable and only
one is included in the model.  It was not possible to
have another attempt to determine the structure as the
crystals had deteriorated further.

The difference map indicated the presence of diffuse electron
density believed to be a mixture of disordered solvent 
and sodium triflate.  SQUEEZE was used leaving a void 

from which the electron density was removed.
;

loop_
_platon_squeeze_void_nr
_platon_squeeze_void_average_x
_platon_squeeze_void_average_y
_platon_squeeze_void_average_z
_platon_squeeze_void_volume
_platon_squeeze_void_count_electrons
_platon_squeeze_void_content
1 0.814 0.008 0.126 7676 3612 ' '
_platon_squeeze_void_probe_radius 1.20
_platon_squeeze_details          
; 
The discrete Fourier transform of the void region were treated as 
contributions to the A and B parts of the calculated structure factors.
;

_cell_length_a                   17.9227(7)
_cell_length_b                   32.9420(9)
_cell_length_c                   47.9786(16)
_cell_angle_alpha                90
_cell_angle_beta                 90
_cell_angle_gamma                90
_cell_volume                     28326.9(16)

_symmetry_cell_setting           orthorhombic
_symmetry_space_group_name_H-M   'P c a n '
_symmetry_space_group_name_Hall  '-P 2n 2c'
loop_
_symmetry_equiv_pos_as_xyz
x,y,z
-x,-y,-z
x+1/2,-y+1/2,z
-x+1/2,y+1/2,-z
-x+1/2,-y+1/2,z+1/2
x+1/2,y+1/2,-z+1/2
x,-y,-z+1/2
-x,y,z+1/2

loop_
_atom_type_symbol
_atom_type_scat_dispersion_real
_atom_type_scat_dispersion_imag
_atom_type_scat_Cromer_Mann_a1
_atom_type_scat_Cromer_Mann_b1
_atom_type_scat_Cromer_Mann_a2
_atom_type_scat_Cromer_Mann_b2
_atom_type_scat_Cromer_Mann_a3
_atom_type_scat_Cromer_Mann_b3
_atom_type_scat_Cromer_Mann_a4
_atom_type_scat_Cromer_Mann_b4
_atom_type_scat_Cromer_Mann_c
_atom_type_scat_source
C 0.0181 0.0091 2.3100 20.8439 1.0200 10.2075 1.5886 0.5687 0.8650 51.6512
0.2156 'International Tables Vol C 4.2.6.8 and 6.1.1.4'
H 0.0000 0.0000 0.4930 10.5109 0.3229 26.1257 0.1402 3.1424 0.0408 57.7998
0.0030 'International Tables Vol C 4.2.6.8 and 6.1.1.4'
N 0.0311 0.0180 12.2126 0.0057 3.1322 9.8933 2.0125 28.9975 1.1663 0.5826
-11.5290 'International Tables Vol C 4.2.6.8 and 6.1.1.4'
O 0.0492 0.0322 3.0485 13.2771 2.2868 5.7011 1.5463 0.3239 0.8670 32.9089
0.2508 'International Tables Vol C 4.2.6.8 and 6.1.1.4'
Eu -8.9294 11.1857 24.6274 2.3879 19.0886 0.1942 13.7603 13.7546 2.9227
123.1740 2.5745 'International Tables Vol C 4.2.6.8 and 6.1.1.4'
F 0.0727 0.0534 3.5392 10.2825 2.6412 4.2944 1.5170 0.2615 1.0243 26.1476
0.2776 'International Tables Vol C 4.2.6.8 and 6.1.1.4'
S 0.3331 0.5567 6.9053 1.4679 5.2034 22.2151 1.4379 0.2536 1.5863 56.1720
0.8669 'International Tables Vol C 4.2.6.8 and 6.1.1.4'
Na 0.1353 0.1239 4.7626 3.2850 3.1736 8.8422 1.2674 0.3136 1.1128 129.4240
0.6760 'International Tables Vol C 4.2.6.8 and 6.1.1.4'
Cl 0.3639 0.7018 11.4604 0.0104 7.1964 1.1662 6.2556 18.5194 1.6455 47.7784
-9.5574 'International Tables Vol C 4.2.6.8 and 6.1.1.4'


_cell_formula_units_Z            8

# Given Formula = C125 H125 Cl1 Eu2 F6 N8 Na1 O30 S2 
# Dc =      1.29 Fooo =  11288.00 Mu =     74.03 M =   2759.89
# Found Formula = C101 H134 Eu4 F3 N16 Na1 O44 S1 
# Dc =      1.41 FOOO =  12080.00 Mu =    133.56 M =   2996.16

_chemical_formula_sum            'C101 H134 Eu4 F3 N16 Na1 O44 S1'
_chemical_formula_moiety         'C101 H134 Eu4 F3 N16 Na1 O44 S1'
_chemical_compound_source        .
_chemical_formula_weight         2996.16


_cell_measurement_reflns_used    14291
_cell_measurement_theta_min      5
_cell_measurement_theta_max      60
_cell_measurement_temperature    90

_exptl_crystal_description       plate
_exptl_crystal_colour            clear_pale_yellow
_exptl_crystal_size_min          0.040
_exptl_crystal_size_mid          0.085
_exptl_crystal_size_max          0.085

_exptl_crystal_density_diffrn    1.405
_exptl_crystal_density_meas      'not measured'
_exptl_crystal_density_method    'not measured'
# Non-dispersive F(000): 
_exptl_crystal_F_000             12080
_exptl_absorpt_coefficient_mu    13.356

# Sheldrick geometric approximatio 0.32 0.59 
_exptl_absorpt_correction_type   multi-scan
_exptl_absorpt_process_details   'CrysAlisPro, (Agilent, 2011)'
_exptl_absorpt_correction_T_min  0.38
_exptl_absorpt_correction_T_max  0.59
_diffrn_measurement_device_type  'XtaLAB Synergy, Dualflex, HyPix'
_diffrn_detector                 'CCD plate'
_diffrn_detector_type            HyPix
_diffrn_radiation_monochromator  mirror
_diffrn_radiation_type           'Cu K\a'
_diffrn_radiation_wavelength     1.54180
_diffrn_measurement_method       ω

# If a reference occurs more than once, delete the author 
# and date from subsequent references. 
_computing_data_collection       'CrysAlisPro 1.171.39.30t (Rigaku OD, 2017)'
_computing_cell_refinement       'CrysAlisPro 1.171.39.30t (Rigaku OD, 2017)'
_computing_data_reduction        'CrysAlisPro 1.171.39.30t (Rigaku OD, 2017)'
_computing_structure_solution    'Superflip (Palatinus & Chapuis, 2007)'
_computing_structure_refinement  'CRYSTALS (Betteridge et al., 2003)'
_computing_publication_material  'CRYSTALS (Betteridge et al., 2003)'
_computing_molecular_graphics    'CAMERON (Watkin et al., 1996)'

_diffrn_standards_interval_time  .
_diffrn_standards_interval_count .
_diffrn_standards_number         0
_diffrn_standards_decay_%        .

_diffrn_ambient_temperature      90
_diffrn_reflns_number            103297
_reflns_number_total             19887
_diffrn_reflns_av_R_equivalents  0.121
_diffrn_reflns_av_sigmaI/netI    0.1437
# Number of reflections without Friedels Law is 38471 
# Number of reflections with Friedels Law is 21697 
# Theoretical number of reflections is about 14832 


_diffrn_reflns_theta_min         3.685
_diffrn_reflns_theta_max         58.931
_diffrn_measured_fraction_theta_max 0.998

_diffrn_reflns_theta_full        58.931
_diffrn_measured_fraction_theta_full 0.998


_diffrn_reflns_limit_h_min       -19
_diffrn_reflns_limit_h_max       18
_diffrn_reflns_limit_k_min       -36
_diffrn_reflns_limit_k_max       28
_diffrn_reflns_limit_l_min       -53
_diffrn_reflns_limit_l_max       44
_reflns_limit_h_min              -19
_reflns_limit_h_max              19
_reflns_limit_k_min              0
_reflns_limit_k_max              36
_reflns_limit_l_min              0
_reflns_limit_l_max              53

_oxford_diffrn_Wilson_B_factor   4.00
_oxford_diffrn_Wilson_scale      42.99

_atom_sites_solution_primary     Other #heavy,direct,difmap,geom,iterative
# _atom_sites_solution_secondary  difmap
_atom_sites_solution_hydrogens   difmap

_refine_diff_density_min         -5.30
_refine_diff_density_max         8.30


# The current dictionary definitions do not cover the 
# situation where the reflections used for refinement were 
# selected by a user-defined sigma threshold 


# The values actually used during refinement 
_oxford_reflns_threshold_expression_ref I>-3.0\s(I)
_refine_ls_number_reflns         27811
_refine_ls_number_restraints     4401
_refine_ls_number_parameters     1525
_oxford_refine_ls_R_factor_ref   0.1953
_refine_ls_wR_factor_ref         0.4689
_refine_ls_goodness_of_fit_ref   0.9996
_refine_ls_shift/su_max          0.0018082
_refine_ls_shift/su_mean         0.0000714


# The values computed with all filters except I/sigma 
_oxford_reflns_number_all        27812
_refine_ls_R_factor_all          0.1953
_refine_ls_wR_factor_all         0.4690

# The values computed with a 2 sigma cutoff - a la SHELX 
_reflns_threshold_expression     I>2.0σ(I)
_reflns_number_gt                19887
_refine_ls_R_factor_gt           0.1745
_refine_ls_wR_factor_gt          0.4583

# choose from: rm (reference molecule of known chirality), 
# ad (anomolous dispersion - Flack), rmad (rm and ad), 
# syn (from synthesis), unk (unknown) or . (not applicable). 
_chemical_absolute_configuration .


_refine_ls_structure_factor_coef Fsqd
_refine_ls_matrix_type           full
_refine_ls_hydrogen_treatment    constr #undef, noref, refall,
# refxyz, refU, constr or mixed
_refine_ls_weighting_scheme      calc
_refine_ls_weighting_details     
;
 Method= Modified Sheldrick 
 w=1/[σ²(F²) + ( 0.20P)² + 0.00P] 
 ,where P=(max(Fo²,0) + 2Fc²)/3 
;

# Uequiv = arithmetic mean of Ui i.e. Ueqiv = (U1+U2+U3)/3

# Replace last . with number of unfound hydrogen atoms attached to an atom.

# ..._refinement_flags_... 
# . no refinement constraints           S special position constraint on site
# G rigid group refinement of site      R riding atom
# D distance or angle restraint on site T thermal displacement constraints
# U Uiso or Uij restraint (rigid bond)  P partial occupancy constraint


loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_U_iso_or_equiv
_atom_site_occupancy
_atom_site_adp_type
_atom_site_refinement_flags_posn
_atom_site_refinement_flags_adp
_atom_site_refinement_flags_occupancy
_atom_site_disorder_assembly
_atom_site_disorder_group
_atom_site_attached_hydrogens
Eu1 Eu 0.27100(7) 0.58335(3) 0.58937(3) 0.0511 1.0000 Uani . . . . . .
N101 N 0.3551(8) 0.6426(4) 0.5655(3) 0.0627 1.0000 Uani D U . . . .
N102 N 0.4177(9) 0.5640(4) 0.5865(3) 0.0605 1.0000 Uani D U . . . .
N103 N 0.3357(8) 0.5725(4) 0.6390(3) 0.0621 1.0000 Uani D U . . . .
N104 N 0.2762(6) 0.6525(4) 0.6206(3) 0.0558 1.0000 Uani D U . . . .
O101 O 0.2971(5) 0.5742(4) 0.5411(3) 0.0625 1.0000 Uani D U . . . .
O102 O 0.2949(6) 0.5113(3) 0.59522(18) 0.0556 1.0000 Uani D U . . . .
O103 O 0.1889(7) 0.5701(2) 0.6259(3) 0.0557 1.0000 Uani D U . . . .
O109 O 0.1683(7) 0.5378(3) 0.5670(3) 0.0558 1.0000 Uani . U . . . .
C101 C 0.4346(9) 0.6336(5) 0.5713(5) 0.0672 1.0000 Uani D U . . . .
C102 C 0.4553(12) 0.5897(4) 0.5657(4) 0.0673 1.0000 Uani D U . . . .
C103 C 0.4506(11) 0.5705(6) 0.6144(3) 0.0687 1.0000 Uani D U . . . .
C104 C 0.4060(9) 0.5492(6) 0.6372(4) 0.0670 1.0000 Uani D U . . . .
C105 C 0.3509(10) 0.6129(4) 0.6512(5) 0.0677 1.0000 Uani D U . . . .
C106 C 0.2895(9) 0.6441(5) 0.6504(3) 0.0550 1.0000 Uani D U . . . .
C107 C 0.3340(10) 0.6814(5) 0.6105(3) 0.0582 1.0000 Uani D U . . . .
C108 C 0.3333(12) 0.6811(4) 0.5790(3) 0.0625 1.0000 Uani D U . . . .
C111 C 0.3349(5) 0.6436(5) 0.5358(3) 0.0692 1.0000 Uani D U . . . .
C112 C 0.3070(5) 0.6038(4) 0.5243(3) 0.0591 1.0000 Uani D U . . . .
O113 O 0.2943(5) 0.6006(4) 0.4990(3) 0.0720 1.0000 Uani D U . . . .
C114 C 0.4168(8) 0.5220(4) 0.5760(2) 0.0607 1.0000 Uani D U . . . .
C115 C 0.3551(7) 0.4948(4) 0.5858(2) 0.0551 1.0000 Uani D U . . . .
O116 O 0.3611(7) 0.4570(3) 0.58490(19) 0.0631 1.0000 Uani D U . . . .
C117 C 0.2829(8) 0.5507(3) 0.6569(4) 0.0663 1.0000 Uani D U . . . .
C118 C 0.2026(8) 0.5614(3) 0.6512(3) 0.0657 1.0000 Uani D U . . . .
O119 O 0.1559(9) 0.5606(3) 0.6703(3) 0.0923 1.0000 Uani D U . . . .
O120 O 0.2090(6) 0.8161(3) 0.6470(3) 0.0941 1.0000 Uani D U . . . .
C121 C 0.2054(7) 0.6736(5) 0.6195(3) 0.0572 1.0000 Uani D U . . . .
C122 C 0.1831(6) 0.7085(4) 0.6403(3) 0.0557 1.0000 Uani D U . . . .
C123 C 0.2088(7) 0.7463(3) 0.6329(3) 0.0647 1.0000 Uani D U . . . .
C124 C 0.1890(6) 0.7806(4) 0.6518(2) 0.0802 1.0000 Uani D U . . . .
O125 O 0.1471(5) 0.7734(3) 0.6759(2) 0.0832 1.0000 Uani D U . . . .
C126 C 0.1234(6) 0.7352(4) 0.6822(3) 0.0723 1.0000 Uani D U . . . .
C127 C 0.1396(6) 0.7019(4) 0.6654(3) 0.0611 1.0000 Uani D U . . . .
C128 C 0.1114(6) 0.6645(5) 0.6744(3) 0.0668 1.0000 Uani D U . . . .
C129 C 0.0695(7) 0.6596(6) 0.6986(3) 0.0756 1.0000 Uani D U . . . .
C130 C 0.0550(7) 0.6940(5) 0.7145(3) 0.0829 1.0000 Uani D U . . . .
C131 C 0.0814(6) 0.7319(6) 0.7065(3) 0.0753 1.0000 Uani D U . . . .
O132 O 0.0166(6) 0.6972(6) 0.7378(3) 0.0976 1.0000 Uani D U . . . .
C133 C -0.0105(9) 0.6567(7) 0.7455(5) 0.1196 1.0000 Uani D U . . . .
Eu2 Eu 0.29732(8) 0.39357(4) 0.59432(3) 0.0606 1.0000 Uani . . . . . .
N201 N 0.2384(9) 0.3271(4) 0.5689(3) 0.0708 1.0000 Uani D U . . . .
N202 N 0.3356(9) 0.3863(4) 0.5414(3) 0.0705 1.0000 Uani D U . . . .
N203 N 0.4436(10) 0.3812(4) 0.5896(3) 0.0707 1.0000 Uani D U . . . .
N204 N 0.3387(9) 0.3221(5) 0.6179(3) 0.0775 1.0000 Uani D U . . . .
O201 O 0.1739(8) 0.3721(3) 0.6084(3) 0.0663 1.0000 Uani D U . . . .
O202 O 0.2222(7) 0.4268(3) 0.5595(2) 0.0660 1.0000 Uani D U . . . .
O203 O 0.3621(8) 0.4091(3) 0.6362(3) 0.0756 1.0000 Uani D U . . . .
O209 O 0.2300(8) 0.4468(4) 0.6199(3) 0.0611 1.0000 Uani . U . . . .
C201 C 0.2704(14) 0.3199(5) 0.5411(4) 0.0791 1.0000 Uani D U . . . .
C202 C 0.2921(13) 0.3570(5) 0.5247(4) 0.0778 1.0000 Uani D U . . . .
C203 C 0.4150(9) 0.3751(7) 0.5374(4) 0.0768 1.0000 Uani D U . . . .
C204 C 0.4669(11) 0.3880(6) 0.5606(3) 0.0708 1.0000 Uani D U . . . .
C205 C 0.4566(14) 0.3378(5) 0.5957(5) 0.0833 1.0000 Uani D U . . . .
C206 C 0.4208(9) 0.3216(7) 0.6221(4) 0.0869 1.0000 Uani D U . . . .
C207 C 0.3135(12) 0.2872(5) 0.6008(5) 0.0845 1.0000 Uani D U . . . .
C208 C 0.2412(12) 0.2885(5) 0.5848(5) 0.0841 1.0000 Uani D U . . . .
C211 C 0.1601(9) 0.3391(3) 0.5649(3) 0.0714 1.0000 Uani D U . . . .
C212 C 0.1276(9) 0.3587(3) 0.5905(3) 0.0755 1.0000 Uani D U . . . .
O213 O 0.0592(8) 0.3613(3) 0.5948(3) 0.0825 1.0000 Uani D U . . . .
C214 C 0.3299(9) 0.4276(4) 0.5301(3) 0.0750 1.0000 Uani D U . . . .
C215 C 0.2578(8) 0.4456(4) 0.5402(2) 0.0725 1.0000 Uani D U . . . .
O216 O 0.2366(8) 0.4781(3) 0.5297(3) 0.0753 1.0000 Uani D U . . . .
C217 C 0.4861(10) 0.4031(3) 0.6109(3) 0.0749 1.0000 Uani D U . . . .
C218 C 0.4326(9) 0.4159(4) 0.6337(3) 0.0954 1.0000 Uani D U . . . .
O219 O 0.4648(12) 0.4352(4) 0.6527(3) 0.1527 1.0000 Uani D U . . . .
O220 O 0.2662(6) 0.1854(3) 0.6813(3) 0.1262 1.0000 Uani D U . . . .
C221 C 0.2970(10) 0.3243(6) 0.6437(4) 0.0819 1.0000 Uani D U . . . .
C222 C 0.3117(7) 0.2891(4) 0.6654(3) 0.0802 1.0000 Uani D U . . . .
C223 C 0.2786(8) 0.2524(4) 0.6622(3) 0.0876 1.0000 Uani D U . . . .
C224 C 0.2936(6) 0.2200(4) 0.6829(3) 0.0907 1.0000 Uani D U . . . .
O225 O 0.3408(6) 0.2296(4) 0.7049(3) 0.0932 1.0000 Uani D U . . . .
C226 C 0.3713(7) 0.2673(4) 0.7076(3) 0.0857 1.0000 Uani D U . . . .
C227 C 0.3597(7) 0.2985(5) 0.6887(3) 0.0797 1.0000 Uani D U . . . .
C228 C 0.3953(7) 0.3348(5) 0.6947(4) 0.0910 1.0000 Uani D U . . . .
C229 C 0.4399(9) 0.3387(6) 0.7181(3) 0.0928 1.0000 Uani D U . . . .
C230 C 0.4515(7) 0.3073(5) 0.7369(3) 0.0947 1.0000 Uani D U . . . .
C231 C 0.4160(7) 0.2708(6) 0.7311(3) 0.0882 1.0000 Uani D U . . . .
O232 O 0.4923(7) 0.3075(5) 0.7598(3) 0.1144 1.0000 Uani D U . . . .
C233 C 0.5295(10) 0.3466(7) 0.7649(6) 0.1486 1.0000 Uani D U . . . .
Eu3 Eu -0.01187(8) 0.41402(4) 0.61422(3) 0.0641 1.0000 Uani . . . . . .
N301 N -0.0988(10) 0.3517(5) 0.6123(4) 0.0823 1.0000 Uani D U . . . .
N302 N -0.1613(10) 0.4363(4) 0.6187(3) 0.0761 1.0000 Uani D U . . . .
N303 N -0.0485(8) 0.4465(5) 0.6627(4) 0.0740 1.0000 Uani D U . . . .
N304 N 0.0091(7) 0.3605(4) 0.6592(4) 0.0797 1.0000 Uani D U . . . .
O301 O -0.0641(5) 0.4063(4) 0.5687(3) 0.0812 1.0000 Uani D U . . . .
O302 O -0.0401(7) 0.4848(4) 0.60769(19) 0.0703 1.0000 Uani D U . . . .
O303 O 0.0913(8) 0.4376(3) 0.6406(3) 0.0698 1.0000 Uani D U . . . .
O309 O 0.0738(9) 0.4465(4) 0.5790(3) 0.0771 1.0000 Uani . U . . . .
C301 C -0.1744(10) 0.3600(6) 0.6230(5) 0.0925 1.0000 Uani D U . . . .
C302 C -0.1917(13) 0.3983(4) 0.6069(5) 0.0820 1.0000 Uani D U . . . .
C303 C -0.1788(11) 0.4465(6) 0.6481(4) 0.0769 1.0000 Uani D U . . . .
C304 C -0.1175(9) 0.4714(6) 0.6614(5) 0.0818 1.0000 Uani D U . . . .
C305 C -0.0519(13) 0.4175(6) 0.6862(5) 0.0862 1.0000 Uani D U . . . .
C306 C 0.0041(12) 0.3835(6) 0.6856(4) 0.0790 1.0000 Uani D U . . . .
C307 C -0.0516(12) 0.3302(6) 0.6589(5) 0.0872 1.0000 Uani D U . . . .
C308 C -0.0748(14) 0.3172(5) 0.6299(5) 0.0946 1.0000 Uani D U . . . .
C311 C -0.0957(7) 0.3403(6) 0.5828(4) 0.0937 1.0000 Uani D U . . . .
C312 C -0.0945(6) 0.3729(4) 0.5608(4) 0.1001 1.0000 Uani D U . . . .
O313 O -0.1206(6) 0.3677(6) 0.5368(3) 0.1496 1.0000 Uani D U . . . .
C314 C -0.1642(10) 0.4680(4) 0.5975(2) 0.0807 1.0000 Uani D U . . . .
C315 C -0.1017(8) 0.4984(4) 0.5980(2) 0.0693 1.0000 Uani D U . . . .
O316 O -0.1079(8) 0.5344(3) 0.58966(18) 0.0650 1.0000 Uani D U . . . .
C317 C 0.0118(9) 0.4738(4) 0.6712(4) 0.0815 1.0000 Uani D U . . . .
C318 C 0.0877(9) 0.4576(3) 0.6637(3) 0.0741 1.0000 Uani D U . . . .
O319 O 0.1395(9) 0.4646(3) 0.6803(3) 0.0956 1.0000 Uani D U . . . .
O320 O 0.0845(7) 0.2116(4) 0.7042(3) 0.1465 1.0000 Uani D U . . . .
C321 C 0.0770(9) 0.3380(6) 0.6539(4) 0.0848 1.0000 Uani D U . . . .
C322 C 0.1059(7) 0.3122(5) 0.6795(3) 0.0891 1.0000 Uani D U . . . .
C323 C 0.0794(8) 0.2734(4) 0.6787(3) 0.0989 1.0000 Uani D U . . . .
C324 C 0.1053(7) 0.2476(4) 0.7026(3) 0.1114 1.0000 Uani D U . . . .
O325 O 0.1525(7) 0.2623(4) 0.7236(3) 0.1134 1.0000 Uani D U . . . .
C326 C 0.1759(8) 0.3017(5) 0.7220(4) 0.1047 1.0000 Uani D U . . . .
C327 C 0.1554(7) 0.3281(5) 0.7008(3) 0.0970 1.0000 Uani D U . . . .
C328 C 0.1849(8) 0.3671(6) 0.7026(4) 0.0983 1.0000 Uani D U . . . .
C329 C 0.2318(9) 0.3797(7) 0.7240(3) 0.1066 1.0000 Uani D U . . . .
C330 C 0.2552(8) 0.3550(6) 0.7459(3) 0.1190 1.0000 Uani D U . . . .
C331 C 0.2230(8) 0.3170(7) 0.7425(4) 0.1149 1.0000 Uani D U . . . .
O332 O 0.2999(8) 0.3658(6) 0.7666(3) 0.1251 1.0000 Uani D U . . . .
C333 C 0.3310(11) 0.4070(7) 0.7685(6) 0.1628 1.0000 Uani D U . . . .
Eu4 Eu -0.04191(8) 0.59617(4) 0.58293(3) 0.0564 1.0000 Uani . . . . . .
N401 N 0.0047(8) 0.6500(4) 0.5439(3) 0.0607 1.0000 Uani D U . . . .
N402 N -0.1057(8) 0.5831(4) 0.5337(3) 0.0603 1.0000 Uani D U . . . .
N403 N -0.1886(10) 0.6091(4) 0.5845(3) 0.0683 1.0000 Uani D U . . . .
N404 N -0.0684(8) 0.6774(5) 0.5954(3) 0.0716 1.0000 Uani D U . . . .
O401 O 0.0820(8) 0.6191(2) 0.5863(3) 0.0592 1.0000 Uani D U . . . .
O402 O 0.0195(7) 0.5483(3) 0.55335(19) 0.0592 1.0000 Uani D U . . . .
O403 O -0.0934(8) 0.5980(2) 0.6297(3) 0.0699 1.0000 Uani D U . . . .
O409 O 0.0374(8) 0.5574(4) 0.6144(3) 0.0611 1.0000 Uani . U . . . .
C401 C -0.0427(12) 0.6474(5) 0.5187(4) 0.0651 1.0000 Uani D U . . . .
C402 C -0.0594(12) 0.6034(4) 0.5122(4) 0.0646 1.0000 Uani D U . . . .
C403 C -0.1839(9) 0.5977(6) 0.5333(4) 0.0679 1.0000 Uani D U . . . .
C404 C -0.2221(10) 0.5882(6) 0.5605(3) 0.0657 1.0000 Uani D U . . . .
C405 C -0.2030(12) 0.6530(4) 0.5840(5) 0.0782 1.0000 Uani D U . . . .
C406 C -0.1490(9) 0.6763(6) 0.6023(4) 0.0745 1.0000 Uani D U . . . .
C407 C -0.0597(12) 0.7036(5) 0.5706(4) 0.0728 1.0000 Uani D U . . . .
C408 C 0.0087(11) 0.6926(4) 0.5538(4) 0.0715 1.0000 Uani D U . . . .
C411 C 0.0787(8) 0.6336(3) 0.5373(3) 0.0608 1.0000 Uani D U . . . .
C412 C 0.1200(8) 0.6262(3) 0.5641(3) 0.0582 1.0000 Uani D U . . . .
O413 O 0.1894(7) 0.6284(2) 0.5652(3) 0.0557 1.0000 Uani D U . . . .
C414 C -0.0961(8) 0.5395(4) 0.5286(2) 0.0630 1.0000 Uani D U . . . .
C415 C -0.0227(7) 0.5238(3) 0.5397(2) 0.0620 1.0000 Uani D U . . . .
O416 O -0.0029(7) 0.4875(3) 0.5359(2) 0.0705 1.0000 Uani D U . . . .
C417 C -0.2144(10) 0.5914(3) 0.6105(3) 0.0684 1.0000 Uani D U . . . .
C418 C -0.1627(8) 0.5909(3) 0.6348(3) 0.0620 1.0000 Uani D U . . . .
O419 O -0.1799(9) 0.5847(2) 0.6593(3) 0.0699 1.0000 Uani D U . . . .
O420 O 0.0177(6) 0.8277(3) 0.6375(3) 0.0919 1.0000 Uani D U . . . .
C421 C -0.0160(9) 0.6842(5) 0.6182(4) 0.0744 1.0000 Uani D U . . . .
C422 C -0.0315(7) 0.7234(4) 0.6362(3) 0.0737 1.0000 Uani D U . . . .
C423 C 0.0040(8) 0.7573(3) 0.6266(3) 0.0770 1.0000 Uani D U . . . .
C424 C -0.0112(6) 0.7943(4) 0.6437(2) 0.0818 1.0000 Uani D U . . . .
O425 O -0.0576(5) 0.7927(3) 0.6669(2) 0.0775 1.0000 Uani D U . . . .
C426 C -0.0903(7) 0.7570(3) 0.6745(3) 0.0759 1.0000 Uani D U . . . .
C427 C -0.0799(7) 0.7208(4) 0.6603(3) 0.0718 1.0000 Uani D U . . . .
C428 C -0.1148(7) 0.6856(5) 0.6696(4) 0.0811 1.0000 Uani D U . . . .
C429 C -0.1612(8) 0.6851(5) 0.6929(3) 0.0836 1.0000 Uani D U . . . .
C430 C -0.1727(7) 0.7210(4) 0.7074(3) 0.0913 1.0000 Uani D U . . . .
C431 C -0.1367(7) 0.7553(5) 0.6976(3) 0.0821 1.0000 Uani D U . . . .
O432 O -0.2135(6) 0.7293(4) 0.7295(3) 0.0926 1.0000 Uani D U . . . .
C433 C -0.2507(8) 0.6923(5) 0.7394(4) 0.0968 1.0000 Uani D U . . . .
Na1 Na 0.2328(5) 0.5350(2) 0.50263(17) 0.0706 1.0000 Uani . U . . . .
S1 S 0.3471(4) 0.5187(2) 0.44666(12) 0.1133 1.0000 Uani D U . . . .
O51 O 0.3718(7) 0.4914(4) 0.42363(18) 0.1828 1.0000 Uani D U . . . .
O52 O 0.3588(7) 0.5630(3) 0.4414(3) 0.1495 1.0000 Uani D U . . . .
O53 O 0.2739(4) 0.5080(4) 0.4595(2) 0.0935 1.0000 Uani D U . . . .
C54 C 0.4119(4) 0.5079(2) 0.47367(14) 0.0968 1.0000 Uani D U . . . .
F55 F 0.4777(4) 0.5238(4) 0.4687(2) 0.1274 1.0000 Uani D U . . . .
F56 F 0.3897(6) 0.5223(4) 0.49790(15) 0.0991 1.0000 Uani D U . . . .
F57 F 0.4220(7) 0.4687(3) 0.4769(2) 0.1328 1.0000 Uani D U . . . .
O58 O 0.1159(9) 0.5565(4) 0.4904(3) 0.0821 1.0000 Uani . U . . . .
H1011 H 0.4451 0.6399 0.5903 0.0796 1.0000 Uiso R . . . . .
H1012 H 0.4643 0.6502 0.5595 0.0796 1.0000 Uiso R . . . . .
H1022 H 0.5078 0.5864 0.5670 0.0785 1.0000 Uiso R . . . . .
H1021 H 0.4392 0.5820 0.5475 0.0785 1.0000 Uiso R . . . . .
H1031 H 0.4513 0.5988 0.6182 0.0818 1.0000 Uiso R . . . . .
H1032 H 0.5002 0.5603 0.6146 0.0818 1.0000 Uiso R . . . . .
H1041 H 0.4315 0.5495 0.6546 0.0773 1.0000 Uiso R . . . . .
H1042 H 0.3961 0.5220 0.6319 0.0773 1.0000 Uiso R . . . . .
H1051 H 0.3642 0.6086 0.6701 0.0812 1.0000 Uiso R . . . . .
H1052 H 0.3923 0.6239 0.6414 0.0812 1.0000 Uiso R . . . . .
H1061 H 0.3048 0.6681 0.6598 0.0676 1.0000 Uiso R . . . . .
H1062 H 0.2456 0.6338 0.6590 0.0676 1.0000 Uiso R . . . . .
H1072 H 0.3237 0.7078 0.6174 0.0738 1.0000 Uiso R . . . . .
H1071 H 0.3819 0.6730 0.6168 0.0738 1.0000 Uiso R . . . . .
H1081 H 0.3651 0.7022 0.5726 0.0764 1.0000 Uiso R . . . . .
H1082 H 0.2835 0.6866 0.5734 0.0764 1.0000 Uiso R . . . . .
H1111 H 0.2962 0.6630 0.5337 0.0805 1.0000 Uiso R . . . . .
H1112 H 0.3772 0.6518 0.5253 0.0805 1.0000 Uiso R . . . . .
H1141 H 0.4627 0.5094 0.5809 0.0719 1.0000 Uiso R . . . . .
H1142 H 0.4130 0.5236 0.5563 0.0719 1.0000 Uiso R . . . . .
H1172 H 0.2939 0.5570 0.6758 0.0766 1.0000 Uiso R . . . . .
H1171 H 0.2890 0.5223 0.6540 0.0766 1.0000 Uiso R . . . . .
H1211 H 0.1688 0.6533 0.6226 0.0680 1.0000 Uiso R . . . . .
H1212 H 0.2003 0.6840 0.6011 0.0680 1.0000 Uiso R . . . . .
H1231 H 0.2377 0.7503 0.6165 0.0751 1.0000 Uiso R . . . . .
H1281 H 0.1219 0.6412 0.6634 0.0796 1.0000 Uiso R . . . . .
H1291 H 0.0514 0.6336 0.7039 0.0921 1.0000 Uiso R . . . . .
H1311 H 0.0703 0.7551 0.7174 0.0926 1.0000 Uiso R . . . . .
H1331 H -0.0384 0.6585 0.7623 0.1441 1.0000 Uiso R . . . . .
H1332 H 0.0306 0.6389 0.7481 0.1441 1.0000 Uiso R . . . . .
H1333 H -0.0415 0.6465 0.7310 0.1441 1.0000 Uiso R . . . . .
H2011 H 0.3153 0.3051 0.5438 0.0946 1.0000 Uiso R . . . . .
H2012 H 0.2363 0.3039 0.5306 0.0946 1.0000 Uiso R . . . . .
H2022 H 0.2470 0.3698 0.5193 0.0932 1.0000 Uiso R . . . . .
H2021 H 0.3195 0.3494 0.5086 0.0932 1.0000 Uiso R . . . . .
H2031 H 0.4168 0.3463 0.5368 0.0912 1.0000 Uiso R . . . . .
H2032 H 0.4319 0.3858 0.5201 0.0912 1.0000 Uiso R . . . . .
H2041 H 0.4740 0.4164 0.5582 0.0832 1.0000 Uiso R . . . . .
H2042 H 0.5131 0.3744 0.5581 0.0832 1.0000 Uiso R . . . . .
H2051 H 0.5089 0.3344 0.5978 0.0980 1.0000 Uiso R . . . . .
H2052 H 0.4397 0.3222 0.5802 0.0980 1.0000 Uiso R . . . . .
H2061 H 0.4336 0.3380 0.6376 0.1021 1.0000 Uiso R . . . . .
H2062 H 0.4370 0.2946 0.6252 0.1021 1.0000 Uiso R . . . . .
H2072 H 0.3121 0.2640 0.6125 0.0984 1.0000 Uiso R . . . . .
H2071 H 0.3509 0.2837 0.5870 0.0984 1.0000 Uiso R . . . . .
H2081 H 0.2009 0.2881 0.5976 0.0988 1.0000 Uiso R . . . . .
H2082 H 0.2370 0.2660 0.5725 0.0988 1.0000 Uiso R . . . . .
H2111 H 0.1576 0.3578 0.5499 0.0860 1.0000 Uiso R . . . . .
H2112 H 0.1317 0.3156 0.5604 0.0860 1.0000 Uiso R . . . . .
H2141 H 0.3708 0.4435 0.5363 0.0896 1.0000 Uiso R . . . . .
H2142 H 0.3298 0.4268 0.5103 0.0896 1.0000 Uiso R . . . . .
H2172 H 0.5229 0.3855 0.6185 0.0935 1.0000 Uiso R . . . . .
H2171 H 0.5097 0.4262 0.6030 0.0935 1.0000 Uiso R . . . . .
H2211 H 0.3100 0.3490 0.6527 0.0973 1.0000 Uiso R . . . . .
H2212 H 0.2453 0.3246 0.6393 0.0973 1.0000 Uiso R . . . . .
H2231 H 0.2461 0.2473 0.6469 0.1073 1.0000 Uiso R . . . . .
H2281 H 0.3890 0.3574 0.6826 0.1070 1.0000 Uiso R . . . . .
H2291 H 0.4631 0.3642 0.7213 0.1081 1.0000 Uiso R . . . . .
H2311 H 0.4226 0.2481 0.7431 0.1026 1.0000 Uiso R . . . . .
H2331 H 0.5580 0.3448 0.7816 0.1676 1.0000 Uiso R . . . . .
H2332 H 0.4930 0.3673 0.7668 0.1676 1.0000 Uiso R . . . . .
H2333 H 0.5616 0.3528 0.7498 0.1676 1.0000 Uiso R . . . . .
H3011 H -0.1749 0.3644 0.6425 0.1136 1.0000 Uiso R . . . . .
H3012 H -0.2082 0.3387 0.6184 0.1136 1.0000 Uiso R . . . . .
H3022 H -0.2443 0.4011 0.6054 0.1002 1.0000 Uiso R . . . . .
H3021 H -0.1708 0.3953 0.5888 0.1002 1.0000 Uiso R . . . . .
H3031 H -0.2240 0.4616 0.6485 0.0931 1.0000 Uiso R . . . . .
H3032 H -0.1847 0.4221 0.6583 0.0931 1.0000 Uiso R . . . . .
H3041 H -0.1320 0.4792 0.6797 0.0983 1.0000 Uiso R . . . . .
H3042 H -0.1082 0.4950 0.6506 0.0983 1.0000 Uiso R . . . . .
H3051 H -0.0429 0.4328 0.7027 0.1008 1.0000 Uiso R . . . . .
H3052 H -0.1006 0.4062 0.6870 0.1008 1.0000 Uiso R . . . . .
H3061 H -0.0096 0.3646 0.6997 0.0891 1.0000 Uiso R . . . . .
H3062 H 0.0521 0.3942 0.6897 0.0891 1.0000 Uiso R . . . . .
H3072 H -0.0939 0.3410 0.6682 0.1056 1.0000 Uiso R . . . . .
H3071 H -0.0342 0.3069 0.6685 0.1056 1.0000 Uiso R . . . . .
H3081 H -0.1149 0.2985 0.6315 0.1158 1.0000 Uiso R . . . . .
H3082 H -0.0336 0.3042 0.6212 0.1158 1.0000 Uiso R . . . . .
H3111 H -0.1391 0.3247 0.5791 0.1118 1.0000 Uiso R . . . . .
H3112 H -0.0526 0.3239 0.5803 0.1118 1.0000 Uiso R . . . . .
H3141 H -0.2084 0.4830 0.6010 0.0961 1.0000 Uiso R . . . . .
H3142 H -0.1669 0.4560 0.5795 0.0961 1.0000 Uiso R . . . . .
H3172 H 0.0101 0.4762 0.6909 0.0945 1.0000 Uiso R . . . . .
H3171 H 0.0042 0.4997 0.6630 0.0945 1.0000 Uiso R . . . . .
H3211 H 0.1151 0.3569 0.6493 0.1003 1.0000 Uiso R . . . . .
H3212 H 0.0685 0.3204 0.6385 0.1003 1.0000 Uiso R . . . . .
H3231 H 0.0475 0.2635 0.6644 0.1177 1.0000 Uiso R . . . . .
H3281 H 0.1721 0.3862 0.6885 0.1170 1.0000 Uiso R . . . . .
H3291 H 0.2485 0.4070 0.7237 0.1230 1.0000 Uiso R . . . . .
H3311 H 0.2358 0.2982 0.7567 0.1331 1.0000 Uiso R . . . . .
H3331 H 0.3621 0.4098 0.7844 0.1895 1.0000 Uiso R . . . . .
H3332 H 0.2905 0.4255 0.7698 0.1895 1.0000 Uiso R . . . . .
H3333 H 0.3592 0.4126 0.7522 0.1895 1.0000 Uiso R . . . . .
H4011 H -0.0884 0.6610 0.5222 0.0791 1.0000 Uiso R . . . . .
H4012 H -0.0181 0.6598 0.5034 0.0791 1.0000 Uiso R . . . . .
H4022 H -0.0134 0.5893 0.5108 0.0777 1.0000 Uiso R . . . . .
H4021 H -0.0848 0.6022 0.4948 0.0777 1.0000 Uiso R . . . . .
H4031 H -0.1846 0.6261 0.5300 0.0832 1.0000 Uiso R . . . . .
H4032 H -0.2100 0.5842 0.5187 0.0832 1.0000 Uiso R . . . . .
H4041 H -0.2728 0.5965 0.5590 0.0757 1.0000 Uiso R . . . . .
H4042 H -0.2200 0.5598 0.5638 0.0757 1.0000 Uiso R . . . . .
H4051 H -0.2529 0.6589 0.5893 0.0945 1.0000 Uiso R . . . . .
H4052 H -0.1947 0.6619 0.5654 0.0945 1.0000 Uiso R . . . . .
H4061 H -0.1663 0.7035 0.6039 0.0884 1.0000 Uiso R . . . . .
H4062 H -0.1522 0.6634 0.6200 0.0884 1.0000 Uiso R . . . . .
H4072 H -0.0559 0.7311 0.5766 0.0864 1.0000 Uiso R . . . . .
H4071 H -0.1026 0.7005 0.5592 0.0864 1.0000 Uiso R . . . . .
H4081 H 0.0519 0.6961 0.5650 0.0839 1.0000 Uiso R . . . . .
H4082 H 0.0116 0.7100 0.5380 0.0839 1.0000 Uiso R . . . . .
H4111 H 0.1052 0.6531 0.5265 0.0717 1.0000 Uiso R . . . . .
H4112 H 0.0746 0.6090 0.5270 0.0717 1.0000 Uiso R . . . . .
H4141 H -0.1351 0.5252 0.5378 0.0759 1.0000 Uiso R . . . . .
H4142 H -0.0984 0.5343 0.5092 0.0759 1.0000 Uiso R . . . . .
H4172 H -0.2589 0.6048 0.6161 0.0839 1.0000 Uiso R . . . . .
H4171 H -0.2252 0.5638 0.6065 0.0839 1.0000 Uiso R . . . . .
H4211 H -0.0196 0.6616 0.6304 0.0908 1.0000 Uiso R . . . . .
H4212 H 0.0331 0.6857 0.6108 0.0908 1.0000 Uiso R . . . . .
H4231 H 0.0355 0.7573 0.6107 0.0937 1.0000 Uiso R . . . . .
H4281 H -0.1067 0.6609 0.6599 0.1002 1.0000 Uiso R . . . . .
H4291 H -0.1844 0.6607 0.6988 0.1028 1.0000 Uiso R . . . . .
H4311 H -0.1446 0.7800 0.7075 0.1012 1.0000 Uiso R . . . . .
H4331 H -0.2805 0.6980 0.7554 0.1182 1.0000 Uiso R . . . . .
H4332 H -0.2136 0.6729 0.7442 0.1182 1.0000 Uiso R . . . . .
H4333 H -0.2813 0.6818 0.7250 0.1182 1.0000 Uiso R . . . . .
H1091 H 0.1172 0.5415 0.5623 0.0652 1.0000 Uiso R . . . . .
H1092 H 0.1861 0.5115 0.5623 0.0652 1.0000 Uiso R . . . . .
H2091 H 0.1809 0.4440 0.6272 0.0732 1.0000 Uiso R . . . . .
H2092 H 0.2548 0.4720 0.6227 0.0732 1.0000 Uiso R . . . . .
H3091 H 0.1226 0.4403 0.5726 0.0892 1.0000 Uiso R . . . . .
H3092 H 0.0482 0.4603 0.5645 0.0892 1.0000 Uiso R . . . . .
H4091 H 0.0887 0.5617 0.6183 0.0720 1.0000 Uiso R . . . . .
H4092 H 0.0143 0.5354 0.6238 0.0720 1.0000 Uiso R . . . . .
H581 H 0.0774 0.5415 0.4816 0.0972 1.0000 Uiso R . . . . .
H582 H 0.1165 0.5820 0.4811 0.0972 1.0000 Uiso R . . . . .

_refine_ls_extinction_method     None
_oxford_refine_ls_scale          0.13981(11)
loop_
_geom_bond_atom_site_label_1
_geom_bond_site_symmetry_1
_geom_bond_atom_site_label_2
_geom_bond_site_symmetry_2
_geom_bond_distance
_geom_bond_publ_flag
Eu1 . N101 . 2.720(15) yes
Eu1 . N102 . 2.708(16) yes
Eu1 . N103 . 2.671(16) yes
Eu1 . N104 . 2.727(14) yes
Eu1 . O101 . 2.383(13) yes
Eu1 . O102 . 2.427(11) yes
Eu1 . O103 . 2.331(13) yes
Eu1 . O109 . 2.606(12) yes
Eu1 . C111 . 3.441(17) yes
Eu1 . O413 . 2.383(11) yes
N101 . C101 . 1.482(9) yes
N101 . C108 . 1.477(9) yes
N101 . C111 . 1.467(9) yes
N102 . C102 . 1.473(9) yes
N102 . C103 . 1.478(9) yes
N102 . C114 . 1.475(9) yes
N103 . C104 . 1.478(9) yes
N103 . C105 . 1.479(9) yes
N103 . C117 . 1.466(9) yes
N104 . C106 . 1.477(9) yes
N104 . C107 . 1.489(9) yes
N104 . C121 . 1.448(8) yes
O101 . C112 . 1.276(9) yes
O101 . Na1 . 2.530(16) yes
O102 . C115 . 1.290(8) yes
O103 . C118 . 1.271(9) yes
O109 . H1091 . 0.950 no
O109 . H1092 . 0.950 no
C101 . C102 . 1.519(9) yes
C101 . H1011 . 0.950 no
C101 . H1012 . 0.950 no
C102 . H1022 . 0.950 no
C102 . H1021 . 0.950 no
C103 . C104 . 1.525(9) yes
C103 . H1031 . 0.950 no
C103 . H1032 . 0.950 no
C104 . H1041 . 0.950 no
C104 . H1042 . 0.950 no
C105 . C106 . 1.507(9) yes
C105 . H1051 . 0.950 no
C105 . H1052 . 0.950 no
C106 . H1061 . 0.950 no
C106 . H1062 . 0.950 no
C107 . C108 . 1.512(9) yes
C107 . H1072 . 0.950 no
C107 . H1071 . 0.950 no
C108 . H1081 . 0.950 no
C108 . H1082 . 0.950 no
C111 . C112 . 1.506(9) yes
C111 . H1111 . 0.950 no
C111 . H1112 . 0.950 no
C112 . O113 . 1.243(9) yes
O113 . Na1 . 2.434(16) yes
C114 . C115 . 1.500(9) yes
C114 . H1141 . 0.950 no
C114 . H1142 . 0.950 no
C115 . O116 . 1.248(8) yes
O116 . Eu2 . 2.426(12) yes
C117 . C118 . 1.507(9) yes
C117 . H1172 . 0.950 no
C117 . H1171 . 0.950 no
C118 . O119 . 1.241(9) yes
O120 . C124 . 1.246(8) yes
C121 . C122 . 1.576(9) yes
C121 . H1211 . 0.950 no
C121 . H1212 . 0.950 no
C122 . C123 . 1.375(9) yes
C122 . C127 . 1.450(9) yes
C123 . C124 . 1.490(8) yes
C123 . H1231 . 0.950 no
C124 . O125 . 1.400(8) yes
O125 . C126 . 1.362(9) yes
C126 . C127 . 1.392(9) yes
C126 . C131 . 1.392(9) yes
C127 . C128 . 1.402(9) yes
C128 . C129 . 1.393(9) yes
C128 . H1281 . 0.950 no
C129 . C130 . 1.393(9) yes
C129 . H1291 . 0.950 no
C130 . C131 . 1.387(9) yes
C130 . O132 . 1.316(9) yes
C131 . H1311 . 0.950 no
O132 . C133 . 1.470(9) yes
C133 . H1331 . 0.950 no
C133 . H1332 . 0.950 no
C133 . H1333 . 0.950 no
Eu2 . N201 . 2.722(16) yes
Eu2 . N202 . 2.643(17) yes
Eu2 . N203 . 2.663(18) yes
Eu2 . N204 . 2.717(16) yes
Eu2 . O201 . 2.419(14) yes
Eu2 . O202 . 2.409(11) yes
Eu2 . O203 . 2.375(14) yes
Eu2 . O209 . 2.459(13) yes
N201 . C201 . 1.469(9) yes
N201 . C208 . 1.484(9) yes
N201 . C211 . 1.470(9) yes
N202 . C202 . 1.475(9) yes
N202 . C203 . 1.482(9) yes
N202 . C214 . 1.469(9) yes
N203 . C204 . 1.471(9) yes
N203 . C205 . 1.478(9) yes
N203 . C217 . 1.466(9) yes
N204 . C206 . 1.484(9) yes
N204 . C207 . 1.483(9) yes
N204 . C221 . 1.448(8) yes
O201 . C212 . 1.274(9) yes
O202 . C215 . 1.282(9) yes
O203 . C218 . 1.287(9) yes
O209 . H2091 . 0.950 no
O209 . H2092 . 0.950 no
C201 . C202 . 1.504(9) yes
C201 . H2011 . 0.950 no
C201 . H2012 . 0.950 no
C202 . H2022 . 0.950 no
C202 . H2021 . 0.950 no
C203 . C204 . 1.510(9) yes
C203 . H2031 . 0.950 no
C203 . H2032 . 0.950 no
C204 . H2041 . 0.950 no
C204 . H2042 . 0.950 no
C205 . C206 . 1.516(9) yes
C205 . H2051 . 0.950 no
C205 . H2052 . 0.950 no
C206 . H2061 . 0.950 no
C206 . H2062 . 0.950 no
C207 . C208 . 1.507(9) yes
C207 . H2072 . 0.950 no
C207 . H2071 . 0.950 no
C208 . H2081 . 0.950 no
C208 . H2082 . 0.950 no
C211 . C212 . 1.505(9) yes
C211 . H2111 . 0.950 no
C211 . H2112 . 0.950 no
C212 . O213 . 1.246(9) yes
O213 . Eu3 . 2.347(14) yes
C214 . C215 . 1.504(9) yes
C214 . H2141 . 0.950 no
C214 . H2142 . 0.950 no
C215 . O216 . 1.244(9) yes
O216 . Na1 . 2.279(15) yes
C217 . C218 . 1.515(9) yes
C217 . H2172 . 0.950 no
C217 . H2171 . 0.950 no
C218 . O219 . 1.253(9) yes
O220 . C224 . 1.243(8) yes
C221 . C222 . 1.578(9) yes
C221 . H2211 . 0.950 no
C221 . H2212 . 0.950 no
C222 . C223 . 1.358(9) yes
C222 . C227 . 1.444(9) yes
C223 . C224 . 1.485(8) yes
C223 . H2231 . 0.950 no
C224 . O225 . 1.388(8) yes
O225 . C226 . 1.365(9) yes
C226 . C227 . 1.387(9) yes
C226 . C231 . 1.387(9) yes
C227 . C228 . 1.384(9) yes
C228 . C229 . 1.384(9) yes
C228 . H2281 . 0.950 no
C229 . C230 . 1.388(9) yes
C229 . H2291 . 0.950 no
C230 . C231 . 1.390(9) yes
C230 . O232 . 1.320(9) yes
C231 . H2311 . 0.950 no
O232 . C233 . 1.472(9) yes
C233 . H2331 . 0.950 no
C233 . H2332 . 0.950 no
C233 . H2333 . 0.950 no
Eu3 . N301 . 2.579(17) yes
Eu3 . N302 . 2.785(19) yes
Eu3 . N303 . 2.643(18) yes
Eu3 . N304 . 2.813(17) yes
Eu3 . O301 . 2.390(16) yes
Eu3 . O302 . 2.408(12) yes
Eu3 . O303 . 2.372(14) yes
Eu3 . O309 . 2.520(15) yes
Eu3 . C301 . 3.440(19) yes
N301 . C301 . 1.475(9) yes
N301 . C308 . 1.483(9) yes
N301 . C311 . 1.462(9) yes
N302 . C302 . 1.478(9) yes
N302 . C303 . 1.481(9) yes
N302 . C314 . 1.458(9) yes
N303 . C304 . 1.485(9) yes
N303 . C305 . 1.481(9) yes
N303 . C317 . 1.464(9) yes
N304 . C306 . 1.478(9) yes
N304 . C307 . 1.477(9) yes
N304 . C321 . 1.448(9) yes
O301 . C312 . 1.286(9) yes
O302 . C315 . 1.280(9) yes
O303 . C318 . 1.289(9) yes
O309 . H3091 . 0.950 no
O309 . H3092 . 0.950 no
C301 . C302 . 1.511(9) yes
C301 . H3011 . 0.950 no
C301 . H3012 . 0.950 no
C302 . H3022 . 0.950 no
C302 . H3021 . 0.950 no
C303 . C304 . 1.513(9) yes
C303 . H3031 . 0.950 no
C303 . H3032 . 0.950 no
C304 . H3041 . 0.950 no
C304 . H3042 . 0.950 no
C305 . C306 . 1.504(9) yes
C305 . H3051 . 0.950 no
C305 . H3052 . 0.950 no
C306 . H3061 . 0.950 no
C306 . H3062 . 0.950 no
C307 . C308 . 1.510(9) yes
C307 . H3072 . 0.950 no
C307 . H3071 . 0.950 no
C308 . H3081 . 0.950 no
C308 . H3082 . 0.950 no
C311 . C312 . 1.507(9) yes
C311 . H3111 . 0.950 no
C311 . H3112 . 0.950 no
C312 . O313 . 1.253(9) yes
C314 . C315 . 1.504(9) yes
C314 . H3141 . 0.950 no
C314 . H3142 . 0.950 no
C315 . O316 . 1.254(9) yes
O316 . Eu4 . 2.375(12) yes
C317 . C318 . 1.505(9) yes
C317 . H3172 . 0.950 no
C317 . H3171 . 0.950 no
C318 . O319 . 1.244(9) yes
O320 . C324 . 1.245(8) yes
C321 . C322 . 1.579(9) yes
C321 . H3211 . 0.950 no
C321 . H3212 . 0.950 no
C322 . C323 . 1.362(9) yes
C322 . C327 . 1.452(9) yes
C323 . C324 . 1.503(9) yes
C323 . H3231 . 0.950 no
C324 . O325 . 1.401(8) yes
O325 . C326 . 1.366(9) yes
C326 . C327 . 1.390(9) yes
C326 . C331 . 1.392(9) yes
C327 . C328 . 1.393(9) yes
C328 . C329 . 1.390(9) yes
C328 . H3281 . 0.950 no
C329 . C330 . 1.393(9) yes
C329 . H3291 . 0.950 no
C330 . C331 . 1.386(9) yes
C330 . O332 . 1.323(9) yes
C331 . H3311 . 0.950 no
O332 . C333 . 1.469(9) yes
C333 . H3331 . 0.950 no
C333 . H3332 . 0.950 no
C333 . H3333 . 0.950 no
Eu4 . N401 . 2.710(16) yes
Eu4 . N402 . 2.657(16) yes
Eu4 . N403 . 2.665(17) yes
Eu4 . N404 . 2.784(16) yes
Eu4 . O401 . 2.351(14) yes
Eu4 . O402 . 2.390(11) yes
Eu4 . O403 . 2.424(14) yes
Eu4 . O409 . 2.434(13) yes
N401 . C401 . 1.481(9) yes
N401 . C408 . 1.482(9) yes
N401 . C411 . 1.468(9) yes
N402 . C402 . 1.486(9) yes
N402 . C403 . 1.482(9) yes
N402 . C414 . 1.467(9) yes
N403 . C404 . 1.472(9) yes
N403 . C405 . 1.470(9) yes
N403 . C417 . 1.452(9) yes
N404 . C406 . 1.483(9) yes
N404 . C407 . 1.478(9) yes
N404 . C421 . 1.459(8) yes
O401 . C412 . 1.283(8) yes
O402 . C415 . 1.287(9) yes
O403 . C418 . 1.287(9) yes
O409 . H4091 . 0.950 no
O409 . H4092 . 0.950 no
C401 . C402 . 1.511(9) yes
C401 . H4011 . 0.950 no
C401 . H4012 . 0.950 no
C402 . H4022 . 0.950 no
C402 . H4021 . 0.950 no
C403 . C404 . 1.508(9) yes
C403 . H4031 . 0.950 no
C403 . H4032 . 0.950 no
C404 . H4041 . 0.950 no
C404 . H4042 . 0.950 no
C405 . C406 . 1.516(9) yes
C405 . H4051 . 0.950 no
C405 . H4052 . 0.950 no
C406 . H4061 . 0.950 no
C406 . H4062 . 0.950 no
C407 . C408 . 1.513(9) yes
C407 . H4072 . 0.950 no
C407 . H4071 . 0.950 no
C408 . H4081 . 0.950 no
C408 . H4082 . 0.950 no
C411 . C412 . 1.506(9) yes
C411 . H4111 . 0.950 no
C411 . H4112 . 0.950 no
C412 . O413 . 1.247(8) yes
C414 . C415 . 1.509(9) yes
C414 . H4141 . 0.950 no
C414 . H4142 . 0.950 no
C415 . O416 . 1.261(8) yes
C417 . C418 . 1.488(9) yes
C417 . H4172 . 0.950 no
C417 . H4171 . 0.950 no
C418 . O419 . 1.232(9) yes
O420 . C424 . 1.250(8) yes
C421 . C422 . 1.576(9) yes
C421 . H4211 . 0.950 no
C421 . H4212 . 0.950 no
C422 . C423 . 1.364(9) yes
C422 . C427 . 1.449(9) yes
C423 . C424 . 1.495(8) yes
C423 . H4231 . 0.950 no
C424 . O425 . 1.393(8) yes
O425 . C426 . 1.364(9) yes
C426 . C427 . 1.387(9) yes
C426 . C431 . 1.387(9) yes
C427 . C428 . 1.391(9) yes
C428 . C429 . 1.391(9) yes
C428 . H4281 . 0.950 no
C429 . C430 . 1.386(9) yes
C429 . H4291 . 0.950 no
C430 . C431 . 1.383(9) yes
C430 . O432 . 1.316(9) yes
C431 . H4311 . 0.950 no
O432 . C433 . 1.471(9) yes
C433 . H4331 . 0.950 no
C433 . H4332 . 0.950 no
C433 . H4333 . 0.950 no
Na1 . O53 . 2.369(14) yes
Na1 . O58 . 2.289(18) yes
S1 . O51 . 1.491(5) yes
S1 . O52 . 1.494(5) yes
S1 . O53 . 1.492(5) yes
S1 . C54 . 1.776(4) yes
C54 . F55 . 1.312(5) yes
C54 . F56 . 1.317(5) yes
C54 . F57 . 1.313(5) yes
O58 . H581 . 0.950 no
O58 . H582 . 0.950 no
loop_
_geom_angle_atom_site_label_1
_geom_angle_site_symmetry_1
_geom_angle_atom_site_label_2
_geom_angle_site_symmetry_2
_geom_angle_atom_site_label_3
_geom_angle_site_symmetry_3
_geom_angle
_geom_angle_publ_flag
N101 . Eu1 . N102 . 67.0(4) yes
N101 . Eu1 . N103 . 103.4(4) yes
N102 . Eu1 . N103 . 66.0(4) yes
N101 . Eu1 . N104 . 67.3(4) yes
N102 . Eu1 . N104 . 101.0(3) yes
N103 . Eu1 . N104 . 66.9(4) yes
N101 . Eu1 . O101 . 64.7(4) yes
N102 . Eu1 . O101 . 74.4(4) yes
N103 . Eu1 . O101 . 139.9(4) yes
N104 . Eu1 . O101 . 129.3(4) yes
N101 . Eu1 . O102 . 130.8(4) yes
N102 . Eu1 . O102 . 66.7(4) yes
N103 . Eu1 . O102 . 71.9(3) yes
N104 . Eu1 . O102 . 138.3(3) yes
O101 . Eu1 . O102 . 87.4(3) yes
N101 . Eu1 . O103 . 143.3(3) yes
N102 . Eu1 . O103 . 127.3(4) yes
N103 . Eu1 . O103 . 65.0(4) yes
N104 . Eu1 . O103 . 76.4(3) yes
O101 . Eu1 . O103 . 146.3(4) yes
N101 . Eu1 . O109 . 129.1(4) yes
N102 . Eu1 . O109 . 122.0(4) yes
N103 . Eu1 . O109 . 126.6(4) yes
N104 . Eu1 . O109 . 137.0(4) yes
O101 . Eu1 . O109 . 70.4(4) yes
N101 . Eu1 . C111 . 24.1(3) yes
N102 . Eu1 . C111 . 77.0(3) yes
N103 . Eu1 . C111 . 126.7(4) yes
N104 . Eu1 . C111 . 85.3(4) yes
O101 . Eu1 . C111 . 44.1(3) yes
N101 . Eu1 . O413 . 71.9(4) yes
N102 . Eu1 . O413 . 135.9(4) yes
N103 . Eu1 . O413 . 141.5(4) yes
N104 . Eu1 . O413 . 76.6(3) yes
O101 . Eu1 . O413 . 74.1(4) yes
O102 . Eu1 . O103 . 80.9(3) yes
O102 . Eu1 . O109 . 67.0(3) yes
O103 . Eu1 . O109 . 75.9(4) yes
O102 . Eu1 . C111 . 126.2(3) yes
O103 . Eu1 . C111 . 151.6(3) yes
O109 . Eu1 . C111 . 105.0(4) yes
O102 . Eu1 . O413 . 140.6(3) yes
O103 . Eu1 . O413 . 95.5(4) yes
O109 . Eu1 . O413 . 74.0(3) yes
C111 . Eu1 . O413 . 58.9(3) yes
Eu1 . N101 . C101 . 108.0(11) yes
Eu1 . N101 . C108 . 106.6(11) yes
C101 . N101 . C108 . 110.1(14) yes
Eu1 . N101 . C111 . 106.6(9) yes
C101 . N101 . C111 . 115.1(14) yes
C108 . N101 . C111 . 110.0(12) yes
Eu1 . N102 . C102 . 110.1(11) yes
Eu1 . N102 . C103 . 107.9(11) yes
C102 . N102 . C103 . 110.5(15) yes
Eu1 . N102 . C114 . 103.2(10) yes
C102 . N102 . C114 . 108.1(11) yes
C103 . N102 . C114 . 116.7(13) yes
Eu1 . N103 . C104 . 112.8(11) yes
Eu1 . N103 . C105 . 108.2(11) yes
C104 . N103 . C105 . 109.4(14) yes
Eu1 . N103 . C117 . 108.0(11) yes
C104 . N103 . C117 . 109.2(12) yes
C105 . N103 . C117 . 109.2(13) yes
Eu1 . N104 . C106 . 112.4(9) yes
Eu1 . N104 . C107 . 112.2(9) yes
C106 . N104 . C107 . 108.8(13) yes
Eu1 . N104 . C121 . 110.6(9) yes
C106 . N104 . C121 . 105.5(11) yes
C107 . N104 . C121 . 106.9(14) yes
Eu1 . O101 . C112 . 122.9(10) yes
Eu1 . O101 . Na1 . 133.2(5) yes
C112 . O101 . Na1 . 89.7(10) yes
Eu1 . O102 . C115 . 121.4(9) yes
Eu1 . O103 . C118 . 129.7(11) yes
Eu1 . O109 . H1091 . 134.8 no
Eu1 . O109 . H1092 . 112.6 no
H1091 . O109 . H1092 . 112.6 no
N101 . C101 . C102 . 113.0(15) yes
N101 . C101 . H1011 . 109.2 no
C102 . C101 . H1011 . 109.2 no
N101 . C101 . H1012 . 108.1 no
C102 . C101 . H1012 . 107.8 no
H1011 . C101 . H1012 . 109.5 no
C101 . C102 . N102 . 108.3(14) yes
C101 . C102 . H1022 . 109.8 no
N102 . C102 . H1022 . 109.9 no
C101 . C102 . H1021 . 110.1 no
N102 . C102 . H1021 . 109.2 no
H1022 . C102 . H1021 . 109.5 no
N102 . C103 . C104 . 111.9(15) yes
N102 . C103 . H1031 . 108.8 no
C104 . C103 . H1031 . 108.6 no
N102 . C103 . H1032 . 109.2 no
C104 . C103 . H1032 . 108.8 no
H1031 . C103 . H1032 . 109.5 no
C103 . C104 . N103 . 104.5(14) yes
C103 . C104 . H1041 . 111.8 no
N103 . C104 . H1041 . 110.8 no
C103 . C104 . H1042 . 109.9 no
N103 . C104 . H1042 . 110.2 no
H1041 . C104 . H1042 . 109.5 no
N103 . C105 . C106 . 118.0(14) yes
N103 . C105 . H1051 . 107.0 no
C106 . C105 . H1051 . 107.8 no
N103 . C105 . H1052 . 107.1 no
C106 . C105 . H1052 . 107.3 no
H1051 . C105 . H1052 . 109.5 no
C105 . C106 . N104 . 105.6(14) yes
C105 . C106 . H1061 . 110.2 no
N104 . C106 . H1061 . 110.3 no
C105 . C106 . H1062 . 110.5 no
N104 . C106 . H1062 . 110.7 no
H1061 . C106 . H1062 . 109.5 no
N104 . C107 . C108 . 108.4(14) yes
N104 . C107 . H1072 . 109.8 no
C108 . C107 . H1072 . 110.5 no
N104 . C107 . H1071 . 109.9 no
C108 . C107 . H1071 . 108.8 no
H1072 . C107 . H1071 . 109.5 no
C107 . C108 . N101 . 116.2(14) yes
C107 . C108 . H1081 . 108.5 no
N101 . C108 . H1081 . 109.0 no
C107 . C108 . H1082 . 106.9 no
N101 . C108 . H1082 . 106.7 no
H1081 . C108 . H1082 . 109.5 no
N101 . C111 . Eu1 . 49.2(7) yes
N101 . C111 . C112 . 114.8(13) yes
Eu1 . C111 . C112 . 70.3(8) yes
N101 . C111 . H1111 . 107.3 no
Eu1 . C111 . H1111 . 103.0 no
C112 . C111 . H1111 . 107.7 no
N101 . C111 . H1112 . 109.0 no
Eu1 . C111 . H1112 . 145.8 no
C112 . C111 . H1112 . 108.5 no
H1111 . C111 . H1112 . 109.5 no
C111 . C112 . O101 . 118.7(14) yes
C111 . C112 . O113 . 119.6(13) yes
O101 . C112 . O113 . 121.7(14) yes
C112 . O113 . Na1 . 95.0(10) yes
N102 . C114 . C115 . 117.4(12) yes
N102 . C114 . H1141 . 108.5 no
C115 . C114 . H1141 . 107.4 no
N102 . C114 . H1142 . 106.8 no
C115 . C114 . H1142 . 107.0 no
H1141 . C114 . H1142 . 109.5 no
C114 . C115 . O102 . 118.3(12) yes
C114 . C115 . O116 . 121.3(12) yes
O102 . C115 . O116 . 120.5(13) yes
C115 . O116 . Eu2 . 144.1(11) yes
N103 . C117 . C118 . 113.3(13) yes
N103 . C117 . H1172 . 108.5 no
C118 . C117 . H1172 . 108.6 no
N103 . C117 . H1171 . 108.7 no
C118 . C117 . H1171 . 108.3 no
H1172 . C117 . H1171 . 109.5 no
C117 . C118 . O103 . 114.2(14) yes
C117 . C118 . O119 . 120.5(15) yes
O103 . C118 . O119 . 125.3(16) yes
N104 . C121 . C122 . 123.3(9) yes
N104 . C121 . H1211 . 104.9 no
C122 . C121 . H1211 . 103.9 no
N104 . C121 . H1212 . 107.0 no
C122 . C121 . H1212 . 107.7 no
H1211 . C121 . H1212 . 109.5 no
C121 . C122 . C123 . 114.3(13) yes
C121 . C122 . C127 . 123.6(13) yes
C123 . C122 . C127 . 122.1(13) yes
C122 . C123 . C124 . 116.7(13) yes
C122 . C123 . H1231 . 121.4 no
C124 . C123 . H1231 . 121.9 no
C123 . C124 . O120 . 122.2(9) yes
C123 . C124 . O125 . 120.2(11) yes
O120 . C124 . O125 . 117.7(9) yes
C124 . O125 . C126 . 120.5(12) yes
O125 . C126 . C127 . 122.3(14) yes
O125 . C126 . C131 . 115.3(13) yes
C127 . C126 . C131 . 122.4(14) yes
C122 . C127 . C126 . 118.3(13) yes
C122 . C127 . C128 . 125.6(13) yes
C126 . C127 . C128 . 116.1(14) yes
C127 . C128 . C129 . 123.6(17) yes
C127 . C128 . H1281 . 117.9 no
C129 . C128 . H1281 . 118.5 no
C128 . C129 . C130 . 117.7(18) yes
C128 . C129 . H1291 . 120.8 no
C130 . C129 . H1291 . 121.5 no
C129 . C130 . C131 . 121.1(17) yes
C129 . C130 . O132 . 129.0(18) yes
C131 . C130 . O132 . 110.0(16) yes
C126 . C131 . C130 . 119.2(16) yes
C126 . C131 . H1311 . 120.7 no
C130 . C131 . H1311 . 120.0 no
C130 . O132 . C133 . 108.2(18) yes
O132 . C133 . H1331 . 109.3 no
O132 . C133 . H1332 . 109.7 no
H1331 . C133 . H1332 . 109.5 no
O132 . C133 . H1333 . 109.4 no
H1331 . C133 . H1333 . 109.5 no
H1332 . C133 . H1333 . 109.5 no
O116 . Eu2 . N201 . 142.5(4) yes
O116 . Eu2 . N202 . 77.1(4) yes
N201 . Eu2 . N202 . 66.2(4) yes
O116 . Eu2 . N203 . 69.6(4) yes
N201 . Eu2 . N203 . 102.8(5) yes
N202 . Eu2 . N203 . 69.4(5) yes
O116 . Eu2 . N204 . 134.1(4) yes
N201 . Eu2 . N204 . 66.1(4) yes
N202 . Eu2 . N204 . 104.5(4) yes
N203 . Eu2 . N204 . 68.5(4) yes
O116 . Eu2 . O201 . 137.4(4) yes
N201 . Eu2 . O201 . 62.3(4) yes
N202 . Eu2 . O201 . 118.6(5) yes
N203 . Eu2 . O201 . 151.6(4) yes
N204 . Eu2 . O201 . 83.1(4) yes
O116 . Eu2 . O202 . 75.0(3) yes
N201 . Eu2 . O202 . 80.7(4) yes
N202 . Eu2 . O202 . 61.3(5) yes
N203 . Eu2 . O202 . 124.1(5) yes
N204 . Eu2 . O202 . 146.7(4) yes
O116 . Eu2 . O203 . 75.0(3) yes
N201 . Eu2 . O203 . 138.0(4) yes
N202 . Eu2 . O203 . 134.9(5) yes
N203 . Eu2 . O203 . 67.9(5) yes
N204 . Eu2 . O203 . 72.6(4) yes
O116 . Eu2 . O209 . 73.1(4) yes
N201 . Eu2 . O209 . 127.4(5) yes
N202 . Eu2 . O209 . 132.3(4) yes
N203 . Eu2 . O209 . 129.4(4) yes
N204 . Eu2 . O209 . 123.0(4) yes
O201 . Eu2 . O202 . 79.4(4) yes
O201 . Eu2 . O203 . 105.9(5) yes
O202 . Eu2 . O203 . 139.6(3) yes
O201 . Eu2 . O209 . 67.7(4) yes
O202 . Eu2 . O209 . 75.4(4) yes
O203 . Eu2 . O209 . 70.3(4) yes
Eu2 . N201 . C201 . 112.6(11) yes
Eu2 . N201 . C208 . 116.4(12) yes
C201 . N201 . C208 . 108.4(15) yes
Eu2 . N201 . C211 . 102.2(9) yes
C201 . N201 . C211 . 107.4(15) yes
C208 . N201 . C211 . 109.2(12) yes
Eu2 . N202 . C202 . 116.3(12) yes
Eu2 . N202 . C203 . 113.2(11) yes
C202 . N202 . C203 . 106.1(16) yes
Eu2 . N202 . C214 . 104.6(10) yes
C202 . N202 . C214 . 111.7(12) yes
C203 . N202 . C214 . 104.4(14) yes
Eu2 . N203 . C204 . 109.7(11) yes
Eu2 . N203 . C205 . 106.6(13) yes
C204 . N203 . C205 . 106.9(14) yes
Eu2 . N203 . C217 . 112.2(11) yes
C204 . N203 . C217 . 116.0(14) yes
C205 . N203 . C217 . 104.9(15) yes
Eu2 . N204 . C206 . 109.5(11) yes
Eu2 . N204 . C207 . 110.9(11) yes
C206 . N204 . C207 . 111.7(16) yes
Eu2 . N204 . C221 . 99.8(9) yes
C206 . N204 . C221 . 113.5(15) yes
C207 . N204 . C221 . 110.9(18) yes
Eu2 . O201 . C212 . 120.6(10) yes
Eu2 . O202 . C215 . 116.2(9) yes
Eu2 . O203 . C218 . 116.1(11) yes
Eu2 . O209 . H2091 . 124.7 no
Eu2 . O209 . H2092 . 117.5 no
H2091 . O209 . H2092 . 117.9 no
N201 . C201 . C202 . 116.3(16) yes
N201 . C201 . H2011 . 106.9 no
C202 . C201 . H2011 . 105.6 no
N201 . C201 . H2012 . 108.6 no
C202 . C201 . H2012 . 109.7 no
H2011 . C201 . H2012 . 109.5 no
C201 . C202 . N202 . 112.7(16) yes
C201 . C202 . H2022 . 106.7 no
N202 . C202 . H2022 . 107.9 no
C201 . C202 . H2021 . 110.2 no
N202 . C202 . H2021 . 109.8 no
H2022 . C202 . H2021 . 109.5 no
N202 . C203 . C204 . 115.3(16) yes
N202 . C203 . H2031 . 106.5 no
C204 . C203 . H2031 . 106.4 no
N202 . C203 . H2032 . 109.0 no
C204 . C203 . H2032 . 110.0 no
H2031 . C203 . H2032 . 109.5 no
C203 . C204 . N203 . 118.6(17) yes
C203 . C204 . H2041 . 105.8 no
N203 . C204 . H2041 . 107.5 no
C203 . C204 . H2042 . 108.0 no
N203 . C204 . H2042 . 107.2 no
H2041 . C204 . H2042 . 109.5 no
N203 . C205 . C206 . 116.0(16) yes
N203 . C205 . H2051 . 106.8 no
C206 . C205 . H2051 . 106.7 no
N203 . C205 . H2052 . 108.6 no
C206 . C205 . H2052 . 109.0 no
H2051 . C205 . H2052 . 109.5 no
C205 . C206 . N204 . 107.7(16) yes
C205 . C206 . H2061 . 110.7 no
N204 . C206 . H2061 . 109.9 no
C205 . C206 . H2062 . 109.6 no
N204 . C206 . H2062 . 109.4 no
H2061 . C206 . H2062 . 109.5 no
N204 . C207 . C208 . 121.5(16) yes
N204 . C207 . H2072 . 107.7 no
C208 . C207 . H2072 . 107.5 no
N204 . C207 . H2071 . 105.4 no
C208 . C207 . H2071 . 104.8 no
H2072 . C207 . H2071 . 109.5 no
C207 . C208 . N201 . 108.4(16) yes
C207 . C208 . H2081 . 108.8 no
N201 . C208 . H2081 . 108.7 no
C207 . C208 . H2082 . 111.3 no
N201 . C208 . H2082 . 110.1 no
H2081 . C208 . H2082 . 109.5 no
N201 . C211 . C212 . 112.3(14) yes
N201 . C211 . H2111 . 108.6 no
C212 . C211 . H2111 . 108.6 no
N201 . C211 . H2112 . 108.7 no
C212 . C211 . H2112 . 109.1 no
H2111 . C211 . H2112 . 109.5 no
C211 . C212 . O201 . 116.5(15) yes
C211 . C212 . O213 . 123.1(15) yes
O201 . C212 . O213 . 120.4(17) yes
C212 . O213 . Eu3 . 130.6(11) yes
N202 . C214 . C215 . 107.9(13) yes
N202 . C214 . H2141 . 110.0 no
C215 . C214 . H2141 . 109.9 no
N202 . C214 . H2142 . 110.1 no
C215 . C214 . H2142 . 109.5 no
H2141 . C214 . H2142 . 109.5 no
C214 . C215 . O202 . 118.0(13) yes
C214 . C215 . O216 . 118.1(14) yes
O202 . C215 . O216 . 123.9(16) yes
C215 . O216 . Na1 . 161.4(14) yes
N203 . C217 . C218 . 108.1(15) yes
N203 . C217 . H2172 . 109.2 no
C218 . C217 . H2172 . 109.4 no
N203 . C217 . H2171 . 110.3 no
C218 . C217 . H2171 . 110.3 no
H2172 . C217 . H2171 . 109.5 no
C217 . C218 . O203 . 129.7(17) yes
C217 . C218 . O219 . 112.0(16) yes
O203 . C218 . O219 . 118.3(18) yes
N204 . C221 . C222 . 116.0(10) yes
N204 . C221 . H2211 . 107.7 no
C222 . C221 . H2211 . 106.9 no
N204 . C221 . H2212 . 108.2 no
C222 . C221 . H2212 . 108.5 no
H2211 . C221 . H2212 . 109.5 no
C221 . C222 . C223 . 120.5(16) yes
C221 . C222 . C227 . 116.8(15) yes
C223 . C222 . C227 . 122.6(15) yes
C222 . C223 . C224 . 119.1(15) yes
C222 . C223 . H2231 . 120.8 no
C224 . C223 . H2231 . 120.1 no
C223 . C224 . O220 . 122.9(10) yes
C223 . C224 . O225 . 117.2(13) yes
O220 . C224 . O225 . 119.9(9) yes
C224 . O225 . C226 . 121.5(13) yes
O225 . C226 . C227 . 123.7(16) yes
O225 . C226 . C231 . 112.5(14) yes
C227 . C226 . C231 . 123.9(15) yes
C222 . C227 . C226 . 115.9(15) yes
C222 . C227 . C228 . 128.3(15) yes
C226 . C227 . C228 . 115.7(16) yes
C227 . C228 . C229 . 121.0(20) yes
C227 . C228 . H2281 . 119.6 no
C229 . C228 . H2281 . 119.4 no
C228 . C229 . C230 . 123(2) yes
C228 . C229 . H2291 . 117.9 no
C230 . C229 . H2291 . 119.0 no
C229 . C230 . C231 . 116.4(18) yes
C229 . C230 . O232 . 128.5(19) yes
C231 . C230 . O232 . 115.1(16) yes
C230 . C231 . C226 . 120.0(17) yes
C230 . C231 . H2311 . 120.0 no
C226 . C231 . H2311 . 120.0 no
C230 . O232 . C233 . 113.1(19) yes
O232 . C233 . H2331 . 109.3 no
O232 . C233 . H2332 . 109.4 no
H2331 . C233 . H2332 . 109.5 no
O232 . C233 . H2333 . 109.7 no
H2331 . C233 . H2333 . 109.5 no
H2332 . C233 . H2333 . 109.5 no
O213 . Eu3 . N301 . 74.0(5) yes
O213 . Eu3 . N302 . 138.3(5) yes
N301 . Eu3 . N302 . 68.4(5) yes
O213 . Eu3 . N303 . 141.7(5) yes
N301 . Eu3 . N303 . 101.8(5) yes
N302 . Eu3 . N303 . 65.6(5) yes
O213 . Eu3 . N304 . 76.7(4) yes
N301 . Eu3 . N304 . 67.0(5) yes
N302 . Eu3 . N304 . 103.5(4) yes
N303 . Eu3 . N304 . 67.1(4) yes
O213 . Eu3 . O301 . 76.7(4) yes
N301 . Eu3 . O301 . 69.2(5) yes
N302 . Eu3 . O301 . 73.8(4) yes
N303 . Eu3 . O301 . 138.6(4) yes
N304 . Eu3 . O301 . 133.4(5) yes
O213 . Eu3 . O302 . 141.2(3) yes
N301 . Eu3 . O302 . 129.7(5) yes
N302 . Eu3 . O302 . 63.4(4) yes
N303 . Eu3 . O302 . 70.7(4) yes
N304 . Eu3 . O302 . 137.3(4) yes
O213 . Eu3 . O303 . 91.9(5) yes
N301 . Eu3 . O303 . 138.7(4) yes
N302 . Eu3 . O303 . 128.4(5) yes
N303 . Eu3 . O303 . 65.8(5) yes
N304 . Eu3 . O303 . 72.0(4) yes
O213 . Eu3 . O309 . 73.6(4) yes
N301 . Eu3 . O309 . 132.9(5) yes
N302 . Eu3 . O309 . 121.7(5) yes
N303 . Eu3 . O309 . 124.7(5) yes
N304 . Eu3 . O309 . 134.3(4) yes
O213 . Eu3 . C301 . 97.2(5) yes
N301 . Eu3 . C301 . 23.2(4) yes
N302 . Eu3 . C301 . 46.6(4) yes
N303 . Eu3 . C301 . 83.8(5) yes
N304 . Eu3 . C301 . 72.3(5) yes
O301 . Eu3 . O302 . 84.3(4) yes
O301 . Eu3 . O303 . 145.9(4) yes
O302 . Eu3 . O303 . 85.2(4) yes
O301 . Eu3 . O309 . 70.8(5) yes
O302 . Eu3 . O309 . 68.3(4) yes
O303 . Eu3 . O309 . 75.2(4) yes
O301 . Eu3 . C301 . 74.0(5) yes
O302 . Eu3 . C301 . 109.8(4) yes
O303 . Eu3 . C301 . 139.9(5) yes
O309 . Eu3 . C301 . 144.8(6) yes
Eu3 . N301 . C301 . 113.3(12) yes
Eu3 . N301 . C308 . 114.5(13) yes
C301 . N301 . C308 . 102.1(16) yes
Eu3 . N301 . C311 . 102.5(11) yes
C301 . N301 . C311 . 114.8(16) yes
C308 . N301 . C311 . 110.2(16) yes
Eu3 . N302 . C302 . 95.8(12) yes
Eu3 . N302 . C303 . 109.7(11) yes
C302 . N302 . C303 . 118.6(16) yes
Eu3 . N302 . C314 . 99.7(11) yes
C302 . N302 . C314 . 109.0(13) yes
C303 . N302 . C314 . 119.5(14) yes
Eu3 . N303 . C304 . 113.2(13) yes
Eu3 . N303 . C305 . 114.9(13) yes
C304 . N303 . C305 . 110.7(16) yes
Eu3 . N303 . C317 . 108.1(12) yes
C304 . N303 . C317 . 106.6(13) yes
C305 . N303 . C317 . 102.4(14) yes
Eu3 . N304 . C306 . 109.2(11) yes
Eu3 . N304 . C307 . 108.4(12) yes
C306 . N304 . C307 . 108.2(16) yes
Eu3 . N304 . C321 . 107.3(11) yes
C306 . N304 . C321 . 117.7(16) yes
C307 . N304 . C321 . 105.7(17) yes
Eu3 . O301 . C312 . 121.8(12) yes
Eu3 . O302 . C315 . 124.7(10) yes
Eu3 . O303 . C318 . 125.9(11) yes
Eu3 . O309 . H3091 . 133.4 no
Eu3 . O309 . H3092 . 113.6 no
H3091 . O309 . H3092 . 108.1 no
N301 . C301 . C302 . 99.5(16) yes
Eu3 . C301 . C302 . 71.3(11) yes
N301 . C301 . H3011 . 112.3 no
Eu3 . C301 . H3011 . 92.8 no
C302 . C301 . H3011 . 112.0 no
N301 . C301 . H3012 . 111.7 no
Eu3 . C301 . H3012 . 153.2 no
C302 . C301 . H3012 . 111.6 no
H3011 . C301 . H3012 . 109.5 no
C301 . C302 . N302 . 115.9(17) yes
C301 . C302 . H3022 . 108.7 no
N302 . C302 . H3022 . 108.3 no
C301 . C302 . H3021 . 107.4 no
N302 . C302 . H3021 . 106.9 no
H3022 . C302 . H3021 . 109.5 no
N302 . C303 . C304 . 111.9(17) yes
N302 . C303 . H3031 . 108.8 no
C304 . C303 . H3031 . 109.1 no
N302 . C303 . H3032 . 108.9 no
C304 . C303 . H3032 . 108.7 no
H3031 . C303 . H3032 . 109.5 no
C303 . C304 . N303 . 108.8(15) yes
C303 . C304 . H3041 . 109.8 no
N303 . C304 . H3041 . 109.8 no
C303 . C304 . H3042 . 109.8 no
N303 . C304 . H3042 . 109.1 no
H3041 . C304 . H3042 . 109.5 no
N303 . C305 . C306 . 116.0(17) yes
N303 . C305 . H3051 . 106.6 no
C306 . C305 . H3051 . 107.3 no
N303 . C305 . H3052 . 108.6 no
C306 . C305 . H3052 . 108.7 no
H3051 . C305 . H3052 . 109.5 no
C305 . C306 . N304 . 116.0(17) yes
C305 . C306 . H3061 . 107.6 no
N304 . C306 . H3061 . 106.8 no
C305 . C306 . H3062 . 108.8 no
N304 . C306 . H3062 . 108.0 no
H3061 . C306 . H3062 . 109.5 no
N304 . C307 . C308 . 114.0(18) yes
N304 . C307 . H3072 . 109.2 no
C308 . C307 . H3072 . 108.7 no
N304 . C307 . H3071 . 107.3 no
C308 . C307 . H3071 . 108.1 no
H3072 . C307 . H3071 . 109.5 no
C307 . C308 . N301 . 112.8(17) yes
C307 . C308 . H3081 . 108.6 no
N301 . C308 . H3081 . 108.8 no
C307 . C308 . H3082 . 108.8 no
N301 . C308 . H3082 . 108.4 no
H3081 . C308 . H3082 . 109.5 no
N301 . C311 . C312 . 119.8(15) yes
N301 . C311 . H3111 . 106.8 no
C312 . C311 . H3111 . 105.3 no
N301 . C311 . H3112 . 107.4 no
C312 . C311 . H3112 . 107.7 no
H3111 . C311 . H3112 . 109.5 no
C311 . C312 . O301 . 114.1(16) yes
C311 . C312 . O313 . 122.8(16) yes
O301 . C312 . O313 . 123.1(18) yes
N302 . C314 . C315 . 116.2(13) yes
N302 . C314 . H3141 . 106.3 no
C315 . C314 . H3141 . 105.7 no
N302 . C314 . H3142 . 109.8 no
C315 . C314 . H3142 . 109.1 no
H3141 . C314 . H3142 . 109.5 no
C314 . C315 . O302 . 114.4(13) yes
C314 . C315 . O316 . 124.1(13) yes
O302 . C315 . O316 . 121.5(14) yes
C315 . O316 . Eu4 . 144.0(11) yes
N303 . C317 . C318 . 112.4(14) yes
N303 . C317 . H3172 . 107.8 no
C318 . C317 . H3172 . 107.2 no
N303 . C317 . H3171 . 109.4 no
C318 . C317 . H3171 . 110.4 no
H3172 . C317 . H3171 . 109.5 no
C317 . C318 . O303 . 115.6(15) yes
C317 . C318 . O319 . 117.2(16) yes
O303 . C318 . O319 . 127.3(18) yes
N304 . C321 . C322 . 114.5(11) yes
N304 . C321 . H3211 . 108.0 no
C322 . C321 . H3211 . 107.3 no
N304 . C321 . H3212 . 108.4 no
C322 . C321 . H3212 . 109.1 no
H3211 . C321 . H3212 . 109.5 no
C321 . C322 . C323 . 111.7(15) yes
C321 . C322 . C327 . 123.5(16) yes
C323 . C322 . C327 . 124.8(16) yes
C322 . C323 . C324 . 113.8(16) yes
C322 . C323 . H3231 . 123.4 no
C324 . C323 . H3231 . 122.8 no
C323 . C324 . O320 . 119.6(10) yes
C323 . C324 . O325 . 122.6(13) yes
O320 . C324 . O325 . 117.8(10) yes
C324 . O325 . C326 . 118.2(15) yes
O325 . C326 . C327 . 123.8(19) yes
O325 . C326 . C331 . 119.5(17) yes
C327 . C326 . C331 . 116.7(18) yes
C322 . C327 . C326 . 116.8(17) yes
C322 . C327 . C328 . 127.6(17) yes
C326 . C327 . C328 . 115.6(17) yes
C327 . C328 . C329 . 123(2) yes
C327 . C328 . H3281 . 118.2 no
C329 . C328 . H3281 . 118.4 no
C328 . C329 . C330 . 124(2) yes
C328 . C329 . H3291 . 117.3 no
C330 . C329 . H3291 . 118.2 no
C329 . C330 . C331 . 108(2) yes
C329 . C330 . O332 . 126(2) yes
C331 . C330 . O332 . 126(2) yes
C326 . C331 . C330 . 132(2) yes
C326 . C331 . H3311 . 114.5 no
C330 . C331 . H3311 . 113.9 no
C330 . O332 . C333 . 122(2) yes
O332 . C333 . H3331 . 111.3 no
O332 . C333 . H3332 . 107.8 no
H3331 . C333 . H3332 . 109.5 no
O332 . C333 . H3333 . 109.3 no
H3331 . C333 . H3333 . 109.5 no
H3332 . C333 . H3333 . 109.5 no
O316 . Eu4 . N401 . 143.9(4) yes
O316 . Eu4 . N402 . 76.6(4) yes
N401 . Eu4 . N402 . 68.0(4) yes
O316 . Eu4 . N403 . 69.0(4) yes
N401 . Eu4 . N403 . 102.7(4) yes
N402 . Eu4 . N403 . 68.1(4) yes
O316 . Eu4 . N404 . 135.2(4) yes
N401 . Eu4 . N404 . 64.7(4) yes
N402 . Eu4 . N404 . 105.9(3) yes
N403 . Eu4 . N404 . 70.9(4) yes
O316 . Eu4 . O401 . 137.4(4) yes
N401 . Eu4 . O401 . 63.0(4) yes
N402 . Eu4 . O401 . 121.3(4) yes
N403 . Eu4 . O401 . 151.5(4) yes
N404 . Eu4 . O401 . 80.7(4) yes
O316 . Eu4 . O402 . 75.2(3) yes
N401 . Eu4 . O402 . 83.1(3) yes
N402 . Eu4 . O402 . 64.2(4) yes
N403 . Eu4 . O402 . 125.2(4) yes
N404 . Eu4 . O402 . 147.2(4) yes
O316 . Eu4 . O403 . 72.9(3) yes
N401 . Eu4 . O403 . 137.7(3) yes
N402 . Eu4 . O403 . 131.4(5) yes
N403 . Eu4 . O403 . 66.0(5) yes
N404 . Eu4 . O403 . 73.3(4) yes
O316 . Eu4 . O409 . 75.9(4) yes
N401 . Eu4 . O409 . 126.2(4) yes
N402 . Eu4 . O409 . 135.8(4) yes
N403 . Eu4 . O409 . 129.9(5) yes
N404 . Eu4 . O409 . 118.0(4) yes
O401 . Eu4 . O402 . 79.5(4) yes
O401 . Eu4 . O403 . 106.7(5) yes
O402 . Eu4 . O403 . 137.8(3) yes
O401 . Eu4 . O409 . 64.8(4) yes
O402 . Eu4 . O409 . 75.7(4) yes
O403 . Eu4 . O409 . 70.2(4) yes
Eu4 . N401 . C401 . 110.4(11) yes
Eu4 . N401 . C408 . 114.5(11) yes
C401 . N401 . C408 . 110.1(14) yes
Eu4 . N401 . C411 . 100.8(9) yes
C401 . N401 . C411 . 108.6(14) yes
C408 . N401 . C411 . 112.0(11) yes
Eu4 . N402 . C402 . 107.8(11) yes
Eu4 . N402 . C403 . 111.6(11) yes
C402 . N402 . C403 . 111.8(14) yes
Eu4 . N402 . C414 . 104.9(9) yes
C402 . N402 . C414 . 105.0(11) yes
C403 . N402 . C414 . 115.2(14) yes
Eu4 . N403 . C404 . 107.8(11) yes
Eu4 . N403 . C405 . 109.2(12) yes
C404 . N403 . C405 . 112.1(14) yes
Eu4 . N403 . C417 . 106.0(10) yes
C404 . N403 . C417 . 110.8(13) yes
C405 . N403 . C417 . 110.8(14) yes
Eu4 . N404 . C406 . 101.0(10) yes
Eu4 . N404 . C407 . 111.7(10) yes
C406 . N404 . C407 . 107.3(15) yes
Eu4 . N404 . C421 . 101.5(9) yes
C406 . N404 . C421 . 117.6(15) yes
C407 . N404 . C421 . 116.5(17) yes
Eu4 . O401 . C412 . 120.1(10) yes
Eu4 . O402 . C415 . 116.5(8) yes
Eu4 . O403 . C418 . 122.6(11) yes
Eu4 . O409 . H4091 . 127.6 no
Eu4 . O409 . H4092 . 116.2 no
H4091 . O409 . H4092 . 116.2 no
N401 . C401 . C402 . 109.9(14) yes
N401 . C401 . H4011 . 108.9 no
C402 . C401 . H4011 . 108.6 no
N401 . C401 . H4012 . 110.0 no
C402 . C401 . H4012 . 110.1 no
H4011 . C401 . H4012 . 109.5 no
C401 . C402 . N402 . 113.5(15) yes
C401 . C402 . H4022 . 108.2 no
N402 . C402 . H4022 . 108.3 no
C401 . C402 . H4021 . 108.6 no
N402 . C402 . H4021 . 108.8 no
H4022 . C402 . H4021 . 109.5 no
N402 . C403 . C404 . 110.4(15) yes
N402 . C403 . H4031 . 109.5 no
C404 . C403 . H4031 . 110.0 no
N402 . C403 . H4032 . 108.9 no
C404 . C403 . H4032 . 108.5 no
H4031 . C403 . H4032 . 109.5 no
C403 . C404 . N403 . 113.4(16) yes
C403 . C404 . H4041 . 108.1 no
N403 . C404 . H4041 . 108.3 no
C403 . C404 . H4042 . 109.3 no
N403 . C404 . H4042 . 108.4 no
H4041 . C404 . H4042 . 109.5 no
N403 . C405 . C406 . 112.1(15) yes
N403 . C405 . H4051 . 111.1 no
C406 . C405 . H4051 . 110.2 no
N403 . C405 . H4052 . 107.0 no
C406 . C405 . H4052 . 106.8 no
H4051 . C405 . H4052 . 109.5 no
C405 . C406 . N404 . 120.3(16) yes
C405 . C406 . H4061 . 108.3 no
N404 . C406 . H4061 . 108.2 no
C405 . C406 . H4062 . 104.6 no
N404 . C406 . H4062 . 105.6 no
H4061 . C406 . H4062 . 109.5 no
N404 . C407 . C408 . 112.0(16) yes
N404 . C407 . H4072 . 108.7 no
C408 . C407 . H4072 . 109.4 no
N404 . C407 . H4071 . 108.4 no
C408 . C407 . H4071 . 108.8 no
H4072 . C407 . H4071 . 109.5 no
C407 . C408 . N401 . 111.0(15) yes
C407 . C408 . H4081 . 109.1 no
N401 . C408 . H4081 . 109.7 no
C407 . C408 . H4082 . 108.9 no
N401 . C408 . H4082 . 108.6 no
H4081 . C408 . H4082 . 109.5 no
N401 . C411 . C412 . 108.5(12) yes
N401 . C411 . H4111 . 108.7 no
C412 . C411 . H4111 . 109.1 no
N401 . C411 . H4112 . 110.9 no
C412 . C411 . H4112 . 110.1 no
H4111 . C411 . H4112 . 109.5 no
C411 . C412 . O401 . 118.6(14) yes
C411 . C412 . O413 . 121.1(13) yes
O401 . C412 . O413 . 120.3(14) yes
C412 . O413 . Eu1 . 126.6(9) yes
N402 . C414 . C415 . 112.3(12) yes
N402 . C414 . H4141 . 108.8 no
C415 . C414 . H4141 . 108.0 no
N402 . C414 . H4142 . 109.6 no
C415 . C414 . H4142 . 108.6 no
H4141 . C414 . H4142 . 109.5 no
C414 . C415 . O402 . 118.5(12) yes
C414 . C415 . O416 . 121.4(12) yes
O402 . C415 . O416 . 120.1(13) yes
N403 . C417 . C418 . 118.5(15) yes
N403 . C417 . H4172 . 108.8 no
C418 . C417 . H4172 . 107.9 no
N403 . C417 . H4171 . 105.8 no
C418 . C417 . H4171 . 106.1 no
H4172 . C417 . H4171 . 109.5 no
C417 . C418 . O403 . 116.8(15) yes
C417 . C418 . O419 . 126.2(15) yes
O403 . C418 . O419 . 116.9(15) yes
N404 . C421 . C422 . 114.9(10) yes
N404 . C421 . H4211 . 107.4 no
C422 . C421 . H4211 . 107.2 no
N404 . C421 . H4212 . 108.7 no
C422 . C421 . H4212 . 109.1 no
H4211 . C421 . H4212 . 109.5 no
C421 . C422 . C423 . 113.8(14) yes
C421 . C422 . C427 . 119.5(14) yes
C423 . C422 . C427 . 126.7(14) yes
C422 . C423 . C424 . 113.5(14) yes
C422 . C423 . H4231 . 123.3 no
C424 . C423 . H4231 . 123.2 no
C423 . C424 . O420 . 120.8(9) yes
C423 . C424 . O425 . 121.1(12) yes
O420 . C424 . O425 . 118.1(9) yes
C424 . O425 . C426 . 120.2(13) yes
O425 . C426 . C427 . 123.6(15) yes
O425 . C426 . C431 . 120.4(13) yes
C427 . C426 . C431 . 116.1(14) yes
C422 . C427 . C426 . 115.0(14) yes
C422 . C427 . C428 . 125.2(14) yes
C426 . C427 . C428 . 119.8(15) yes
C427 . C428 . C429 . 122.4(18) yes
C427 . C428 . H4281 . 119.0 no
C429 . C428 . H4281 . 118.5 no
C428 . C429 . C430 . 118.8(19) yes
C428 . C429 . H4291 . 120.7 no
C430 . C429 . H4291 . 120.6 no
C429 . C430 . C431 . 117.3(17) yes
C429 . C430 . O432 . 131.6(16) yes
C431 . C430 . O432 . 111.2(14) yes
C426 . C431 . C430 . 125.6(16) yes
C426 . C431 . H4311 . 117.0 no
C430 . C431 . H4311 . 117.4 no
C430 . O432 . C433 . 110.0(15) yes
O432 . C433 . H4331 . 110.7 no
O432 . C433 . H4332 . 108.5 no
H4331 . C433 . H4332 . 109.5 no
O432 . C433 . H4333 . 109.1 no
H4331 . C433 . H4333 . 109.5 no
H4332 . C433 . H4333 . 109.5 no
O216 . Na1 . O113 . 139.3(5) yes
O216 . Na1 . O101 . 89.5(4) yes
O113 . Na1 . O101 . 52.6(4) yes
O216 . Na1 . O53 . 100.4(5) yes
O113 . Na1 . O53 . 97.4(5) yes
O101 . Na1 . O53 . 133.4(5) yes
O216 . Na1 . O58 . 115.3(7) yes
O113 . Na1 . O58 . 96.9(5) yes
O101 . Na1 . O58 . 116.4(5) yes
O53 . Na1 . O58 . 100.2(5) yes
O51 . S1 . O52 . 115.05(5) yes
O51 . S1 . O53 . 115.05(5) yes
O52 . S1 . O53 . 115.05(5) yes
O51 . S1 . C54 . 103.07(5) yes
O52 . S1 . C54 . 103.07(5) yes
O53 . S1 . C54 . 103.06(5) yes
Na1 . O53 . S1 . 123.0(6) yes
S1 . C54 . F55 . 111.97(5) yes
S1 . C54 . F56 . 111.97(5) yes
F55 . C54 . F56 . 106.87(5) yes
S1 . C54 . F57 . 111.96(5) yes
F55 . C54 . F57 . 106.87(5) yes
F56 . C54 . F57 . 106.86(5) yes
Na1 . O58 . H581 . 128.1 no
Na1 . O58 . H582 . 112.6 no
H581 . O58 . H582 . 105.0 no
loop_
_geom_hbond_atom_site_label_D
_geom_hbond_site_symmetry_D
_geom_hbond_atom_site_label_H
_geom_hbond_site_symmetry_H
_geom_hbond_atom_site_label_A
_geom_hbond_site_symmetry_A
_geom_hbond_angle_DHA
_geom_hbond_distance_DH
_geom_hbond_distance_HA
_geom_hbond_distance_DA
_geom_hbond_publ_flag
C104 . H1042 . C115 . 129 0.95 2.50 3.18(2) yes
C106 . H1062 . C118 . 122 0.95 2.53 3.14(2) yes
C107 . H1072 . C123 . 136 0.95 2.53 3.28(2) yes
C107 . H1071 . C424 3_565 136 0.95 2.55 3.30(2) yes
C108 . H1082 . O413 . 121 0.95 2.58 3.18(2) yes
C121 . H1211 . O401 . 128 0.95 2.59 3.26(2) yes
C131 . H1311 . O232 6_456 157 0.95 2.47 3.37(2) yes
C206 . H2061 . C218 . 121 0.95 2.57 3.16(2) yes
C207 . H2072 . C223 . 134 0.95 2.49 3.22(2) yes
C221 . H2211 . O203 . 132 0.95 2.33 3.05(2) yes
C221 . H2212 . O201 . 130 0.95 2.51 3.20(2) yes
C231 . H2311 . O132 6_546 145 0.95 2.55 3.37(2) yes
C302 . H3021 . O301 . 137 0.95 2.17 2.94(2) yes
C302 . H3021 . C312 . 154 0.95 2.06 2.94(2) yes
C304 . H3042 . C315 . 126 0.95 2.53 3.18(2) yes
C307 . H3071 . C323 . 139 0.95 2.37 3.15(2) yes
C321 . H3211 . O201 . 133 0.95 2.28 3.01(2) yes
C331 . H3311 . O432 6_546 149 0.95 2.53 3.38(2) yes
C406 . H4062 . O403 . 123 0.95 2.44 3.06(2) yes
C406 . H4062 . C418 . 133 0.95 2.50 3.22(2) yes
C406 . H4062 . C428 . 133 0.95 2.58 3.30(2) yes
C411 . H4112 . O58 . 155 0.95 2.57 3.46(2) yes
C421 . H4211 . O403 . 134 0.95 2.48 3.21(2) yes
C428 . H4281 . O403 . 174 0.95 2.54 3.49(2) yes
O109 . H1091 . O402 . 180 0.95 1.82 2.77(2) yes
O109 . H1092 . O216 . 142 0.95 2.12 2.93(2) yes
O209 . H2091 . O303 . 179 0.95 1.74 2.69(2) yes
O209 . H2091 . C318 . 151 0.95 2.46 3.32(2) yes
O209 . H2092 . O102 . 130 0.95 1.98 2.70(2) yes
O309 . H3091 . O202 . 179 0.95 1.94 2.89(2) yes
O309 . H3092 . O416 . 180 0.95 1.88 2.83(2) yes
O409 . H4091 . O103 . 180 0.95 1.85 2.80(2) yes
O409 . H4091 . C118 . 152 0.95 2.58 3.45(2) yes
O409 . H4092 . O302 . 130 0.95 2.08 2.78(2) yes
O58 . H581 . C415 2_566 153 0.95 2.57 3.45(2) yes
O58 . H581 . O416 2_566 179 0.95 1.84 2.79(2) yes
O58 . H582 . O301 2_566 124 0.95 2.59 3.22(2) yes
O58 . H582 . C312 2_566 153 0.95 2.53 3.40(2) yes
O58 . H582 . O313 2_566 178 0.95 1.87 2.82(2) yes




############################################################# 
# start Validation Reply Form
############################################################# 
_vrf_REFNR01_EuL-Monoclinic      
;
PROBLEM: Ratio of reflections to parameters is < 6 for a
RESPONSE: The data were exceptionally weak, leading to a 
paucity of data.  The structure was improved with the 
inclusion of chemical knowledge in the form of same distance, 
thermal siilarity and vibrational restraints in order to 
maintain sensible geometric and displacement parameters.
Despite the challenges associated with the data, there is
no real doubt as to the connectivity, especially given the
other analytical evidence presented.
;
_vrf_PLAT410_EuL-Monoclinic      
;
PROBLEM: Short Intra H...H Contact H4211    ..H4281     .       1.75 Ang.  
RESPONSE: The hydrogen atoms were positioned geometrically 
or according to hydrogen bonding and, due to the constrianed 
nature of the molecule some of the hydrogen atoms are in
close proximity.
;
_vrf_PLAT026_EuL-Monoclinic      
;
PROBLEM: Ratio Observed / Unique Reflections (too) Low ..        38% Check   
RESPONSE: The data were exceptionally weak, due to lack of
order in the solvent sphere leading to a poor 
observed / unique data ratio.
;
_vrf_PLAT082_EuL-Monoclinic      
;
PROBLEM: Low Bond Precision on  C-C Bonds ...............    0.02136 Ang. 
RESPONSE: The poor qulity of the data led to a low precision 
model, but despite this, there is no real doubt as to the 
connectivity, especially given the other analytical evidence 
presented.
;
_vrf_REFNR01_EuL-Triclinic       
;
PROBLEM: Ratio of reflections to parameters is < 6 for a
RESPONSE: Despite collecting that data with synchrotron 
radiation, the data were stil very weak, leading to a 
lack of data.  The structure was controlled by the 
inclusion of chemical knowledge in the form of same distance, 
thermal siilarity and vibrational restraints in order to 
maintain sensible geometric and displacement parameters.
Despite the challenges associated with the data, there is
no real doubt as to the connectivity, especially given the
other analytical evidence presented.
;
_vrf_RINTA01_EuL-Triclinic       
;
PROBLEM: The value of Rint is greater than 0.25
RESPONSE: Due to a combination of the weakness of the data
and the radiation damage, the data do not agree well.  
Despite this, the structure solves and refines surprisingly 
well even without restraints.
;
_vrf_THETM01_EuL-Triclinic       
;
PROBLEM: The value of sine(theta_max)/wavelength is less than 0.550
RESPONSE: The data were very weak, leading to a lack of
high angle data.  The structure was controlled with the 
inclusion of chemical knowledge in the form of same distance, 
thermal siilarity and vibrational restraints.
;
_vrf_PLAT020_EuL-Triclinic       
;
PROBLEM: The Value of Rint is Greater Than 0.12 .........      0.400 Report
RESPONSE: Due to a combination of the weakness of the data
and the radiation damage, the data do not agree well.  
Despite this, the structure solves and refines surprisingly 
well even without restraints.
;
_vrf_PLAT023_EuL-Triclinic       
;
PROBLEM: Resolution (too) Low [sin(theta)/Lambda < 0.6]..      17.94 Degree
RESPONSE: The data were very weak, leading to a lack of
high angle data but despite this, there is no real doubt as 
to the connectivity, especially given the other analytical 
evidence presented.
;
_vrf_PLAT029_EuL-Triclinic       
;
PROBLEM: _diffrn_measured_fraction_theta_full value Low .      0.696 Why?  
RESPONSE: The use of high intensity synchrotron radiation
lead to severe radiation damage and an incomplete dataset.
The data are included here as the structure is different to
those collected elsewhere.
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_vrf_PLAT084_EuL-Orthorhombic    
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PROBLEM: High wR2 Value (i.e. > 0.25) ...................       0.47 Report
RESPONSE: The data were weak and exhibited streaks and other
additional non-Bragg features.  The possibility of twinning
was investigated, but to no avail.  The structure was improved 
with the inclusion of chemical knowledge in the form of same 
distance, thermal siilarity and vibrational restraints in 
order to maintain sensible geometric and displacement 
parameters.  Despite the challenges associated with the data, 
there is no real doubt as to the connectivity, especially 
given the other analytical evidence presented.
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_vrf_PLAT410_EuL-Orthorhombic    
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PROBLEM: Short Intra H...H Contact H1031    ..H1052     .       1.74 Ang.  
RESPONSE: The hydrogen atoms were positioned geometrically 
or according to hydrogen bonding and, due to the constrianed 
nature of the molecule some of the hydrogen atoms are in
close proximity.
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_vrf_THETM01_EuL-Orthorhombic    
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PROBLEM: The value of sine(theta_max)/wavelength is less than 0.575
RESPONSE: The data were very weak, leading to a lack of
high angle data.  The structure was controlled with the 
inclusion of chemical knowledge in the form of same distance, 
thermal siilarity and vibrational restraints.
;
_vrf_PLAT023_EuL-Orthorhombic    
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PROBLEM: Resolution (too) Low [sin(theta)/Lambda < 0.6]..      58.93 Degree
RESPONSE: The data were very weak, leading to a lack of
high angle data but despite this, there is no real doubt as 
to the connectivity, especially given the other analytical 
evidence presented.
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_vrf_PLAT082_EuL-Orthorhombic    
;
PROBLEM: High R1 Value ..................................       0.17 Report
RESPONSE: The data were weak and exhibited streaks and other
additional non-Bragg features.  The possibility of twinning
was investigated, but to no avail.  The structure was improved 
with the inclusion of chemical knowledge in the form of same 
distance, thermal siilarity and vibrational restraints in 
order to maintain sensible geometric and displacement 
parameters.  Despite the challenges associated with the data, 
there is no real doubt as to the connectivity, especially 
given the other analytical evidence presented.
;
_vrf_PLAT342_EuL-Orthorhombic    
;
PROBLEM: Low Bond Precision on  C-C Bonds ...............    0.02169 Ang. 
RESPONSE: The poor qulity of the data led to a low precision 
model, but despite this, there is no real doubt as to the 
connectivity, especially given the other analytical evidence 
presented.
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